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INSTRUMENTAL LABORATORIES AND TECHNOLOGICAL PILOT PLANTS<br />

223<br />

Technical data: dimensions – 300x300 mm; high voltage and current connectors, diagnostic windows.<br />

Application: Studies on plasma discharge influence on physicochemical surface properties of polymer<br />

films, particularly TEM (track-etched membranes).<br />

2. Laboratory of Diffractional Structural Research<br />

Activity profile: X-ray diffraction structural studies on metal-organic compounds originating as degradation<br />

products of substances naturally occurring in the environment. Röntgenostructural phase<br />

analysis of materials. Studies on interactions in a penetrant-polymer membrane system using small<br />

angle scattering of X-rays, synchrotron and neutron radiation. Studies of structural changes occurring<br />

in natural and synthetic polymers under influence of ionising radiation applying X-ray diffraction<br />

and differential scanning calorimetry.<br />

• KM-4 X-ray diffractometer<br />

KUMA DIFFRACTION (Poland)<br />

Application: 4-cycle diffractometer for monocrystal studies.<br />

• CRYOJET - Liquid Nitrogen Cooling System<br />

Oxford Instruments<br />

Application: Liquid nitrogen cooling system for KM-4 single crystal diffractometer.<br />

• HZG4 X-ray diffractometer<br />

Freiberger Präzisionsmechanik (Germany)<br />

Application: Powder diffractometers for studies of polycrystalline, semicrystalline and amorphous<br />

materials.<br />

• URD 6 X-ray diffractometer<br />

Freiberger Präzisionsmechanik (Germany)<br />

Application: Powder diffractometers for studies of polycrystalline, semicrystalline and amorphous<br />

materials.<br />

3. Sol-Gel Laboratory of Modern Materials<br />

Activity profile: The research and production of advanced ceramic materials in the shape of powders,<br />

monoliths, fibres and coatings by classic sol-gel methods with modifications – IChTJ Process or by<br />

CSGP (Complex Sol-Gel Method) are conducted. Materials obtained by this method are the following<br />

powders: alumina and its homogeneous mixtures with Cr 2 O 3 , TiO 3 , Fe 2 O 3 , MgO+Y 2 O 3 , MoO 3 ,<br />

Fe, Mo, Ni and CaO, CeO 2<br />

, Y 2<br />

O 3<br />

stabilized zirconia, β and β’’ aluminas, ferrites, SrZrO 3<br />

, ceramic<br />

superconductors, type YBCO (phases 123, 124), BSCCO (phases 2212, 2223), NdBa 2 Cu 3 O x , their<br />

nanocomposites, Li-Ni-Co-O spinels as cathodic materials for Li rechargeable batteries and fuel<br />

cells MCFC, BaTiO 3 , LiPO 4 , Li titanates: spherical for fusion technology, irregularly shaped as<br />

superconductors and cathodic materials, Pt/WO 3<br />

catalyst. Many of the mentioned above systems, as<br />

well as sensors, type SnO 2 , were prepared as coatings on metallic substrates. Bioceramic materials<br />

based on calcium phosphates (e.g. hydroxyapatite) were synthesized in the form of powders, monoliths<br />

and fibres.<br />

• DTA and TGA thermal analyser<br />

OD-102 Paulik-Paulik-Erdey, MOM (Hungary)<br />

Technical data: balance fundamental sensitivity – 20-0.2 mg/100 scale divisions, weight range – 0-9.990 g,<br />

galvanometer sensitivity – 1x10 –10 A/mm/m, maximum temperature – 1050 o C.<br />

Application: Thermogravimetric studies of materials up to 1050 o C.<br />

• DTA and TGA thermal analyser 1500<br />

MOM (Hungary)<br />

Technical data: temperature range – 20-1500 o C; power requirements – 220 V, 50 Hz.<br />

Application: Thermal analysis of solids in the temperature range 20-1500 o C.<br />

• Research general-purpose microscope<br />

Carl Zeiss Jena (Germany)<br />

Technical data: General purpose microscope, magnification from 25 to 2500 times, illumination of<br />

sample from top or bottom side.<br />

• Metallographic microscope<br />

EPITYP-2, Carl-Zeiss Jena (Germany)<br />

Technical data: magnification from 40 to 1250 times.<br />

Application: Metallographic microscope for studies in polarized light illumination and hardness<br />

measurements.<br />

• Laboratory furnace<br />

CSF 12/13, CARBOLITE (Great Britain)<br />

Application: Temperature treatment of samples in controlled atmosphere up to 1500 o C with automatic<br />

adjustment of final temperature, heating and cooling rate.

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