LTQ Orbitrap XL Hardware Manual

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Contents Chapter 3 User Maintenance.................................................................... 3-1 General Remarks............................................................... 3-2 Returning Parts .............................................................. 3-3 Cleaning the Surface of the Instrument.......................... 3-3 Baking Out the System ..................................................... 3-4 Bakeout Procedure ......................................................... 3-4 Maintaining the Vacuum System ...................................... 3-6 Exchanging the Lubricant Reservoir of the Turbopumps 3-6 Maintenance of the Recirculating Chiller .......................... 3-7 Reservoir ........................................................................ 3-7 Fluid Bag Filter .............................................................. 3-7 Condenser Filter ............................................................ 3-7 Chapter 4 Replaceable Parts.................................................................... 4-1 Parts Basic System............................................................. 4-2 Parts Orbitrap Analyzer.................................................. 4-3 Parts Pumping System Orbitrap..................................... 4-3 Parts Gas and Water Supply........................................... 4-5 Electronic Parts ................................................................. 4-7 Electronics - Right Panel................................................ 4-7 Electronics - Left Panel .................................................. 4-8 Electronics Analyzer ....................................................... 4-8 Electronics Main Supply ................................................ 4-9 Glossary .................................................................................... G-1 Index ............................................................................................I-1 xii LTQ Orbitrap XL Hardware Manual Thermo Fisher Scientific
Figures LTQ Orbitrap XL front view ................................................................ 1-2 Schematic view of the LTQ Orbitrap XL .............................................. 1-3 Top lid opened ...................................................................................... 1-4 System status LEDs ............................................................................... 1-6 Right side of the LTQ Orbitrap XL ...................................................... 1-7 Upper control panel .............................................................................. 1-8 Power control panel with power control LEDs and switches ................. 1-9 Main power switch .............................................................................. 1-10 External connections to the LTQ Orbitrap XL ................................... 1-11 Schematic view of the Orbitrap cell and example of a stable ion trajectory ............................................................................................. 1-13 Layout of the instrument, also showing the applied voltages ................ 1-14 Principle of electrodynamic squeezing of ions in the Orbitrap as the field strength is increased ............................................................................ 1-15 Approximate shape of ion packets of different m/q after stabilization of voltages ............................................................................................... 1-16 HCD collision cell and C-Trap ........................................................... 1-18 Schematical view of vacuum system (CLT compartment not shown) .. 1-19 Vacuum components on the left instrument side ................................ 1-20 Vacuum components on the right instrument side .............................. 1-20 Forepumps cabinet .............................................................................. 1-21 Schematical view of the gas supply ...................................................... 1-25 Valve for HCD collision gas ................................................................ 1-26 Nitrogen pressure regulator and gas flow divider ................................. 1-27 Schematical view of cooling water circuit ............................................ 1-28 Electronic connections to linear trap (covers removed) ........................ 1-31 Electronic boards on the right side of the instrument .......................... 1-32 Preamplifier board ............................................................................... 1-33 Data Acquisition unit (covers removed) .............................................. 1-34 Data Acquisition Digital PCI board .................................................... 1-35 Data Acquisition Analog board ........................................................... 1-36 Instrument Control board ................................................................... 1-38 Power Distribution board ................................................................... 1-39 Power Supply 1 board ......................................................................... 1-44 Electronic boards on the left side of the instrument ............................. 1-45 Ion Optic Supply board ...................................................................... 1-46 Central Electrode Pulser board ............................................................ 1-47 Temperature Controller board ............................................................ 1-49 CLT RF unit (cover removed) ............................................................. 1-51 Central Electrode Power Supply board ................................................ 1-52 High Voltage Power Supply board (cover removed) ............................ 1-54 High Voltage Power Supply board with SPI Bus Termination board .. 1-55 Main power switch in Off position ....................................................... 2-2 Thermo Fisher Scientific LTQ Orbitrap XL Hardware Manual xiii
Page 1 and 2: For Research Use Only Not for use i
Page 3: Place Declaration of Conformity her
Page 6 and 7: Conformité DEEE Ce produit doit ê
Page 8 and 9: Read This First Related Documentati
Page 10 and 11: Read This First Typographical Conve
Page 12 and 13: Read This First Safety and EMC Info
Page 14 and 15: Read This First Safety and EMC Info
Page 17: Contents Chapter 1 Functional Descr
Page 21: Tables System status LEDs of the Pr
Page 24 and 25: Functional Description General Desc
Page 26 and 27: Functional Description General Desc
Page 28 and 29: Functional Description Control Elem
Page 34 and 35: Functional Description Linear Ion T
Page 36 and 37: Functional Description Orbitrap Ana
Page 42 and 43: Functional Description Vacuum Syste
Page 48 and 49: Functional Description Gas Supply I
Page 50 and 51: Functional Description Cooling Wate
Page 52 and 53: Functional Description Printed Circ
Page 68 and 69:
Functional Description Printed Circ
Page 70 and 71:
Page 72 and 73:
Page 74 and 75:
Page 76 and 77:
Page 79 and 80:
Chapter 2 Basic System Operations M
Page 81 and 82:
Basic System Operations Shutting Do
Page 83 and 84:
Shutting Down the System Basic Syst
Page 85 and 86:
Starting Up the System after a Shut
Page 87 and 88:
Basic System Operations Starting Up
Page 89:
Basic System Operations Resetting t
Page 92 and 93:
User Maintenance General Remarks Ge
Page 94 and 95:
User Maintenance Baking Out the Sys
Page 96 and 97:
User Maintenance Maintaining the Va
Page 99 and 100:
Chapter 4 Replaceable Parts This ch
Page 101 and 102:
Parts Orbitrap Analyzer Parts Pumpi
Page 103 and 104:
Parts Gas and Water Supply Replacea
Page 105 and 106:
Electronic Parts Electronics - Righ
Page 107:
Electronics Main Supply Table 4-18.
Page 110 and 111:
Glossary: collision-induced dissoci
Page 112 and 113:
Glossary: IEEE IEEE Institute of El
Page 114 and 115:
Glossary: P/N P/N part number p-p p
Page 116 and 117:
Glossary: V dc V dc volts direct cu
Page 118 and 119:
Index: D control unit, for turbopum
Page 120 and 121:
Index: O O pressure 1-26 pressure r
Page 122:
Index: W quality 1-40 safety thresh
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LTQ Orbitrap XL Hardware Manual

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