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NOTE 4.--Two BBR beams (requiring PAV material) are required at each test temperature. In addition,<br />
four DT samples may also be needed at each test temperature. A minimum of two test temperatures wilI be<br />
required.<br />
6.10 Complete steps 6.1 through 6.9 during the first day of testing. This will allow<br />
further testing to begin on the second day, when the PAV procedure is complete.<br />
6.11 At the conclusior_ of the PAV procedure, carefully remove the residue from the<br />
vessel and combine individual pans of the same aged asphalt binder. Prepare two bending<br />
beam specimens for each test temperature according to TP1. Retain sufficient residue to<br />
prepare four direct tension specimens for each test temperature if required.<br />
6.12 Perform the DSR test (TP5) on the PAV residue. Begin at a test temperature<br />
of 16°C for PG 52; 19°C for PG 58; 22°C for PG 64; and 28°C for PG 70, unless there is<br />
other information to suggest the temperature at which G'sin 8 is < 5000 kPa. Decrease or<br />
increase the test temperature at 3.0°C increments until the value for G'sin 8 exceeds<br />
5000 kPa.<br />
6.13 Determine the beginning test temperature for the BBR test (TP1) on the PAV<br />
residue from table 1 of MP1. Use the starting PG determined in section 6.3 and the lowest<br />
temperature from section 6.12 where the value for G'sin 8 did not exceed 5000 kPa, unless<br />
there is other information to suggest the temperature at which the stiffness is < 300.0 MPa,<br />
and the slope m is > 0.300.<br />
6.14 Test pairs of BBR specimens according to TP1. Begin at the test temperature<br />
selected in section 6.13 and increase at 6.0°C increments, until a stiffness and slope meeting<br />
the requirements of MP1 are obtained. Test fresh BBR specimens at each temperature.<br />
Determine the extent of physical hardening, report the creep stiffness (S) and the slope (m)<br />
of the log creep stiffness versus log time relationship measured at 1 and 24 hours. Prepare<br />
two sets each of two BBR specimens of original asphalt binder. Test one set after 1 hour of<br />
conditioning and the second set after 24 hours of conditioning. The latter is conducted at<br />
the lowest grading test temperature (Tmi_+ 10°C).<br />
6.15 Certain asphalt binders may satisfy the MP1 slope requirement at substantially<br />
lower temperatures than they satisfy the stiffness requirement. If the creep stiffness is<br />
between 300 and 600 MPa at a test temperature at which the slope (m) is > 0.300, it may<br />
be possible to satisfy the DT (TP3) failure strain requirement in lieu of the creep stiffness<br />
requirement. Test four DT specimens according to TP3 at the test temperature at which m ><br />
0.300, and determine if the failure strain is > 1.0%.<br />
6.16 If the failure strain is < 1.0%, test additional sets of four DT specimens.<br />
Increase the test temperature in 6.0°C increments until a failure strain > 1.0% is obtained.<br />
Determine the test temperature at which m > 0.300 and the creep stiffness is < 300.0 MPa,<br />
or, if the creep stiffness is between 300.0 and 600.0 MPa, the failure strain is > 1.0%.<br />
6.17 Using the results of steps 6.12 through 6.16, determine the final grade of the<br />
asphalt binder.<br />
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