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224 INSTRUMENTAL LABORATORIES AND TECHNOLOGICAL PILOT PLANTS II. DEPARTMENT OF RADIOISOTOPE INSTRUMENTS AND METHODS Laboratory of Industrial Radiometry Activity profile: Research and development of non-destructive methods and measuring instruments utilizing physical phenomena connected with the interaction of radiation with matter: development of new methods and industrial instruments for measurement of physical quantities and analysis of chemical composition; development of measuring instruments for environmental protection (dust monitors, radon meters); implementation of new methods of calibration and signal processing (multivariate models, artificial neural networks); designing, construction and manufacturing of measuring instruments and systems; testing of industrial and laboratory instruments. • Multichannel analyser board with software for X and γ-ray spectrometry Canberra • Function generator FG-513, American Reliace INC III. DEPARTMENT OF RADIOCHEMISTRY 1. Laboratory of Coordination and Radiopharmaceutical Chemistry Activity profile: Preparation of novel complexes, potential radiopharmaceuticals, e.g. derivatives of tricarbonyltechnetium(I) ( 99m Tc) with chelating ligands mono- and bifunctional. Studying of their hydrophilic-lipophilic properties, structure and their interactions with peptides. Also rhenium(VI) complexes with dendrimeric ligands are synthesised and studied. Novel platinum and palladium complexes with organic ligands, analogs of cisplatin, are synthesised and studied as potential antitumor agents. Solvent extraction separation of trivalent actinides from lanthanides is studied, directed towards nuclear waste treatment. Studies in the field of isotope chemistry of middle and heavy elements in order to find correlations between isotope separation factor and the structure of species which exchange isotopes in chemical systems, as well as to select the methods suitable for isotope enrichment. (For the research equipment, common for both Laboratories, see below.) 2. Laboratory of Heavy Elements Activity profile: Synthesis and studies of the structure of heavy p-block elements in the solid state and in solution. Elaboration of new methods for binding of 211 At, 47 Sc and 103m/105 Rh to biomolecules. Elaboration of new medically important radionuclide generators, e.g. 82 Sr/ 82 Rh, 103 Ru/ 103m Rh, 44 Ti/ 44 Sc. • Spectrometric set ORTEC Multichannel analyser, type 7150, semiconductor detector Application: Measurements and identification of γ- and α-radioactive nuclides. • Spectrometric set TUKAN, IPJ (Świerk, Poland) Multichannel analyser, type SILENA with a PC card type TUKAN Application: Measurements and identification of γ-radioactive nuclides. • Gas chromatograph 610, UNICAM (England) Application: Analysis of the composition of mixtures of organic substances in the gas and liquid state. • High Performance Liquid Chromatography system Gradient HPLC pump L-7100, Merck (Germany) with γ-radiation detector, INCT (Poland) Application: Analytical and preparative separations of radionuclides and/or various chemical forms of radionuclides. • Capillary electrophoresis system PrinCE Technologies with a UV-VIS detector (Bischoff Lambda 1010) and a radiometric detector Activity Gauge type Tc-99m (INCT, Poland) Application: Analytical separation of various radiochemical and chemical species, in particular charged. • UV-VIS spectrophotometer DU 68, Beckman (Austria), modernized and computerized Application: Recording of electronic spectra of metal complexes and organic compounds in solution. Analytical determination of the concentration of these compounds. • FT-IR spectrophotometer EQUINOX 55, Bruker (Germany) Application: Measurements of IR spectra of metal complexes and other species in the solid state and in solution.
INSTRUMENTAL LABORATORIES AND TECHNOLOGICAL PILOT PLANTS 225 IV. DEPARTMENT OF NUCLEAR METHODS OF PROCESS ENGINEERING 1. Laboratory for Flue Gases Analysis Activity profile: Experimental research connected with elaboration of removal technology for SO 2 and NO x and other hazardous pollutants from flue gases. • Ultrasonic generator of aerosols TYTAN XLG • Gas chromatograph Perkin-Elmer (USA) • Gas analyser LAND Application: Determination of SO 2 , NO x , O 2 , hydrocarbons, and CO 2 concentrations. • Impactor MARK III Andersen (USA) Application: Measurement of aerosol particle diameter and particle diameter distribution. 2. Laboratory of Stable Isotope Ratio Mass Spectrometry Activity profile: Study of isotope ratios of stable isotopes in hydrogeological, environmental, medical and food samples. • Mass spectrometer DELTA plus Finnigan MAT (Bremen, Germany) Technical data: DELTA plus can perform gas isotope ratio measurements of H/D, 13 C/ 12 C, 15 N/ 14 N, 18 O/ 16 O, 34 S/ 32 S. Application: For measurements of hydrogen (H/D) and oxygen ( 18 O/ 16 O) in water samples with two automatic systems: H/Device and GasBench II. The system is fully computerized and controlled by the software ISODAT operating in multiscan mode (realtime). The H/Device is a preparation system for hydrogen from water and volatile organic compounds determination. Precision of hydrogen isotope ratio determination is about 0.5‰ for water. The GasBench II is a unit for on-line oxygen isotope ratio measurements in water samples by “continuous flow” techniques. With GasBench II, water samples (0.5 ml) can be routinely analyzed with a precision and accuracy of 0.05‰. The total volume of water sample for oxygen and hydrogen determination is about 2 ml. • Elemental Analyzer Flash 1112 NCS Thermo Finnigan (Italy) Application: For measurement of carbon, nitrogen and sulfur contents and their isotope composition in organic matter (foodstuff and environmental samples). • Gas chromatograph mass spectrometer GC MS-QP 5050A, GC-17A, Shimadzu (Japan) Technical data: capillary column – SPB 5, HP-5MS, SUPELCOWAX-10. 3. Radiotracers Laboratory Activity profile: Radiotracer research in the field of: environmental protection, hydrology, underground water flow, sewage transport and dispersion in rivers and sea, dynamic characteristics of industrial installations and waste water treatment stations. • Heavy lead chamber (10 cm Pb wall thickness) for up to 3.7x10 10 Bq (1 Ci) radiotracer activity preparations in liquid or solid forms • Field radiometers for radioactivity measurements • Apparatus for liquid sampling • Turner fluorimeters for dye tracer concentration measurements • Automatic devices for liquid tracers injection • Liquid-scintillation counter Model 1414-003 ”Guardian”, Wallac-Oy (Finland) Application: Extra low-level measurements of α and β radionuclide concentrations, especially for H-3, Ra-226, Rn-222 in environmental materials, e.g. underground waters, surface natural waters; in other liquid samples as waste waters, biological materials, mine waters, etc. 4. Membrane Laboratory Activity profile: Research in the field of application of membranes for radioactive waste processing and separation of isotopes. • Membrane distillation plant for concentration of solutions Technical data: output ~0.05 m 3 /h, equipped with spiral-wound PTFE module G-4.0-6-7 (SEP GmbH) with heat recovery in two heat-exchangers.
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ANNUAL REPORT 2005 50 years in the
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CONTENTS GENERAL INFORMATION 9 MANA
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DETERMINATION OF CADMIUM, LEAD, COP
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NUCLEONIC CONTROL SYSTEMS AND ACCEL
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GENERAL INFORMATION 9 GENERAL INFOR
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MANAGEMENT OF THE INSTITUTE 11 MANA
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MANAGEMENT OF THE INSTITUTE 13 •
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SCIENTIFIC STAFF 15 5. Danilczuk Ma
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RADIATION CHEMISTRY AND PHYSICS, RA
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20 RADIATION CHEMISTRY AND PHYSICS,
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RADIOBIOLOGY
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100 RADIOBIOLOGY THE ROLE OF LYSOSO
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102 many found the ratio to be high
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104 RADIOBIOLOGY DNA INTER-STRAND C
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108 The possible reason of this eff
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NUCLEAR TECHNOLOGIES AND METHODS 11
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THE INCT PUBLICATIONS IN 2005 143 T
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THE INCT PUBLICATIONS IN 2005 145 2
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NUKLEONIKA 169 NUKLEONIKA THE INTER
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NUKLEONIKA 171 7. Influence of time
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