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Chapter III CHN Analysis, FT IR ….. parameters of - histidine doped KDP crystals and also found less value of axial ratios for doped crystals than the pure KDP crystal. Kushwaha et al [40] have recently reported the powder XRD pattern of L- threonine doped KDP crystals and observed a systematic variation in the intensity of diffraction peaks with varying L-threonine concentration. They did not report any extra peak due to doping of L-threonine. Also, recently Parikh et al [18] have reported that the single phase nature of L-alanine doped KDP crystals. Altogether, L-arginine and L-histidine doped KDP crystals [41] and L-arginine doped KDP crystals [42] were reported. They reported the single phase nature and slight change in the unit cell parameters on doping. 3.5.2 Powder XRD of Pure and Amino Acids Doped KDP Crystals In the present study, the powdered samples were analyzed by employing Cu K radiation of X-ray. The data were analyzed by using computer software powder X. The standard unit cell parameters of KDP were given as reference and the unit cell parameters for each sample were calculated by the software with assignment of different planes to Bragg reflections. Figures (3.14 -3.16) represent the powder XRD patterns of pure and the different amount of various amino acids doped KDP crystals and unit cell parameters of different samples are listed in table (3.5). 151
Chapter III CHN Analysis, FT IR ….. Figure: 3.14 Powder x– ray diffraction pattern for L – histidine doped KDP crystals. Figure 3.15 Powder x– ray diffraction pattern for L – threonine doped KDP crystals. 152
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Saurashtra University Re - Accredit
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Statements Under O. Ph.D.7 of Saura
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ACKNOWLEDGEMENT The author expresse
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in-law, Mother- in -law and all oth
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of NLO materials in rapidly develop
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doped samples in comparison to the
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micro-hardness decreases. Also, as
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Papers Published in National and In
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Seminar on Recent Advances in Conde
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Chapter I Brief Introduction... Cha
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Chapter II Solution Growth…. Tabl
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Load (N) Chapter VIII Micro-hardnes
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