Full set of Notes with Fill-Ins - San Jose State University

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Chem 155 Unit 14 250 of 316Handling of solids: pelletizing:grindput into die5 – 10 tons of pressurea few minutes…vacuum to reduce voidsHandling of Solids: mulling:sample2-5 mg2 μm“Nujol” =mineral(aliphatic ) oil1. Grind sample finely2. Mix with mulling oil3. Sandwich w/ KBr/NaClplatesor“Fluorolube” =fluorocarbon oilPage 250 of 316
Chem 155 Unit 14 251 of 316A general problem with pellets and mulls:A = -log[P/Po]How do you measure Po?You use an open beam to approximate PoSo – the spectra you obtain, are a sum ofabsorbances – the spectra contain:Sample plus window plus mulling oilabsorbance plus reflection losses.IR spectra obtained with these sampling methods areuseful for identification, not quantitation:qualitativeThe two pieces of information that are useful:Functional group identificationSpectral ‘fingerprinting’Page 251 of 316
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