Full set of Notes with Fill-Ins - San Jose State University

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Chem 155 Unit 11 206 of 316Lanthanide and Actinide Ions:Lanthanide and Actinice ions have unusual spectralproperties.• Lots of weak visibleand infrared lines• Very narrow bands!The 4f and 5f orbitalsare smaller than thefilled 6s and 7s orbitalsso the f orbitals are not‘split’ or broadenedvery much by solventligands• Electronicconfigurations differ inenergy due primarily toorbital angularmomentum, i.e.magnetic interactionsdescribed by Russell-Saunders and othercoupling schemes.Page 206 of 316
Chem 155 Unit 11 207 of 316Photometric TitrationTrace metals may be analyzed by by UV-Visabsorption using a method known as photometrictitration.For the complexation reaction:S + T PS = Analyte metal ion – e.g. Fe 3+T = Titrant – e.g. SCN -P = Product – e.g. FeSCN 2+Consider a big, stirred cuvette that you titrate with T.To which of the above schemes would the FeSCN 2+titration above correspond?Page 207 of 316
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Full set of Notes with Fill-Ins - San Jose State University

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