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April, 192S F<strong>org</strong>ing- Stamping - Heat Treating 131<br />
1. Permanence — capability of resisting the<br />
action of the air or of furnace gases at working<br />
temperatures.<br />
2. Uniform scale — continuous and regular increase<br />
of e.m.f. for increase of temperature over the<br />
working range.<br />
3. Power — relatively high e.m.f.<br />
4. Economy — low cost for service rendered.<br />
5. Reproducibility—permitting numerous couples<br />
to be made all having the same characteristics.<br />
6. Constancy of calibration — minimum tendency<br />
to take on impurities which will change the<br />
temperature •—• e.m.f. relation of the couple.<br />
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FIG. 85—End of Thermocouple.<br />
BBS B B3SB3BeBaBaBBgB—<br />
FIG. 86—Base metal couple, bare.<br />
FIG. 87—Base metal couple, with sheath and head.<br />
In selecting a couple the first thing generally to<br />
be considered is the temperature range over which it<br />
will be required to work- The higher the temperature<br />
the more expensive the metals, as a rule.<br />
For temperatures up to about 900 degrees C, which<br />
cover ordinary heat treating practice, a couple consisting<br />
of a wire of iron and one of constantan (an<br />
alloy of copper and nickel), is extensively used. This<br />
combination has a high e.m.f., is reasonably permanent,<br />
and is moderate in cost.<br />
Another widely used couple is made from two patented<br />
heat resisting alloys known as "chromel" and<br />
"alumel". Chromel is an alloy of chromium and nickel;<br />
alumel an alloy of aluminum and nickel. They<br />
have the property of resisting oxidation at high temperatures.<br />
This couple has a somewhat lower e.m.f.<br />
than the iron-constantan pair, and its first cost is<br />
higher, but its life is longer at ordinary heat treating<br />
temperatures, and it may be used as high as 1100 deg.<br />
C, or for short periods, as high as 1300 deg. C. These<br />
two couples, and others made of common metals, are<br />
called "base metal" couples.<br />
For higher temperatures, up to about 1500 deg. C,<br />
which is the practical limit for the use of thermocouples,<br />
a combination consisting of one wire of pure<br />
platinum, and one of an alloy of 90 per cent platinum<br />
and 10 per cent rhodium, should be employed.<br />
This is known as the Le Chatelier, or "noble metal"<br />
couple. Its e.m.f. is only about one-fifth that of the<br />
iron-constantan couple, and its cost is quite high, but<br />
it is the only couple which will give satisfactory service<br />
above 1100 deg. C.<br />
Protection Tubes and Mounting.<br />
In order to prolong its life, protect it from mechanical<br />
damage and from attack or contamination by<br />
furnace gases or liquid heat treating baths in which it<br />
may be immersed, the portion of a couple which is ex<br />
posed to high temperatures is usually covered by a<br />
sheath or protection tube. The nature of this sheath<br />
is determined by the condition under which the couple<br />
must operate. For use with iron constantan couples<br />
a wrought iron or low carbon steel tube, securely<br />
plugged or welded at the end, makes a cheap and satisfactory<br />
sheath. For use with base metal couples at<br />
higher temperatures, tubes of special heat resisting alloys<br />
are preferable. Nichrome and chromel tubes are<br />
widely used and other good alloys are available. Various<br />
refractory protection tubes, such as porcelain, fire<br />
clay, graphite, etc., are useful in some cases, but these<br />
have the disadvantage of being easily broken, and as<br />
they are not such good conductors of heat as metals,<br />
they tend to make the couple sluggish in responding to<br />
fluctuations in the furnace temperature.<br />
Platinum is rapidly contaminated by vapors from<br />
other metals at high temperatures, and must be protected<br />
from metallic vapors coming from the charge or<br />
from metal parts of the furnace. Glazed porcelain or<br />
fused silica tubes are usually employed and these must<br />
be gas tight- These tubes are fragile and may be protected<br />
from mechanical damage by an outer protection<br />
tube of heat resisting alloys, carborundum, etc.<br />
The thermocouple itself is generally a separate unit<br />
from the wires or leads which connect it to the measuring<br />
instrument. Base metal couples are usually made<br />
of rather heavy wires (1/16 to y, in., but more frequently<br />
about y in.), of a suitable length to extend<br />
into the furnace to the desired point. They are welded<br />
together at the hot end, by means of an oxyacetylene<br />
welding flame or electric arc, sometimes being<br />
twisted together a few turns for greater strength. In-<br />
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FIG. 88 (left)—Rotary switch for connecting several couples<br />
to indicator.<br />
FIG. 89 (right)—Bus bar for connecting several couples to<br />
recorder.<br />
sulating beads are slipped over each wire to preve<br />
them from short circuiting along their length. This is<br />
illustrated in Fig. 85. These heavy wires terminate<br />
in a "head" outside the furnace where they are connected<br />
to lighter wires, sometimes flexible; which run<br />
to the indicating instrument, see Fig. 86. This head<br />
is usually mounted at the end of the protection tube,<br />
so that the whole is a convenient unit for handling or<br />
replacement, as shown in Fig. 87.<br />
Extension Leads.<br />
For base metal couples, it is customary to run wires<br />
of the same metals but of smaller size from the head<br />
of the couple to the indicating or recording instru-