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comprehensive site investigation and remediation objectives report

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CLIENT: Illinois Environmental Protection Agency<br />

Work Order: 0811162<br />

Project: LPC#1970905180<br />

ANALYTICAL QC SUMMARY REPORT<br />

TestCode:<br />

6020_S<br />

Sample ID: 0811162-001AMS<br />

SampType: MS<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 11/28/2008<br />

SeqNo: 522982<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Mercury 1.004 0.116 1.159 0 86.7 75 125<br />

0 0<br />

Nickel 51.15 0.579 28.97 27.36 82.1 75 125<br />

0 0<br />

Silver 22.16 0.579 28.97 0 76.5 75 125<br />

0 0<br />

Strontium 69.94 0.579 28.97 39.5 105 75 125<br />

0 0<br />

Thallium 27.51 0.579 28.97 0.3977 93.6 75 125<br />

0 0<br />

Vanadium 48.73 0.579 28.97 23.29 87.8 75 125<br />

0 0<br />

Zinc 61.35 1.16 28.97 40.97 70.3 75 125 0 0<br />

S<br />

Sample ID: 0811162-001AMS<br />

SampType: MS<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/1/2008<br />

SeqNo: 523481<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Boron 17.57 11.6 28.97 7.921 33.3 75 125 0 0<br />

S<br />

Selenium 21.37 0.579 28.97 0.5553 71.8 75 125 0 0<br />

S<br />

Sodium 195.3 57.9 289.7 70.83 43 75 125 0 0<br />

S<br />

Sample ID: 0811162-001AMS<br />

SampType: MS<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081201A<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523563<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Potassium 5795<br />

572 285.8 3571 779 75 125 0 0<br />

S<br />

Sample ID: 0811162-001AMS<br />

SampType: MS<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081201A<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523592<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Aluminum 17710 1140 28.58 13430 15000 75 125 0 0<br />

S<br />

Qualifiers:<br />

ND - Not Detected at the Reporting Limit<br />

S - Spike Recovery outside accepted recovery limits<br />

B - Analyte detected in the associated Method Blank<br />

J - Analyte detected below quantitation limits<br />

R - RPD outside accepted recovery limits<br />

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