Synthesis and Structural Characterization of ... - Jacobs University
Synthesis and Structural Characterization of ... - Jacobs University
Synthesis and Structural Characterization of ... - Jacobs University
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Chapter 5<br />
Published Results<br />
Table 5.2. Te–O(W) Bond Lengths (Å) for Na-26.<br />
Te1 Å Te2 Å<br />
Te – O5TE 1.853(6) Te – O10E 1.853(6)<br />
Te – O12T 1.884(6) Te – O6TE 1.859(6)<br />
Te – O24T 1.986(6) Te – O789 2.061(6)<br />
Te – O6T 2.332(6) Te – O5A 2.199(6)<br />
Table 5.3. Selected Bond Angles (/°) for Na-26.<br />
Te1 /° Te2 /°<br />
O5TE– Te1– O12T 97.8(3) O10E–Te2–O6TE 99.6(3)<br />
O5TE– Te1–O24T 94.9(3) O10E–Te2–O789 92.2(3)<br />
O12T–Te1–O24T 90.6(3) O6TE–Te2–O789 88.1(3)<br />
O5TE–Te1– O6T 82.1(2) O10E–Te2–O5A 83.7(3)<br />
O12T–Te1–O6T 81.2(2) O6TE–Te2–O5A 83.8(3)<br />
O24T–Te1–O6T 170.8(2) O789–Te2–O5A 170.1(2)<br />
Table 5.4. Selected W–O Bond Lenghths (Å) for Na-26.<br />
W–O Å W–O Å<br />
W1–O1T<br />
W1– O14<br />
W1– O110<br />
W1– O123<br />
W1– O12<br />
W1– O12T<br />
1.716(7)<br />
1.787(6)<br />
1.867(7)<br />
1.974(6)<br />
2.111(6)<br />
2.382(6)<br />
W7–O7T<br />
W7–O710<br />
W7–O67<br />
W7–O79<br />
W7–O78<br />
W7–O789<br />
1.743(6)<br />
1.822(6)<br />
1.882(6)<br />
1.890(6)<br />
2.098(6)<br />
2.338(6)<br />
W2–O2T<br />
W2–O2A<br />
W2–O12<br />
W2–O23<br />
W2–O123<br />
W2–O12T<br />
1.738(7)<br />
1.780(7)<br />
1.883(6)<br />
1.952(6)<br />
2.092(6)<br />
2.385(6)<br />
W8–O8T<br />
W8–O8A<br />
W8–O68<br />
W8–O89<br />
W8–O78<br />
W8–O789<br />
1.752(7)<br />
1.759(7)<br />
1.895(6)<br />
1.967(6)<br />
2.215(6)<br />
2.217(6)<br />
170
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