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Chapter 1 Introduction α-[XW 11 O 39 ] n− - 1 Monolacunary Species α-[XM 12 O 40 ] n− - 3 Trilacunary Species = - 1Triad A-α-[XW 9 O 34 ] n− B-α-[XW 9 O 34 ] n− Figure 1.6 Lacunary species derived from the α-Keggin structure. Red octahedra: MO 6 , green sphere: X heteroatom, red sphere: oxygen. 13
Chapter 1 Introduction Removal of two adjacent octahedra from α- and β-[XW 12 O 40 ] n− isomers has not been observed, but only for the γ isomer, the [XM 10 O 36 ] n− , see Figure 1.8. The plenary polyanions are stabilized under very acidic conditions (pH 0-2), monolacunary species are found at slightly acidic pH (4-6), and trilacunary ones are stable at pH (8-10). β 1 -[XW 11 O 39 ] n− β 2 -[XW 11 O 39 ] n− β 3 -[XW 11 O 39 ] n− - 1 β-[XW 12 O 40 ] n− A-β-[XW 9 O 34 ] n− - 3 B-β-[XW 9 O 34 ] n− Figure 1.7 Lacunary species derived from the β-Keggin structure. Red and yellow octahedra: MO 6 , green sphere: X heteroatom, red sphere: oxygen. 14
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