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DEPARTMENT OF ORGANIC CHEMISTRY Head of Department: Telephone: +421252968560 Prof. Tibor Gracza, PhD, DSc Fax: +421252968560 E-mail: tibor.gracza@stuba.sk I. STAFF Full Professors: Prof. Ľubor Fišera, PhD, DSc; Prof. Tibor Gracza, PhD, DSc; Prof. Štefan Marchalín, PhD, DSc; Associate Professors: Dušan Berkeš, PhD; Ľubomír Floch, PhD (until 30. 06. 2006); Viktor Milata, PhD; František Považanec, PhD; Štefan Stankovský, PhD; Katarína Špirková, PhD (until 30. 06. 2006); Ladislav Štibrányi, PhD; Assistant Professors : Mária Bobošíková, PhD; Anna Koreňová, PhD; Angelika Lásiková PhD; Peter Szolcsányi PhD; Peter Šafář, PhD; Research Fellows: Matej Babjak, PhD; Branislav Dugovič, PhD; Andrej Kolarovič, PhD (since 01. 03. 2006); Daniel Végh, PhD, DSc; Peter Zálupský, PhD; Jozefína Žúžiová, PhD; PhD Students: Anita Andicsová; Barbora Baumlová; Maroš Bella (since 01. 10. 2006); Eva Hýrošová; Mária Gardiánová; Rasha Jame (since 01. 10. 2006); Peter Koóš; Peter Kubizna; Andrej Pažitný (since 01. 10. 2006); Martin Petro; Zita Puterová; Juraj Rehák; Tomáš Solčán; Tomáš Wiesenganger; Dagmar Winklerová; Miroslava Žáková (since 01. 10. 2006); Technical staff: Eva Kaisová; Mária Krajčírová; Mária Nemcová; Anton Pavlíček; Jakub Rečičár; Iva Viskupičová; II. TEACHING AND RESEARCH LABORATORIES A. Teaching laboratories: Basic Skills in Organic Chemistry Laboratory I, II. Organic Synthesis Laboratory B. Research laboratories: Laboratory of Organic Synthesis Laboratory of Chiral Cycloaddition Reactions Laboratory of Heterocyclic Chemistry Laboratory of Stereoselective Synthesis Laboratory of Applied Organic Synthesis Laboratory of Natural Compounds Laboratory of Nuclear Magnetic Resonance Spectroscopy Laboratory of IR and UV Spectroscopy Laboratory of Gas Chromatography III. TEACHING A. Undergraduate Study: 2. semester (Bc) Chemical Information 1/2/0 Zálupský, Berkeš 2. semester (Bc) General and Organic Chemistry Laboratory 0/0/4 Stankovský, Kotočová 3. semester (Bc) Organic Chemistry 2/2/0 Gracza 3. semester (Bc) Organic and Bioorganic Chemistry 2/1/0 Marchalín, Štibrányi Organic Chemistry Laboratory 0/0/4 all teachers and research workers 4. semester (Bc) Organic Chemistry 2/2/0 Fišera, Považanec Organic Chemistry Laboratory 0/0/4 all teachers and research workers 3. semester (Bc) (Pt) Organic Chemistry 1/1/0 Fišera, Štibrányi 176
Organic Chemistry Laboratory 0/0/4 Lásiková, Wiesenganger 4. semester (Bc) (Pt) Organic Chemistry 1/1/0 Špirková Organic Chemistry Laboratory 0/0/4 Stankovský, Winklerová 5. semester (Bc) Chemical Information 1/1/0 Zálupský, 6. semester (Bc) Chemical Specialities 2/2/0 Mravec, Štibrányi Semestral Project 0/0/4 Berkeš, Fišera, Koreňová, Stankovský, Šafář 1. semester (MSc) Organometallic Compounds 1/1/0 Gracza Mechanisms of Organic Reactions I 3/1/0 Fišera Bioorganic Chemistry 2/0/0 Berkeš Laboratory Project I 0/0/10 Koreňová, Berkeš 1. semester (MSc) Organic Chemistry III 1/1/0 Považanec 2. semester (MSc) Organic Synthesis 2/1/0 Floch Asymmetric Synthesis 2/1/0 Gracza Stereochemistry 0/2/0 Štibrányi Spectroscopic Methods in the Control of Technology 2/2/0 Milata, Segľa 2. semester (MSc) Laboratory Project II 0/0/6 Šafař, Štibrányi Training at Industrial Fišera, Gracza, Lásiková, Marchalín, Milata, 15 d Production Floor Považanec, Szolcsányi 3. semester (MSc) Mechanisms of Organic Reactions II 1/1/0 Marchalín Applied Organic Synthesis 1/1/0 Považanec Physical Organic Chemistry I 0/2/0 Milata Chemistry of Heterocyclic Compounds 2/0/0 Stankovský Chemistry of Natural Substances and Drugs 2/0/0 Berkeš Chemical Information Systems 2/0/0 Zálupský 3. semester (MSc) Laboratory Project 0/0/10 Fišera, Gracza, Lásiková, Marchalín, Milata, Považanec, Szolcsányi 4. semester (MSc) Diploma Seminar Považanec Diploma Thesis Project Fišera, Milata, Štibrányi, Végh C. Doctoral Study: 1. semester (PhD) Advanced Organic Chemistry 2/0/0 Gracza 1. semester (PhD) Advanced Stereochemistry 2/0/0 Fišera 2. semester (PhD) Structure Reactivity Relationship 2/0/0 Marchalín 3. semester (PhD) Advanced Organic Chemistry 2/0/0 Milata 3. semester (PhD) Chemistry of Heterocyclic Compounds 2/0/0 Végh IV. CURRENT RESEARCH PROJECTS VEGA project No 1/3549/2006 Asymmetric and Stereoselective Reactions. Dipolar Cycloadditions, Sm(II)-Induced Additions, Cyclizations and Oxycarbonylations in the Total Syntheses of Natural Products and Its Analogues (Lubor Fišera) The Sm(II) induced diastereoselective reductive coupling of sugar derived nitrones with ethyl acrylate will provide access to a variety of functionalized amino acids directly, or to amino acids as constituents of small peptides. The stereoselective synthesis of optically active polysubstituted pyrrolidin-2-ones and piperidine-2-ones from chiral amino acids which are promising precursors for the synthesis of several pyrrolizidine, pyrrolidine, indolizidine and piperidine alkaloids. The synthesis of non-proteinogenic amino acids derived nitrones, isoxazolidinyl nucleosides, spironucleosides and azanucleosides. The study of the effect of Lewis acids to influence diastereoselectivity of nitrone cycloaddition reactions. Asymmetric palladium(II)-catalyzed oxy-/aminocarbonylation and oxa-/aminobicyclization of unsaturated polyols and aminopolyols. Catalyst design using the calculation of the model for transition state. Correlation of enantioselectivity with calculated models of the transition states for prediction of the reaction stereoselectivity and stereochemistry of the products. The application of these reactions as the asymmetric key-steps in the total syntheses of natural compounds. Project duration: from 01.01.2006 to 31.12.2008 177
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ANNUAL REPORT 2006 Faculty of Chemi
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FOREWORD The Faculty of Chemical an
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B. Research laboratories: Laborator
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signal transducers are investigated
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(Pavol Tarapčík). The project is
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Department of Organic Chemistry, Un
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Kirchner, M. 29th International Sym
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Čacho, F. On-line Preconcentration
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DNA, dsDNA damage and apoptosis in
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[19] Flickyngerová, Soňa, Ovádek
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techniques for ultratrace pesticide
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METHODS. In Absracts of the 29 th I
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Comenius University, Faculty of Pha
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INSTITUTE OF INORGANIC CHEMISTRY, T
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MVTS Project No NEM/Slov/DAAD/Darm0
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Institute of Applied Synthetic Chem
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Koman, M. Institute of Chemical Tec
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type ligands. International Journal
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IV. CURRENT RESEARCH PROJECTS VEGA
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B. International Cooperation Instit
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C. Dissertations (PhD) Name Title o
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III. TEACHING A. Undergraduate Stud
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B. International Cooperation Instit
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triazolo[1,5/a]pyrimidine-6carbonit
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INSTITUTE OF BIOCHEMISTRY, NUTRITIO
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APVT Project No 20-003904 Biochemic
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Andrea Šovčíková Martin Šimkov
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Ondrejkovičová I., Chapter: Chemi
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[29] Paulikova, H, Valkova, Z, Kadl
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IV. CURRENT RESEARCH PROJECTS A. VE
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Research Institute of Drugs, Modra
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Moravčíková P. Development of ph
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priestoroch. In Zborník z workshop
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Laboratory for microbial degradatio
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of soil will be also included in th
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D. Erasmus/Socrates - Graz Universi
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Veterinary Sciences Slugeň Dušan
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Molnárová, J. Palatáš, M. Sedl
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[12] Čertík, M., Ješko, D.: Geno
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DEPARTMENT OF CHEMICAL AND BIOCHEMI
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3.semester(MS) Laboratory M.Polakov
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stability of food enzymes, the inac
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Project duration: from 2006 to 2008
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VŠCHT Praha, ČR CIBA Spezialität
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Markoš Jozef Slovak Society of Che
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Jelemenský SACEC 2006, Durban, Uni
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[8] Katrlík, J., Mastihuba, V., Vo
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Conference Biocatalysis in the Food
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DEPARTMENT OF CHEMICAL PHYSICS Head
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The stability of polymers with sele
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D. Membership in International Orga
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Article in conference proceedings [
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DEPARTMENT OF CHEMICAL TECHNOLOGY O
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VI. COOPERATION A. Cooperation in S
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B. Graduate Theses (MS Degree) for
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3. semester (MSc) Risk Properties o
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Project duration: from 01.05.2006 t
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Institute of Chemical Technology, P
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Hutňan,M. Excursion on Biogas Stat
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[12] Derco, Ján, Dudáš, Jozef, J
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Optional 2. semester (MSc) Special
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Legéň Jaroslav Slovak Chemical So
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