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Chapter VIII Micro-hardness studies…<br />

Where, E is the Young’s modulus and H is the hardness.<br />

However, there are several reports on cracking around indentations in<br />

several materials. PETN and RDX are important plastic explosive materials.<br />

The fracture mechanism of indentation cracks was studied by Hagan and<br />

Choudhari [99] by using the formulation suggested by Lawn and Fuller [97] as<br />

follows:<br />

P C 3/2 = ((2 E/(1-v 2 )) 1/2<br />

316<br />

(8.16)<br />

Where, P is the load of indenter, C is the length of crack, E is the Young’s<br />

modulus, ν is the Poisson’s ratio and is the coefficient of function between the<br />

indenter and indented material, which is generally obtained by rubbing against<br />

standard hard surface. The fracture toughness of ferrites has been studied by<br />

Johnson et al. [100]. They used Vickers indenter and applied the formula<br />

proposed by Evans and Charles [98]. Moreover, they hypothesized that the<br />

large cations, Ca +2 and Fe +2 on the grain boundaries cause locally-distorted<br />

structure which is an easy fracture path. Ferrites exhibit high strength and<br />

fracture toughness but also experience grain boundary fracture in contrast to<br />

trans-granular fracture in weaker counterparts. Altogether, fracture toughness<br />

of doped bismuth oxide electrolytes have been reported by Sammes [101].<br />

Burnett and Page [102] have studied crack propagation and patterns around<br />

Vickers indentation mark on sapphire and glass with and without ion<br />

implantations. They also determined the fracture toughness Kc by using the<br />

relation proposed by Lawn and Co-workers [103-104] as follows:<br />

Kc = 0.0139 (E/H) 1/2 P/C 3/2 (8.17)<br />

Where, H is the hardness, E is the modulus of the elasticity, P is the load and C<br />

is the crack length.

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