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Chapter VIII Micro-hardness studies…<br />

load is decreased [13]. The constant ‘a’ is also known as the standard<br />

hardness.<br />

log P = log a + n log d (8.9)<br />

The values of constants a and n are obtained from the plot of log P Vs<br />

log d. Since the relation between log P and log d is linear, the slope of this line<br />

gives the value of constant n and the intercept on log P axis gives the value of<br />

log a and hence the value of a.<br />

In order to analyze the ISE in the hardness testing, one needs to fit the<br />

experimental data according to Kick's law. The behavior of the change in<br />

micro-hardness with the applied load can also be studied by obtaining the<br />

value of n. The variation of micro-hardness with load and its nature of the<br />

value of n are widely studied for various materials. From the observations of<br />

the variations of P with d Haneman and Schultz [67] have reported that in the<br />

low load region, n generally has a value less that 2. Onitsch [68] also found<br />

such low values of n by observing variation of micro-hardness with load, while<br />

Grodzinski [69] had found variation of n values from 1.3 to 4.9 of various<br />

materials. Knoop [70] observed an increase in hardness with decrease in load<br />

where as, Campbell et al [71] and Mott et al [72] observed a decrease in<br />

hardness with decrease in load. On the other hand, Taylor [73] and Toman et<br />

al [74] have reported no significant change in the micro-hardness value with<br />

variation of load. Such contradictory results [75] may be due to the effect of<br />

the surface layers and vibrations produced during the test. Gane et al [31]<br />

studied the micro-hardness at very small loads. They observed a sharp<br />

increase in micro-hardness at small indentation size suggested that this<br />

increase might be due to the high stresses required for homogeneous<br />

nucleation in small dislocation free regions indented. On the contrary, Ivan'ko<br />

302

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