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96 RADIOCHEMISTRY, STABLE ISOTOPES, NUCLEAR ANALYTICAL METHODS, GENERAL CHEMISTRY the packing diagram, Fig.3 – the coordination around the barium(II) ion. A network of hydrogen bonds is responsible for the stability of the crystal. X-ray diffraction data collection was carried out on a KUMA KM4 four circle diffractometer at the Institute of Nuclear Chemistry and Technology. Structure solution and refinement was performed using SHELXL programme package. Fig.3. The coordination around the barium(II) ion in the structure of Ba[H(4,5-IDA)] 2 (H 2 O) 4·2H 2 O. CRYSTAL CHEMISTRY OF COORDINATION COMPOUNDS WITH HETEROCYCLIC CARBOXYLATE LIGANDS. PART LIX. THE CRYSTAL STRUCTURE OF A CALCIUM(II) COMPLEX WITH PYRIDAZINE-3-CARBOXYLATE AND WATER LIGANDS Wojciech Starosta, Janusz Leciejewicz The crystals of bis[(µ 2 -pyridazine-3-carboxylato- -N,O, O’)-trisaqua-calcium(II)] are monoclinic, Fig. The centrosymmetrical dimeric molecule of Ca 2 (C 5 H 3 N 2 O 2 ) 4 (H 2 O) 6 with atom labelling scheme. Unlabelled atoms are related by the symmetry code: -x+1, -y+2, -z+1. Displacement ellipsoids are drawn at the 50% probability level. space group P2 1 /n with a=9.173(1) Å, b=10.539(2) Å, c=14.984(3) Å, β=99.43(3) o and Z=4. The structure contains centrosymmetric dimeric molecules composed of two calcium(II) ions, each coordinated by two pyridazine-3-carboxylate ligand molecules (Ca 2 (C 5 H 3 N 2 O 2 ) 4 (H 2 O) 6 ) via their N,O bonding moieties [Ca-O11 2.432(1) Å, Ca-N11 2.585(1) Å; Ca-O21 2.404(1) Å, Ca-N21 2.606(1) Å] and three water molecules [mean Ca-O 2.389(1) Å]. The calcium ions are bridged by two carboxylate oxygen atoms, each acting in a bidentate mode donated by ligand molecules coordinated to different metal ions forming a bridging path Ca-O11-Ca I (Fig.). The coordination number of the calcium(II) ion is eight, the coordination polyhedron is a strongly deformed decahedron. Coordinated water molecules participate in a hydrogen bond network linking the dimers. X-ray diffraction data collection was carried out on a KUMA KM4 four circle diffractometer at the Institute of Nuclear Chemistry and Technology. Structure solution and refinement was performed using SHELXL programme package
RADIOBIOLOGY
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ANNUAL REPORT 2005 50 years in the
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CONTENTS GENERAL INFORMATION 9 MANA
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DETERMINATION OF CADMIUM, LEAD, COP
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NUCLEONIC CONTROL SYSTEMS AND ACCEL
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GENERAL INFORMATION 9 GENERAL INFOR
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MANAGEMENT OF THE INSTITUTE 11 MANA
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MANAGEMENT OF THE INSTITUTE 13 •
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SCIENTIFIC STAFF 15 5. Danilczuk Ma
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RADIATION CHEMISTRY AND PHYSICS, RA
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20 RADIATION CHEMISTRY AND PHYSICS,
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THE INCT PUBLICATIONS IN 2005 163 V
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NUKLEONIKA 169 NUKLEONIKA THE INTER
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NUKLEONIKA 171 7. Influence of time
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INTERVIEWS IN 2005 173 INTERVIEWS I
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CONFERENCES ORGANIZED AND CO-ORGANI
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EDUCATION 209 EDUCATION Ph.D. PROGR
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RESEARCH PROJECTS AND CONTRACTS 211
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RESEARCH PROJECTS AND CONTRACTS IAE
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LIST OF VISITORS TO THE INCT IN 200
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LECTURES AND SEMINARS DELIVERED OUT
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LECTURES AND SEMINARS DELIVERED OUT
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AWARDS IN 2005 221 AWARDS IN 2005 1
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INSTRUMENTAL LABORATORIES AND TECHN
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INDEX OF THE AUTHORS 235 Lisowska H
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