Proceedings of the International Cyanide Detection Testing Workshop

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This publication should be cited as: Bruckner, A.W. and G. Roberts (editors). 2008. Proceedings of the International Cyanide Detection Testing Workshop. NOAA Technical Memorandum NMFS-OPR-40, Silver Spring, MD 164 pp. Signifi cant support for the development of this document was provided by NOAA Fisheries, Offi ce of Habitat Conservation, and NOAA’s Coral Reef Conservation Program. The views expressed in this document are those of the authors and the participants of the workshop, and do not necessarily refl ect the offi cial views or policies of the U.S. Government, NOAA or DOS. Front Cover Images: (Top) James Cervino – A fi sher uses cyanide to catch marine ornamental fi sh; (Bottom) Stephen Why – Pens used in Micronesia to hold live reef food fi sh. Additional copies of this publication may be requested from: John Foulks National Oceanic and Atmospheric Administration NOAA National Marine Fisheries Service Offi ce of Habitat Conservation 1315 East West Highway Silver Spring, MD 20910 John.Foulks@noaa.gov
Proceedings of the Cyanide Detection Testing Workshop Edited by Andrew W. Bruckner and Glynnis G. Roberts Offi ce of Habitat Conservation Ecosystem Assessment Division NOAA National Marine Fisheries Service 1315 East-West Highway Silver Spring, MD 20910-3282 NOAA Technical Memorandum NMFS-OPR-40 August 2008 U.S. Department of Commerce Carlos Gutierrez, Secretary National Oceanic and Atmospheric Administration Vice Admiral Conrad C. Lautenbacher, Jr., USN (Ret.) Under Secretary for Oceans and Atmosphere National Marine Fisheries Service Jim Balsiger, Assistant Administrator for Fisheries
Page 1: Proceedings of the International Cy
Page 5 and 6: ACKNOWLEDGEMENTS The Proceedings of
Page 7: PREFACE The International Cyanide D
Page 11 and 12: EXECUTIVE SUMMARY The International
Page 13 and 14: ATCA) in homogenized fi sh tissue m
Page 15 and 16: Validation of the ISE method applie
Page 17 and 18: Importing countries should also req
Page 19 and 20: INTRODUCTION Cyanide fi shing is a
Page 21 and 22: through the implementation of a net
Page 23 and 24: Working Group 2 The Export Working
Page 25 and 26: o o o o Can the U.S. require verifi
Page 27 and 28: Polymeric membrane based ion select
Page 29 and 30: Goal 2: Provide recommendations on
Page 31 and 32: hands-on training that develops a d
Page 33 and 34: Goal 3: Identify research needs to
Page 35 and 36: Working Group 1 Participants Bob KO
Page 37 and 38: estimated at roughly 3 to 5 days. H
Page 39 and 40: Goal 2 : Identify steps, agreements
Page 41 and 42: 3) certifi cate, but tests positive
Page 43 and 44: Report from Working Group 3 The Par
Page 45 and 46: No. of Shipments 6,000 5,000 4,000
Page 47 and 48: Goal 3: Provide a recommendation wi
Page 49: Working Group 3 Participants Eric P
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Introduction Since the early 1960
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ainbow trout exposed to 40 mg SCN -
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Blennies, which were net-caught and
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electrical potential (similar to an
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in the Philippines under contract w
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endorsing the IMA’s use of the IS
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The intended products from the rese
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WPCF 1992, 1998). Both of these stu
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ASTM (1997) Standard test methods f
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Kuegsen, M., Kloock, J.P., Knobbe,
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Philippines. In Proceedings from th
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3) 4) 5) 6) the metabolism of cyani
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or new matrices. 5.2.3 Modifi catio
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Level Two: The method should be val
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of cyanide exposure and to identify
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Special considerations for the anal
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tissue samples indispensable. Altho
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y reduction and subsequent separati
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can also be used for analysis of cy
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thiocyanate in saliva and serum bas
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are many discrepancies in the liter
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Table 3. Analytical Methods to dete
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Poisoning, In Textbook of military
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(70) Odoul, M., Fouillet, B., Nouri
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V. (1975) Stable reagents for the c
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(159) Felscher, D. and Wulfmeyer, M
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Purpose of this Document The purpos
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day. One cyanide tablet (2 g) is mi
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10-90% following exposure to cyanid
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existing cyanide detection methods
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- Plasma lactate — elevated plasm
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Method Advantages Disadvantages Hig
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Paper Method Matrix Detection Limit
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Table 4 lists experts identifi ed t
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X Jerry Thomas CDC Em Steve Borron
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References Barber, C. and Pratt, V.
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Rates of Recovery. Environmental Ma
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COUNTRY REPORTS
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The first three of these destructiv
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enforcement is minimal. There is an
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1. Management/guidance to the Minis
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in Vietnam now and requires more ef
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Figure 2: Administrative structure
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References Baquero, J. (1999) Marin
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Acronyms • CDT • Cyanide Detect
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Law/Ordinance/Decree /Decision 52/2
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of samples required for analysis. U
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Field test kit. BFAR recognizes the
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Political Will Having planted the s
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gravely by fi shing communities. Th
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ecome the partner and counterpart o
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Ion-Selective Electrodes for Cyanid
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References Alban, J., Manipula, B.E
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levels with mV readings recorded as
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Trends Determined by Cyanide Testin
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Implementing agencies: • Quaranti
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APPENDIX
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1:30 Overview of and Potential Cyan
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Kristine Johnson Director Kingfi sh
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Assessment of U.S. Role in Trade: U
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