Synthesis and Structural Characterization of ... - Jacobs University

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Chapter 5 Unpublished Results [H 2 Te 24 Mo 44 O 198 ] 34− (1) comprises two {HTe 12 Mo 22 O 98 } {Te 12 Mo 22 } fragments which are connected via two -oxo bridges (Te−O−Te). Hence polyanion 1 can be described as a dimeric molecular entity composed of two {Te 12 Mo 22 } half units which lack any kind of symmetry element (see Figure 5.10 and 5.11). Figure 5.10. Polyhedral (upper) and ball-and-stick (lower) representations of [H 2 Te 24 Mo 44 O 198 ] 34− . The color code is as follows: MoO 6 octahedra (red); Te (blue), Mo (black); O (red). 189
Chapter 5 Unpublished Results Figure 5.11. Polyhedral representation of the asymmetric {HTe 12 Mo 22 O 98 } half-unit. The color code is as follows: MoO 6 octahedra (green, red, light blue); Te (blue); O (red), monoprotonated oxygen (orange). The MoO 6 octahedra were colored differently for clarity. 190
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