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Chem 155 Unit 6 Page 132 of 316High Resolution and Echelle MonochromatorsAtomic spectroscopy demands high resolutionbecause atomic absorption / emission lines are:1. narrow 2.So we want effective bandwidth Δλ EFF =wD -1 = w d cos(r) / nF to be:We also want resolution (R = λ / Δλ = nN)to be:smalllargeΔλ EFFRw should be small -d should be small smallF should be large largen should be large largeBut there are limitations to the above:If w is too small 1 – no light 2 – exceedsw the ability to focus lightdFLimitations in the fabrication of gratingsHow big of a spectrometer is tolerable?What about n?n is the key…Page 132 of 316
Chem 155 Unit 6 Page 133 of 316A monochromator that operates in very high order iscalled:An Echelle monochromatorThe grooves are machined to reflect light at highincident angles – i and r are nearly identical and arecalled βAn echelle monochromator outperforms a Czerny-Turner monochromator in high-resolution applications:Czerny-Turner EchelleF / m 0.5 0.5Groove density 1200 / mm 79 / mmi,r or β 10° 63°R (300nm) 60,000 700,000D -1 (nm / mm) 1.6 0.15Page 133 of 316
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Full set of Notes with Fill-Ins - San Jose State University

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