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7.4.4 Adjust the controls for the environmental chamber to the requisite test<br />
temperature and allow the chamber and the test assembly to stabilize at that temperature.<br />
7.4.5 Precondition the specimen for 100 cycles with a shear stress of 7 kPa. Each<br />
cycle is 0.7 second in duration, and consists of the application, of a 0.1 second haversine load<br />
followed by a 0.6 second rest period.<br />
7.4.6 At the conclusion of the preconditioning, perform the simple shear test by<br />
increasing the shear stress at a rate of 70 kPa/s to: 345 kPa at 40°C or T_ff(PD), 105 kPa at<br />
20°C or Teff(FC), or 35 kPa at 4°C. Maintain the stress at that level for 10 seconds and then<br />
reduce it to 0 kPa at a rate of 25 kPa/s. Continue the test for an additional 10 seconds at a<br />
stress level of 0 kPa.<br />
7.4.7 Record axial deformation, shear deformation, axial load, and shear load at a<br />
rate of about 10 data points per second.<br />
NOTE 13.--The test takes about 20 to 30 minutes to complete from the time the specimen is placed in the<br />
apparatus until it is removed.<br />
7.5 Frequency Sweep Test at Constant Height<br />
7.5.1 Prepare the test specimen in accordance with section 6.<br />
7.5.2 Mount two LVDTs on the test assembly in such a manner that axial (vertical)<br />
and shear (horizontal) deformations can be measured during the test with an accuracy and<br />
precision commensurate with the requirements in M-003 (note 5).<br />
NOTE 14.--This is a strain-controlled test. The maximum strain is limited to 1 x 10 -4 mm]mm. During the<br />
test, the height of the specimen is kept constant. To accomplish this, the vertical load actuator is controlled by<br />
feedback from the vertical (axial) LVDT. The feedback to the horizontal (shear) load actuator is from the LVDT<br />
measuring the horizontal (shear) deformation.<br />
7.5.3 Place the specimen inside the shear test device and clamp it securely in place.<br />
7.5.4 Adjust the controls for the environmental chamber to the requisite test<br />
temperature and allow the chamber and the test assembly to stabilize at that temperature.<br />
7.5.5 Precondition the specimen by applying a sinusoidal shear (horizontal) strain of<br />
approximately 1 x 10 -4 ram/ram at a frequency of 10 Hz for 100 cycles.<br />
7.5.6 At the conclusion of the preconditioning, perform the frequency sweep test in<br />
which 100 cycles of 1 x 10 -4 mm]mm sinusoidal shear (horizontal) strain is applied at the<br />
each of the following frequencies in descending order: 10, 5, 2, 1, 0.5, 0.2, 0.1, 0.05, and<br />
0.02 Hz. Repeat the test on each specimen at three different temperatures, typically 4, 20<br />
ar:d 40°C, starting at the lowest temperature.<br />
7.5.7 Record axial deformation, shear deformation, axial load, and shear load at a<br />
rate of about 50 data points per load cycle.<br />
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