Full set of Notes with Fill-Ins - San Jose State University

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Chem 155 Unit 16 282 of 316Ionization Sources1.1.62 Electron Impact (EI):‘Hard’ ionization:extensive fragmentation1.1.63 Chemical Ionization:Derivative of EI but with 1000:1 excess of:reagent gas e.g.CH 4‘Soft’ ionization:limited fragmentationCH 4 collision with electron CH 4+ , CH 5+ , CH3 +CH 4+ , CH 5+ , CH3 + recombination, rxn w/ CH 4 C 2 H 5+CH 5+ + MH MH 2+ Proton transfer M+1+ CH 4C 2 H 5+ + M M C 2 H 5+ethyl transfer M+15Page 282 of 316
Chem 155 Unit 16 283 of 316Example of CI vs EI MS of 1-octanol:Electron impactionizationchemicalionization (CH 4 )Which is a ‘better’ MS?CI:EI:more easily interpretablecomplex, but highly uniquePage 283 of 316
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