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10.2 Anneal the asphalt binder for the test specimen by heating until it is sufficiently<br />
fluid to pour. Annealing prior to testing removes reversible molecular associations (steric<br />
hardening) that occur during normal storage at ambient temperature.<br />
NOTE6.--Minimum pouring temperatures that produce a consistency equivalent to that of SAE 10W30<br />
motor oil (readily pours but not overly fluid) at room temperature are recommended. The specific temperature will<br />
depend on the grade of binder and its prior aging history, if any. Temperatures less than 135°C are desirable.<br />
Temperatures above 135°C may be required, however, for some modified asphalt binders or heavily aged binders.<br />
10.3 Place the plastic end inserts into both ends of the mold. Place the molds and<br />
inserts into a 163°C oven for 30 minutes.<br />
10.4 After heating, place the mold on a 6- to 7-mm-thick aluminum plate. Do not<br />
preheat the aluminum plate. Pour hot asphalt binder into the mold by starting at one end of<br />
the mold and moving across the mold in a single pass. Pour the specimen in a continuous<br />
stream to avoid entraining air bubbles or gaps. Complete the pouring operation as quickly as<br />
possible to avoid any excessive drop in the temperature of the asphalt binder. Stop pouring<br />
when the asphalt is slightly above the top surface of the mold.<br />
10.5 After pouring the test specimen, allow the entire assembly to cool on the<br />
benchtop at ambient temperature for approximately one hour. Do not quench the specimen to<br />
achieve ambient temperature.<br />
10.6 As soon as the specimen has cooled to room temperature, trim off the excess<br />
asphalt binder with a straight cutting edge (e.g., a flat cheese cutter or spatula) so that the<br />
asphalt binder is flush with the top of the mold. Use care during the trimming operation so<br />
that the asphalt binder is not pulled away from the mold and that the bond between the<br />
plastic inserts and the asphalt binder is not damaged. Trim the specimen in a consistent<br />
manner. Pull the cutting edge along the long axis of the sample flush with the surface of the<br />
mold to remove the excess asphalt binder. After trimming, remove all debris or extraneous<br />
asphalt binder from the holes or slots in the plastic insert.<br />
NOTE7.--Caution:<br />
occurs, discard the sample.<br />
Excessive downward pressure during trimming will distort the sample mold. If this<br />
10.7 Immediately prior to demolding, place the mold containing the specimen in a<br />
freezer at -5 + 5 °C until the specimen is sufficiently stiff to demold without distorting the<br />
sample. Some softer grades may require lower temperatures. Time in the freezer should not<br />
exceed 15 minutes. After demolding, place the sample on the specimen storage plate (see<br />
section 6.4). Measurement of specimen dimensions after demolding is not necessary since<br />
dimensional tolerances are closely controlled in the molding process.<br />
11. PROCEDURE<br />
11.1 Set the environmental chamber at the desired testing temperature and wait until it<br />
stabilizes to within + 0.2°C-of the desired test temperature. When testing for compliance<br />
with MP1, use the test temperatures specified in table 1 of MP1.<br />
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