LCTECH / GPC PRODUCT LINE• Can be integrated in<strong>to</strong> LIMS systems and conforms <strong>to</strong> requirementsfor non-consecutive sample identification <strong>to</strong> processinglists (consecutive non-manipulability sample-ID).• Cleansing of the system is performed after each sample. Theentire flow path is rinsed including the sample needle therebyavoiding carry-over between samples.FEATURE HIGHLIGHTS• Reproducible High Recovery Rates• No Carry-Over• Easy Processing Of Complex Matrices• Reliable - Durable – Quiet• Unattended Operation• Keypad Or PC Control• Designed For Fatty Matrices• Sealed Sample VialsGPC VARIOAUTOMATED GEL PERMEATION CHROMATOGRAPHY SYSTEMGel permeation chroma<strong>to</strong>graphy is a well known technologyfor the removal of fats, proteins, and other large biomoleculesfrom samples in order <strong>to</strong> prevent interference inthe analysis of chlorinated & organo-phosphorous pesticides,PCBs, polyaromatic hydrocarbons (PAH), and othersemi-volatile compounds.The GPC VARIO au<strong>to</strong>mates Gel Permeation Chroma<strong>to</strong>graphy(GPC) technology for the clean-up of complex animaltissues, food products, environmental and many other typesof samples. The high recoveries are easily analyzed by GC-ECD, GC-MS, LC-MS, etc.Ideally suited for high-throughput labora<strong>to</strong>ries requiringreliability and reproducibility, the GPC VARIO is optimizedfor unattended operation, low maintenance, and consistentrecoveries. Each component is engineered for robustnessand low maintenance, and the GPC VARIO provides theease of use necessary for increased throughput and worryfreeoperations.For 24 x 7 operation, the GPC VARIO is designed for limitedmaintenance and service. All ow paths are solvent resistant.Materials are glass, PTFE, stainless steel and PPS-E2.• Sample vials and receptacles for fractions can be sealed withsepta (not required) <strong>to</strong> prevent sample or solvent vapors fromescaping.POPULAR APPLICATIONS INCLUDE• Pesticides And Polychlorinated Biphenyls (PCB)– EN 1528, EPA 8082a• Pesticide Residues – EN 12393, DFG S19• Polycyclic Aromatic Hydrocarbon (PAH) – EPA 8310• Organochlorine Pesticide Residues – AOAC 984.21• Phthalates – EPA 8270c• Gel Permeation Clean-up – EPA 3640a• …And Many More, Including USGS And USDA MethodsSYSTEM COMPONENTS• LCTECH GPC COLUMNThe specially designed GPC column is DIN-compliant filled withS-X3 Bio-Beads, 200-400 mesh. The column construction isglass and PTFE, 1/8” PTFE inlet and outlet, rigid PTFE base andadjustable plunger, sturdy construction, and overpressure stable.• KEYPAD CONTROL WITH LCD DISPLAYA f<strong>our</strong> line display with keypad input enables the system <strong>to</strong> operatein a stand alone mode. The menu driven input is self-explana<strong>to</strong>ryand intuitive for system operation.• SAMPLE HANDLING SYSTEMA precise swivel robot arm, in combination with a spring mountedneedle loop and an inert 10 mL syringe, transfers the liquid withinthe system. There are f<strong>our</strong> solvent paths possible that allow forapplication flexibility and efficient system rinsing functions.• MULTIPLE INJECTION OPTIONSThe user can choose between sample loop overfill, or partial loopfill. Flexibility in sample handling allow for a variety of options,including multiple injections from the same vial with collection in asingle vial (ideal for fatty samples).
LCTECH / GPC PRODUCT LINE• SAMPLE LOOPThe supplied standard loop is made of PTFE and is set <strong>to</strong> 5.0 mL(preparative system) or 1 mL (analytical system). A measuringpro<strong>to</strong>col is supplied and other volumes are available on request.• SAMPLE RACKSRacks are available for flexible sample and GC vial combinations.Options include: 52 positions with 60 mL, 26 positions with 110mL, or 12 positions with 250 mL.• GPC PUMPThe system contains a robust PLC-controlled double pis<strong>to</strong>npreparative (analytical pump also available) pump adjustable from0.04 – 40.00 mL/min. Preparative pump technology has knownfor longevity and reliability in continuous operation environments.The pump flow rate is adjustable with pulsation less the 1.0 %.Over and low pressure shut-off is integrated, and with inert wettedcomponents, the reliability and low maintenance are superior <strong>to</strong>HPLC pump implementations.• SOFTWARE VARIOSOFT (OPTIONAL)The LCTech PC Windows VarioSoft can be integrated in<strong>to</strong> LIMSsystems and conforms <strong>to</strong> requirements for non-consecutivesample identification <strong>to</strong> processing lists (consecutive non-manipulabilitysample-ID). The graphical user interface is modeled aftermost HPLC and GC software for familiar and intuitive control ofthe operations. Sample ID and Job List Sequence are encryptedand s<strong>to</strong>red <strong>to</strong> meet all requirements for data security.• FIXED WAVELENGTH DETECTOR (OPTIONAL)The UV detec<strong>to</strong>r is a 254 nm fixed wavelength detec<strong>to</strong>r controlledby the VarioSoft GPC VARIO software <strong>to</strong> moni<strong>to</strong>r the quality ofthe GPC columns.TECHNICAL DATA OF THE GPC VARIO SAMPLE CLEAN-UP SYSTEMAmbient Temperature (Operational) 10 — 40 °CRelative Humidity (Operational) 0 — 95 %ELECTRONIC DATAPower Supply 230 V ± 10 % or 120 V ± 10 %Communication InterfaceRS 232 for Terminal and PC control. Modemfor remote serviceGPC PUMPTypeDual Pis<strong>to</strong>nFlow RatesAnalytical: 0.10 – 9.95 mL/min Preparative:0.40 – 40.00 mL/minPressure40 bar (instrument)MEASURES & WEIGHTMeasures (W X D X H)Weight (Operational)CATALOG NO.750 X 600 X 1000 mmCa. 110 kgGPC VARIO CATALOG INFORMATIONDESCRIPTIONGel Permeation Chroma<strong>to</strong>graphy (GPC) System - type VARIO,The basic unit comes with a preparative HPLC-pump (flow rate 0.4011006 <strong>to</strong> 40.0 mL/min); one sample loop 5 mL; 110 VAC, 50 Hz.Chroma<strong>to</strong>graphy column, Sample Rack, bottles for equipping the rackas well as waste bottles need <strong>to</strong> be ordered separately.Gel Permeation Chroma<strong>to</strong>graphy (GPC-system) - type VARIO-A,basic unit comes with an analytical HPLC-pump (flow rate 0.10 <strong>to</strong>11007 9.95 mL/min); one sample loop 1 mL; 110 VAC, 50 Hz.Chroma<strong>to</strong>graphy column, Sample Rack, bottles for equipping the rackas well as waste bottles need <strong>to</strong> be ordered separately.NOTE: Racks, columns and accessories will vary by application and labora<strong>to</strong>ry. Thisproduct sold only by quotation.79PRODUCT CATALOGPICKERING LABORATORIES10/11
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TABLE OF CONTENTSINTRODUCTION3 Cust
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INTRODUCTIONINSTALLATION & TRAINING
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“A LOT HAS CHANGED SINCE PRODUCIN
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INSTRUMENTS & HARDWAREFEATURE HIGHL
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INSTRUMENTS & HARDWARE• Indoor us
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INSTRUMENTS & HARDWARECRX400 POST-C
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CHROMATOGRAMS, COLUMNS & GUARDSPick
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GENERAL TERMS & CONDITIONS1 CONTROL
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