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Chem 155 Unit 8 Page 158 of 316Flame as ‘sample holder’:1.For best sensitivity:2.Page 158 of 316Interrogate with hollow cathoderadiation through ‘atom rich’ region.Changes in observation height:Change sensitivity – so don’t moveobservation region during experiment.
Chem 155 Unit 8 Page 159 of 316Optimal observation height:Optimize:Observation regionFlame stoichiometry1. Increased absorbance corresponds to:More gas phase atoms2. Absorbance normally starts low because:Molecules have not been broken downinto atoms yet3. Absorbance normally ends low because:Cr atoms form stable oxides and thisincreases with height.4. Cr profile decreases because:Cr atoms form stable oxides and thisincreases with height.5. Ag profile increases because:Ag atoms do not form stable oxidesPage 159 of 316
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