Synthesis and Structural Characterization of ... - Jacobs University

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Amal H. Ismail Ph.D. Thesis 4.3. X-ray Crystallography ................................................................................................. 151 4.4. Results and Discussion ................................................................................................ 152 4.5. Conclusions ................................................................................................................. 161 4.6. References ................................................................................................................... 162 Chapter V Non-Lanthanide-Containing POMS ................................................................................... 165 5.A. Tellurium-Containing POMs ...................................................................................... 165 5.A.1. Tellurium-Containing Polyoxotungstates: The 20-Tungsto-4-Tellurate(IV) [H 2 Te 4 W 20 O 80 ] 22− and the 15-Tungstotellurate(IV) [NaTeW 15 O 54 ] 13− ......................... 165 5.A.1.1. Introduction ...................................................................................................... 165 5.A.1.2. Synthesis ........................................................................................................... 167 5.A.1.3. X-ray Crystallography ...................................................................................... 168 5.A.1.4. Results and Discussion ..................................................................................... 171 5.A.1.5. Conclusions ...................................................................................................... 180 5.A.1.6. References ........................................................................................................ 181 5.A.2. Tellurium-Containing Polyoxomolybdates: ........................................................ 184 The 44-Molybdo-24-Tellurate(IV), [H 2 Te 24 Mo 44 O 198 ] 34− .............................................. 184 5.A.2.1. Introduction ...................................................................................................... 184 5.A.2.2. Synthesis ........................................................................................................... 185 5.A.2.3. X-ray Crystallography ...................................................................................... 186 5.A.2.4. Results and Discussion ..................................................................................... 188 5.A.2.5. Conclusions ...................................................................................................... 194 5.A.2.6. References ........................................................................................................ 195 5.B. Transition Metal-Containing Heteropolytungstates: ................................................ 198 Copper-, Cobalt-, and Manganese-Containing 17-Tungsto-2-Germanates ................ 198 5.B.1. Introduction ......................................................................................................... 198 viii
Amal H. Ismail Ph.D. Thesis 5.B.2. Synthesis .............................................................................................................. 200 5.B.3. X-ray Crystallography ......................................................................................... 202 5.B.4. Results and Discussion ........................................................................................ 203 5.B.5. Conclusions ......................................................................................................... 211 5.B.6. References ........................................................................................................... 212 Appendix .......................................................................................................................... 216 ix
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