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PP-II-127THE DESIGN OF THE ACTIVE COMPONENTS DISTRIBUTION THROUGHOUTTHE PORES OF DIFFERENT SIZE IN CATALYSTS OF HYDROCATALYTICPROCESSES (OIL REFINING)Smolikov M.D., Udras I.E., Belyi A.S.Institute of Hydrocarbon Processing SB RAS, Omsk, RussiaE-mail: udras@incat.okno.ruThe present-day condition of problem of catalyst active component distribution in thesupporter porous matrix is analyzed. An experimental approach for measurement of thequantity of surface centers of Pt, Pd and Mo in the pores with different size of hydrocatalyticprocesses catalysts on the basis of SiO 2 and Al 2 O 3 is suggested. The results of the influence ofpreparation parameters on the active components distribution on the surface of pores withdifferent radius are cited.Distribution of an active component (AC) in porous structure of hydrocatalytic processescatalysts is an important characteristic because it influences on the local concentration(density) of substances fixed on certain areas of supporter surface and so determines thestability of an active phase to agglomeration. Displacement of the active phase localization inthin supporter pores can determine its accessibility for reactive molecules and also stability todeactivation by coconut sediment at plugging (blocking) of thin pores by coconut. Thus thenature of AC distribution throughout the pores with different size will influence on theretention of catalyst operating characteristics at its exploitation to a great extent.During the preparation process of supported catalysts of hydrocatalytic processes(reforming, hydrofining) combination of diffusion and sorption processes on the soaking stageof porous matrixes of supporters by active substances controls penetration and consequentlydistribution of the active component not only throughout the volume of a supporter granule(this phenomenon is well-known and studied for a long time [1]). At the same time with thedisplacement of the active substances throughout a granule the migration of adsorbedpredecessors throughout the volume of the pores with different size with the followingprecipitation of the active substances in them always takes place. Because of diffusionprocesses the appearance of differences of metal concentration in thin and large pores wouldbe expected.In the work the present-day condition of problem of catalyst active componentdistribution in the supporter porous matrix is analyzed. An experimental approach formeasurement of the quantity of surface centers of Pt, Pd and Mo in the pores with different396
PP-II-127size of hydrocatalytic processes catalysts on the basis of SiO 2 and Al 2 O 3 is suggested. Theresults of the influence of preparation parameters on the active components distribution on thesurface of pores with different radius are cited.References1. Y.S.Shyr, W.Ernst://J.Catalysis, 63, 425 (1980).397
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"Catalysis is not a branch of chemi
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Siberian Branch of Russian Academy
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INTERNATIONAL ADVISORY COMMITTEE:A.
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POSTER PRESENTATIONSSECTION IMECHAN
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PP-I-1more time in the oxidised sta
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PP-I-2Study of chemical reactions p
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PP-I-3It is suggested that during p
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PP-I-4reaction conditions, 100% con
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PP-I-5Catalytic properties of synth
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PP-I-6iii) The magnitude of above m
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PP-I-8ONE-DIMENSIONAL AND THREE-DIM
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PP-I-8This work was carried out at
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PP-I-9formed on their place. The PI
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PP-I-10CatalystЕа 1 ,kJ/mol(77÷1
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PP-I-11to increase of selectivity t
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PP-I-12The nanostructure of CS (clu
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PP-I-13The exchange in high-tempera
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PP-I-15ROLE OF CARBON DIOXIDE IN TH
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PP-I-16DIRECT OXIDATION OF BENZENE
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PP-I-17DFT STUDY OF REDUCTION REACT
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PP-I-18ORIGINAL MONTE CARLO METHOD
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PP-I-19STUDY ON THE MECHANISM OF TH
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PP-I-20NANOSIZED METAL OXIDES AS ST
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PP-I-21THE STUDYING OF THE NATURE O
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PP-I-22SYNTHESIS OF ETHYLENE-BUTADI
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PP-I-24REACTION OF PHENYLACETYLENE
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PP-I-25EFFECT OF THE PRESSURE ON TH
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PP-I-26INTERPRETATION OF THE ETHYLE
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PP-I-27STUDY OF ONE-POT REDUCTIVE D
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PP-I-28TUNING SURFACE MORPHOLOGY OF
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PP-I-29HIGHLY POROUS BLOCK CELLULAR
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PP-I-30STRUCTURE OF PHOTOCATALYTIC
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PP-I-31According to the 13 C MAS NM
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PP-I-32Conversion and selectivity a
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PP-I-34STUDY OF THE MECHANISM OF CA
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PP-I-35COMPARISON CATALYTIC ACTIVIT
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PP-I-36CRITICAL PHENOMENA FOR LANGM
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PP-I-37ISOTHERMS FOR STEPPED SURFAC
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PP-I-38RESOLUTION OF CHIRAL SULFOXI
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PP-I-39INVESTIGATION OF AMINO-CONTA
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PP-I-40APPLICATION OF POSITRON ANNI
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PP-I-41large pores (15-100 μm) of
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PP-I-42 Pd(1x2) Pd(1x1) Pd(1x2)-c
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PP-I-43the Al/Zr molar ratio has an
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PP-I-44transferred on nickel throug
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PP-I-45S BET , XRD, TPR, SEM, TEM a
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PP-I-46normal and branched alkanes
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PP-I-47growth stages (2) and (3) -
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PP-I-48system operated at frequenci
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PP-I-49The reactivity of these mate
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PP-I-51RECONSTRUCTION OF THE Pd(pol
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PP-I-53INTERMEDIATE PRODUCTS IN PAR
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PP-I-55MOLECULAR MECHANISM OF LOW T
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PP-I-56size of metals encapsulated
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PP-I-57activity of synthetic cataly
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PP-I-58us to suggest that oxidation
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PP-I-59characteristics are as follo
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PP-I-60surfaces changes at 50% cove
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PP-I-611) using the parameter conti
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PP-I-62atoms to PhePA molecule. In
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PP-I-63interaction of CO molecule b
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PP-I-64cases method of Coats-Redfer
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PP-I-65adsorbates and metal atoms.
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PP-I-66were extrapolated then to th
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PP-I-67account an influence of oxyg
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PP-I-68been considered. With this a
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PP-I-70MODIFICATION OF ELECTRONIC S
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PP-I-71most of described methods ch
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PP-I-72Table 1Polymeric active carb
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PP-I-73lower than 450 °C with prac
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PP-I-74Fig. 1. Optimized structure
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PP-I-75(Zn Z d ). The catalytic cyc
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PP-I-76Photocatalytic reaction was
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PP-I-78FRAGMENT COMPOSITION OF DIES
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PP-I-79QUANTUM-CHEMICAL STUDIES OF
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PP-I-80INFUENCE OF CHEMICAL TREATME
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PP-I-81ADSORPTION OF SMALL SILVER S
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PP-I-82EXPLOSION SAFETY IN GAS TRAN
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PP-I-83(ONNO) ad → N 2 O ad + O a
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CATALYTIC ACTIVATION OF UNFAVOURABL
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PP-II-1Therefore, the observed incr
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PP-II-2The samples of uranium oxide
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PP-II-3catalysts prepared by hydrot
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PP-II-4[(C 6 H 5 ) 2 (CH 2 =CHSi] 2
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PP-II-6THE NEW Ni, Zr, Ti-CONTAININ
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PP-II-7SPATIALLY RESOLVED UV-VIS MI
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PP-II-8POLYOL MEDIATED SYNTHESIS OF
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PP-II-8CuO phase were detected, sug
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PP-II-9SHS-INTERMETALLIDES ON THE B
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PP-II-10CO OXIDATION IN HYDROGEN ST
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PP-II-11CATALYTIC PERFORMANCE OF CO
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PP-II-12FORMATION OF RADICAL CATION
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CATALYSTS MOLECULAR DESIGN BY SURFA
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PP-II-14THE CATALYTIC ACTIVITY OF F
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OXIDATION TRIMETHYLHYDROHYNONE IN T
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PP-II-16TECHNOLOGY CONCEPTS ON DEVE
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ACTIVATION OF POST-TITANOCENE OLEFI
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STRUCTURE FEATURES OF NANOCRYSTALLI
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THE H 2 ROLE IN SELECTIVE NO X REDU
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PP-II-20THE IN SITU FTIR STUDY OF T
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PP-II-21LUMINESCENT DIAGNOSTICS OF
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PP-II-22MODIFICATION OF PROPERTIES
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PP-II-23FTIR STUDY OF THE REACTION
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PP-II-24pores (the average diameter
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PP-II-25and the amount of the disso
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PP-II-27ACTIVITY OF PALLADIUM CATAL
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MODIFIED POLYOXIDE CATALYSTS FOR SY
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PP-II-29PRODUCTION OF HYDROGENCONTA
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INFLUENCE OF COMPOSITION AND STRUCT
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PP-II-311NEW COMPOSITE OF A POLYACE
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SOME ASPECTS OF THE SELECTION OF ST
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PP-II-33HYDROTREATING CATALYSTS MOD
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PP-II-34NORBORNADIENE IN NEW SHAPE-
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PP-II-36CATALYTIC SYSTEMS BASED ON
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PP-II-37EFFECT OF PHYSIOCHEMICAL PR
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PP-II-38INVESTIGATION OF STRUCTURE
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PP-II-38As a result of the combined
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PP-II-39synthesized by deposition-p
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PP-II-40halogen in NiX 2 (PPh 3 ) 2
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PP-II-41fell cell - with the requir
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PP-II-42SYNTHESIS OF CATALYSTS ON T
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PP-II-43-crucial role play peroxide
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PP-II-44According to the obtained d
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PP-II-46CYCLOALUMINATION OF α,ω-D
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PP-II-47ETHYLENE OLIGOMERIZATION TO
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PP-II-48aluminas are in the range o
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PP-II-49synthesis methods such as s
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PP-II-50Here, we report the first s
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PP-II-51hydrogenation. This peculia
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PP-II-524% and higher. Apparently t
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PP-II-53The secondary methods are b
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PP-II-55NOVEL CHIRAL NITROGEN CONTA
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PP-II-56NON-OXIDATIVE METHANE CONVE
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PP-II-57THE CATALYTIC ACTIVITY OF P
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PP-II-58The analysis of the raw mat
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PP-II-59analysis. Specific surface
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PP-II-60Ni-U catalysts were shown t
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PP-II-61Deep oxidation of CB vapors
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PP-II-62precipitate at 100 o C favo
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PP-II-63Х X n-С н-C 6 , %1008060
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PP-II-64mixture by microwave radiat
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PP-II-65and 99.995 % mass.) were sa
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PP-II-66CATALYTIC SYSTEMS BASED ON
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PHASE ANALYSIS OF MULTIELEMENT CATA
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PP-II-68EFFECT OF THE LIGAND SUBSTI
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PP-II-69Results and discussion: The
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PP-II-70tests in POM reaction and T
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PP-II-71The acidity, measured by tw
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PP-II-72The effect of nature and ac
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PP-II-74STUDY OF METHANE DEHYDROARO
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PP-II-75CATALYTIC OXIDATION OF ORGA
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Knowledge of the surface VO x speci
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PP-II-77propylene polymerization on
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THE EFFECT OF THE SUPPORT ON THE PE
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THE ACIDIC CATALYSIS IN REACTION OF
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HYDROGEN-RICH GAS PURIFICATION FROM
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PP-II-82During the stage of combine
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PP-II-83higher H 2 /propane ratios
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NANOSTRUCTURED MATERIALS BASED ON Z
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ELECTROCATALYTIC REDUCTION OF NITRO
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PP-II-87with CuKα radiation (λ ~
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PP-II-88The properties of the catal
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PP-II-89The stereospecificity of po
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PP-II-91SYNTHESIS AND CHARACTERIZAT
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PP-II-92INFLUENCE OF NATURE OF HETE
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PP-II-93OPTICALLY ACTIVE AMMONIUM S
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PP-II-94THE INFLUENCE OF FORMING CO
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PP-II-95NEW CATALYST OF LOW-TEMPERA
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PP-II-96DRIFTS AND UV-VIS STUDY OF
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PP-II-97NANOSTRUCTURED COMPLEX OXID
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PLATINUM CATALYSTS AND THEIR ACTIVI
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PP-II-99DESIGN OF STRUCTURED CATALY
Page 347 and 348: PP-II-100THE INFLUENCE OF CARBON ON
Page 349 and 350: PP-II-100sp 2 -carbon samples (Sibu
Page 351 and 352: PP-II-101Undoped LaMnO 3 has a stru
Page 353 and 354: PP-II-102The redox mechanisms of ca
Page 355 and 356: PP-II-103weak surface complexes of
Page 357 and 358: PP-II-104Ellipsometric, LA-XRD, TEM
Page 359 and 360: 357PP-II-105It follows that MAO (or
Page 361 and 362: PP-II-106For the description of met
Page 363 and 364: 361PP-II-1070.75, 1) were prepared
Page 365 and 366: PP-II-108(K⋅10 6 l/mole⋅mg⋅eq
Page 367 and 368: PP-II-110EFFECTS OF THE PROPERTIES
Page 369 and 370: PP-II-111CATALYTIC ACTIVITY OF POLY
Page 371 and 372: SYNTHESIS OF OXIRANES FROM RENEWABL
Page 373 and 374: PP-II-113SELECTIVE OXIDATION OF FOR
Page 375 and 376: BIODIESEL PRODUCTION FROM OLEIC ACI
Page 377 and 378: PP-II-115THE MECHANISM OF PHENOL OX
Page 379 and 380: PP-II-116THERMOSTABILITY OF Pd-ZEOL
Page 381 and 382: PP-II-117CO OXIDATION ON CuO-CeO 2
Page 383 and 384: PP-II-118THE ROLE OF I-CONTAINING P
Page 385 and 386: PP-II-119THE BULK POROUS ELECTRODE
Page 387 and 388: PP-II-120Methanol was suggested to
Page 389 and 390: PP-II-121Synthesis of catalysts on
Page 391 and 392: Yield, %PP-II-122Dynamics of variat
Page 393 and 394: PP-II-123The analysis of the hydroc
Page 395 and 396: PP-II-125THE MECHANISM OF COPPER CO
Page 397: PP-II-126The problem of the low act
Page 401 and 402: PP-II-128enhanced stability against
Page 403 and 404: PP-II-130HYDROGEN PRODUCTION BY MET
Page 405 and 406: CATALYTIC HYDROALKOXYCARBONYLATION
Page 407 and 408: NANOSTRUCTURED METAL-POLYMERIC CATA
Page 409 and 410: PP-II-133THE EFFECT OF THE SUPPORT
Page 411 and 412: PP-II-134АLTERNATIVE APPROACH TO D
Page 413 and 414: PP-II-135THE LOW-TEMPERATURE CATALY
Page 415 and 416: CATALYTIC PROPERTIES OF LAYERED OF
Page 417 and 418: PP-II-138EFFECT OF Zr ON THE OXIDAT
Page 419 and 420: PP-II-139THE NATURE OF ACTION OF TH
Page 421 and 422: PP-II-140CYCLOHEXANE OXIDATION OVER
Page 423 and 424: PP-II-141Mo AND W HETEROPOLYACID-CO
Page 425 and 426: HYDROCARBON CONVERSION CATALYSTS BA
Page 427 and 428: PP-II-142selectivity of the hexene-
Page 429 and 430: PP-II-143XPS, XRD and UV-Vis DRS st
Page 431 and 432: PP-II-144from the surface of sample
Page 433 and 434: PP-II-146THE INFLUENCE OF THE ACIDI
Page 435 and 436: PP-II-147CHARACTERISATION OF NEW GO
Page 437 and 438: STUDY ON THE REGULARITIES OF THE FO
Page 439 and 440: PP-II-148Platinum catalysts support
Page 441 and 442: PP-II-149selectivity to LHC, moreov
Page 443 and 444: PP-II-150steamed until a gel format
Page 445 and 446: PP-II-151ELECTRONIC STATE OF Cr n+
Page 447 and 448: PP-II-152METAL SUPPORTED CATALYSTS
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PP-II-153FORECASTING CATALYTIC CHAR
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RE - CONTENTING HC OXIDATION CATALY
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PP-II-155reaction are shown on the
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PP-II-156The product of stereoselec
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PP-II-157Supporting Pd on ZnO coate
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PP-II-158relating to acetone. With
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PP-II-159At the same time, catalyst
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PP-II-160The aim of our work is to
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PP-II-161crystallization state of t
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PP-II-162several carbon materials a
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PP-II-1625. J. M. H. Dirkx, H. S. v
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PP-III-1INFLUENCE OF DISSOLVED OXYG
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PP-III-2and microstructure, oxidati
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PP-III-3Aerosol, vapour of toxiccom
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PP-III-4inserted in PAn either in t
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PP-III-5The mechanism of pyrolysis
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ELECTROCATALYSTS WITH LOW PLATINUM
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PP-III-8VERY PURE SILICA FIBROUS AS
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PP-III-9METAL CONTAINING ZEOLITES -
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THE INFLUENCE OF TREATMENT METHOD O
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PARA-HYDROGEN INDUCED POLARIZATION
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PP-III-12NOVEL CHITOSAN-BASED CATAL
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PP-III-13Fig. 1. Dark adsorption (1
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PP-III-14residual pressure of 0.67
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PP-III-15using the same feedstock.
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PP-III-16Fig. 2. SEM-images of surf
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EPOXIDATION OF RAPESEED OIL BY HYDR
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PP-III-19THE PECULIARITIES OF CATAL
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PP-III-20CATALYTIC MEMBRANE CONTACT
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PP-III-21CATALYTIC ACTIVE LAYERS ON
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PP-III-22MODIFICATION OF COMPOUNDED
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EFFECT OF LIQUID POLYKETONE ON THE
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CATALYSTS SEARCH FOR α-METYLBENZYL
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PP-III-25PARTIAL OXIDATION OF PROPA
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PP-III-27BIODIESEL SYNTHESIS BY CAT
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PP-III-28PRODUCTION OF BIO-SYNGAS V
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PP-III-28Fig. 1. Changes in Н 2 an
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PP-III-29Table 1: Texture and adsor
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PP-III-30dimensionless front veloci
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PP-III-31synthesized. Experiments h
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PP-III-32It is established, that cr
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PP-III-33adsorptive catalysts in ad
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PP-III-34turbocompressor and two ca
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PP-III-35The Cu, Ni/ γ -Al 2 O 3 c
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PP-III-36pressure at 800-900 o C. T
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PP-III-370,50Concentration / Vol.-%
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PP-III-38HETEROGENEOUS-CATALYTIC DE
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PP-III-39HYDROISOMERIZATION OF CATA
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METHOD OF CATALYTIC UTILIZATION OF
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PP-III-41Catalytic properties of Fe
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PP-III-42heat in a steam-power unit
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PP-III-43In this way, the content o
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PP-III-45THE ECOLOGIC AND ECONOMIC
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PP-III-46INFLUENCE OF SUPPORT NATUR
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PP-III-47MIGRATION OF SUPPORTED PLA
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Table 2.PP-III-47The [Pt]/[Al] atom
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PP-III-48Under nitrogen atmosphere
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PP-III-49With aim to achieve the ho
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PP-III-50clinoptilolite (Aydag depo
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PP-III-51References1. Balzhinimaev
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PP-III-52Black light UV lamps. The
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USE OF THE NITROGEN-CONTAINING CARB
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PP-III-54CATALYTIC BEHAVIOUR OF VAR
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PP-III-55and sulfur, was spent (fig
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PP-III-56Specific reaction rates of
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PP-III-57special catalyst system wi
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PP-III-59UTILIZATION OF WASTE BIOMA
Page 585 and 586:
MECHANOCHEMISTRY AND MECHANO-CATALY
Page 587 and 588:
PP-III-62CATALYTIC INTENSIFICATION
Page 589 and 590:
PP-III-64ABOUT WHAT MANUFACTURE OF
Page 591 and 592:
PP-III-65OXDATIVE CONVERSION OF HYD
Page 593 and 594:
PP-III-66COMPLEX QUALITY CONTROL SY
Page 595 and 596:
PP-III-67INFLUENCE OF DIFFUSION, SI
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PP-III-68ONE STEP PROCESS FOR HYDRO
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FEATURES OF DRAG FACTOR FOR COMPLEX
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FIXED BED REACTORS WITH GRADIENT CA
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PP-III-70respective variational pro
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PP-III-71Operation at high volumetr
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PP-III-72It was performed the optim
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PP-III-73production stages of refin
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pik⎛N= fi ⎜∑j ∑⎝ j=1Nik,
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PP-III-75three MCP’s. In the seco
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PP-III-76during the reaction. The i
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PP-III-77enthalpy calculated for va
Page 619 and 620:
PP-III-78calculating kinetics of pa
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PP-III-79ventilators 7 and 10, flam
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PP-III-801) C 6 H 5 CH 3 + 2 [YO]
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PP-III-81Δm/m coating, %204060V=0.
Page 627 and 628:
PP-III-82• diameter of its genera
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PP-III-83ΔP,1mm H 2 O/m40023003420
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Concentration, vol.%PP-III-84The ef
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PP-III-85autocatalyst of thermoconv
Page 635 and 636:
PP-III-86The influence of such para
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PP-III-87hydrocarbons increases wit
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AUTOWAVE PROCESSES IN A STATIC CATA
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PP-III-90KINETIC AND THERMODYNAMIC
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PP-III-91which mathematical descrip
Page 645 and 646:
PP-III-93UTILIZATION OF LARGE-SCALE
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CATALYTIC TECHNOLOGY OF UTILIZATION
Page 649 and 650:
PP-III-95PROPERTIES AND ACTIVITY OF
Page 651 and 652:
PREPARATION AND CHARACTERIZATION OF
Page 653 and 654:
PP-III-98The comparison of TPR runs
Page 655:
ADVERTISEMENT
Page 658 and 659:
PerformancePassionSuccessAutomotive
Page 660 and 661:
Обслуживаемые рынк
Page 662:
Polyurethanes are an integral part
Page 666 and 667:
− prehydrotreating of gasolines a
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Kovalyov E. 123Kovtunov K. 489Kozlo
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List ofparticipantsABRAMOVA Anna Vs
Page 672 and 673:
BOEVA Olga AnatolievnaD.I. Mendelee
Page 674 and 675:
DJEKIC TanjaEindhoven University of
Page 676 and 677:
GIMUNDINOV Shamil AbzalovichD.V. So
Page 678 and 679:
KACHEVSKY Stanislav AndreevichLomon
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KONEV Vasily NikolayevichBoreskov I
Page 682 and 683:
LEDOUX Marc-JacquesCNRS DPI3 Rue Mi
Page 684 and 685:
MIERCZYŃSKI PawełInstitute of Gen
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OBYSKALOVA Elina AnatolievnaBoresko
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REBROV EvgenyEindhoven University o
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SHALAGINA Anastasia EvgenievnaBores
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SPIRIDONOV Alexey AlexeevichBoresko
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VEDYAGIN Alexei Anatol'evichBoresko
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ZAKHARENKO Valery SemenovitchBoresk
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Volume IVolume IICONTENTPOSTER PRES
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PP-I-25 Hocine S., Cherifi O., Bett
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PP-I-52 Timoshenkov S.P., Artemov E
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PP-I-80 Shinkarev V.V., Kuvshinov G
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PP-II-21 Chistoforova N.V., Yelkina
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PP-II-45 Khachani M., Boucetta C.,
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PP-II-68 Malinskaya M.Ju., Sviridov
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PP-II-90 Nikitin V., Mikenas T., Za
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PP-II-114 Sepúlveda J., Santarosa
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PP-II-139 Tkach V.S., Suslov D.S.,
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Section III. Environmental and indu
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PP-III-28 Yakovlev V.A., Kirillov V
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PP-III-52 Shelimov B., Tolkachev N.
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PP-III-77 Mel’gunov M., Kovalev M
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III International Conference“Cata
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