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comprehensive site investigation and remediation objectives report

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CLIENT: Illinois Environmental Protection Agency<br />

Work Order: 0811162<br />

Project: LPC#1970905180<br />

ANALYTICAL QC SUMMARY REPORT<br />

TestCode:<br />

6020_S<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 11/28/2008<br />

SeqNo: 522983<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Zinc 61.61 1.17 29.17 40.97 70.8 75 125 61.35 0.428 20 S<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/1/2008<br />

SeqNo: 523482<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Boron 18.16 11.7 29.17 7.921 35.1 75 125 17.57 3.30 20 S<br />

Selenium 20.56 0.583 29.17 0.5553 68.6 75 125 21.37 3.86 20 S<br />

Sodium 200.8 58.3 291.7 70.83 44.6 75 125 195.3 2.81 20 S<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081201A<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523564<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Potassium 3971<br />

475 237.5 3571 168 75 125 5795 37.4 20 SR<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081201A<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523593<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Aluminum 13880<br />

950 23.75 13430 1890 75 125 17710 24.2 20 SR<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081202B<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523638<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Lead 33.48 23.7 23.75 11.68 91.8 75 125 39.42 16.3 20<br />

Mercury U 4.75 0.9499 0 0 75 125 0 0 20 S<br />

Qualifiers:<br />

ND - Not Detected at the Reporting Limit<br />

S - Spike Recovery outside accepted recovery limits<br />

B - Analyte detected in the associated Method Blank<br />

J - Analyte detected below quantitation limits<br />

R - RPD outside accepted recovery limits<br />

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