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comprehensive site investigation and remediation objectives report

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HAND AUGER SOIL SAMPLING PROTOCOLS<br />

Soil samples will be collected in laboratory-clean glass sample jars, <strong>and</strong> labeled with the<br />

designation, location, date <strong>and</strong> sampler. Collected samples will be preserved on ice <strong>and</strong><br />

picked up by the analytical laboratory. V3 st<strong>and</strong>ard chain-of-custody procedures will be<br />

followed regarding the shipment <strong>and</strong> receipt of samples.<br />

A h<strong>and</strong> auger will be used at the Site, to provide for visual observation of subsurface<br />

conditions, <strong>and</strong> the collection of soil samples at depth. The materials will be returned to<br />

the “hole” in the same manner as removed.<br />

Collected soil samples are visually classified in the field by Site engineer or geologist, in<br />

accordance with ASTM D 2488-84. Sample lithology is recorded using the Unified Soil<br />

Classification System. Soil logs, documenting soil types <strong>and</strong> subsurface conditions, will<br />

be completed by V3’s Site engineer or geologist.<br />

During sampling activities, soils will be screened for the presence of volatile organic<br />

compounds (VOCs) using a photoionization detector (PID). VOCs are common<br />

components of a variety of environmental contaminants, including industrial solvents,<br />

petroleum products <strong>and</strong> a wide range of other industrial compounds. The PID is also<br />

used to monitor ambient air concentrations within the work zone during the sampling, in<br />

accordance with V3’s Site Safety Plan. Personal protective equipment is utilized by<br />

sampling personnel during sampling, as specified in the Site Safety Plan.<br />

Soil samples that are collected for laboratory analysis will be placed in appropriate<br />

sample containers in order of decreasing volatility. For each recovered soil sample,<br />

samples for possible VOC analysis will be collected directly from the recovered sample,<br />

in accordance with USEPA SW-846 Method 5035/8260. Laboratory provided preweighed<br />

vials containing the correct amount of preservatives will be used (10 ml of<br />

methanol per vial <strong>and</strong> a 20% solution of sodium bisulfate (1 gram of sodium bisulfate to<br />

5 ml of water). All samples collected for VOCs will be obtained directly from the<br />

recovered sampler at the specified sample interval using a disposable plastic premeasured<br />

5-gram syringe barrel provided by the laboratory. The barrel will be driven<br />

into the soil surface to remove the soil without exposure to air. The soil will then be<br />

extruded into one 40-ml vial preserved with methanol. The threads of the sample vial<br />

should be cleaned prior to capping. This process will be repeated until two 40-ml vials<br />

preserved with sodium bisulfate are also filled with 5-grams of soil each. One four ounce<br />

jar or smaller will then be filled with soil for dry weight analysis. The samples will be<br />

immediately capped, labeled, <strong>and</strong> placed on ice. For all additional analysis, the<br />

remaining portion of the recovered sample from the specified sample interval will be<br />

homogenized <strong>and</strong> placed into appropriate laboratory specified jars. For all additional<br />

analysis, the remaining portion of the recovered sample from the specified sample<br />

interval will be placed into appropriate laboratory specified jars, labeled with the sample<br />

name, sample location, sample depth (if appropriate), date, time, preservative (if<br />

appropriate), <strong>and</strong> name of sampler. All samples will be immediately placed in a cooler<br />

filled with ice.<br />

To avoid cross-contamination, the h<strong>and</strong> auger will be cleaned between sampling<br />

locations, <strong>and</strong> soil residue is removed during this procedure. Sampling equipment used<br />

\\ilch-itfs01\V3il_Chi\ADMIN\STD OPERATING PROCEDURES\SOPs Source Docs\5.0 Data Gen <strong>and</strong> Acq\5.1 Field<br />

SOPs\Protocols\Drilling & Soil Sampling Protocols\H<strong>and</strong> Auger Soil Sampling Protocols.doc

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