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Chapter IV Thermal Studies of ….. Conclusion 1. Thermo-grams of pure and amino acids doped KDP crystals suggested that as the doping increased the crystals became thermally less stable and dehydrated faster at comparatively lower temperature. 2. The values of kinetic and thermodynamic parameters decreased with The increase in the level of doping. 3. The higher values of activation energy and standard entropy of activation suggested more stable condition for pure KDP crystal than amino acids doped KDP crystals. 4. The positive value of # H o and # S o suggested spontaneous nature of reaction or phase transition at higher temperature. 5. By doping amino acids in KDP crystals, one faces slight sacrifice in the thermal stability of crystals. 181
Chapter IV Thermal Studies of ….. References 1. D. A. Skoog, F. J. Holler, T. A. Nieman, “Principles of Instrumental Analysis”, Saundrs College Publishing, Philadelphia (1998). 2. W. W. Wendlandt, “Thermal Analysis”, Wiley, New York (1985). 3. M. E. Brown, “Introduction to Thermal Analysis: Techniques and Applications”, Chapman and Hall, New York(1988). 4. P. J. Haines, “Thermal Methods of Analysis”, Blackie, London(1995). 5. L. Erdey, “Gravimetric Analysis”, Pergamon Press Ltd. (1963). 6. S. M. Khopkar, “Basic Concept of Analytical Chemistry”, Wiley Eastern, New Delhi (1984). 7. A. Abdel-Kader, A.A. Ammar, S.I. Salch, Thermochim. Acta 176 (1991) 293. 8. E.Ortiz, A. Vargas, B.E. Mellander, J.Phys. Chem of solids 59 (1998) 305. 9. K. S. Lee. J .Phy. Chem. Solids 57 (1996) 333. 10. J. H. Park, K. S. Lee, B. C. Choi, J. Phys. Condensed Mat. 13 (2001) 9411. 11. E. Torijano, R.A. Vargas, J.E. Diosa, B.E. Mellander, Phys. Status Solidi (b) 220 (2000) 659. 12. S. Balamuragan, P. Ramasamy, Spectrochem. Acta. A.Mol Biomal. Spectr. 71 (2009) 1979. 13. S. Chandra, A. Kumar, J. Phys. Condensed Mat. 3 (1991) 5271. 14. M. D. Shirsat, S. S.Hussaini, N. R. Dhumane, V.G. Dongre, Cryst. Res. & Technol. 43 (2008) 756. 182
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Saurashtra University Re - Accredit
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Statements Under O. Ph.D.7 of Saura
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ACKNOWLEDGEMENT The author expresse
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in-law, Mother- in -law and all oth
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of NLO materials in rapidly develop
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doped samples in comparison to the
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micro-hardness decreases. Also, as
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Papers Published in National and In
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Seminar on Recent Advances in Conde
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Chapter I Brief Introduction... Cha
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Chapter II Solution Growth…. Tabl
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Chapter II Solution Growth…. Δ C
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Load (N) Chapter VIII Micro-hardnes
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Chapter IX General Conclusion estab
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Chapter IX General Conclusion case
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