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comprehensive site investigation and remediation objectives report

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CLIENT: Illinois Environmental Protection Agency<br />

Work Order: 0811162<br />

Project: LPC#1970905180<br />

ANALYTICAL QC SUMMARY REPORT<br />

TestCode:<br />

6020_S<br />

Sample ID: 0811162-001AMS<br />

SampType: MS<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 12/1/2008<br />

Run ID: ICPMS2_081202B<br />

Client ID:<br />

X101<br />

Batch ID: 13991 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 12/2/2008<br />

SeqNo: 523637<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Lead 39.42 28.6 28.58 11.68 97.1 75 125<br />

0 0<br />

Mercury U 5.72 1.143 0 0 75 125 0 0<br />

S<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 11/28/2008<br />

SeqNo: 522969<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Calcium 48200 4670 291.7 45050 1080 75 125 45560 5.63 20 S<br />

Iron 24130 2330 291.7 24480 -122 75 125 24620 2.03 20 S<br />

Magnesium 24650 4670 291.7 23270 472 75 125 23640 4.16 20 S<br />

Sample ID: 0811162-001AMSD<br />

SampType: MSD<br />

TestCode: 6020_S<br />

Units: mg/Kg-dry<br />

Prep Date: 11/24/2008<br />

Run ID: ICPMS2_081128B<br />

Client ID:<br />

X101<br />

Batch ID: 13963 TestNo: SW6020 (SW3050B)<br />

Analysis Date: 11/28/2008<br />

SeqNo: 522983<br />

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual<br />

Antimony 6.663 1.17 29.17 0.6892 20.5 75 125 7.425 10.8 20 S<br />

Arsenic 29.24 0.583 29.17 5.491 81.4 75 125 28.98 0.892 20<br />

Barium 68.39 0.583 29.17 39.86 97.8 75 125 68.44 0.0721 20<br />

Beryllium 5.363 0.583 29.17 0.1241 18 75 125 5.039 6.24 20 S<br />

Cadmium 24.45 0.583 29.17 0.1018 83.5 75 125 24.5 0.210 20<br />

Chromium 48.19 0.583 29.17 21.2 92.5 75 125 48.35 0.319 20<br />

Cobalt 34.72 0.583 29.17 10.82 81.9 75 125 35.18 1.34 20<br />

Copper 37.22 1.17 29.17 14.99 76.2 75 125 37.98 2.00 20<br />

Lead 40.25 0.583 29.17 12.3 95.8 75 125 41.04 1.94 20<br />

Manganese 464.4 0.583 29.17 424.2 138 75 125 461.3 0.668 20 S<br />

Mercury 1.033 0.117 1.167 0 88.5 75 125 1.004 2.82 20<br />

Nickel 49.64 0.583 29.17 27.36 76.4 75 125 51.15 3.00 20<br />

Silver 21.9 0.583 29.17 0 75.1 75 125 22.16 1.15 20<br />

Strontium 68.98 0.583 29.17 39.5 101 75 125 69.94 1.38 20<br />

Thallium 27.66 0.583 29.17 0.3977 93.4 75 125 27.51 0.524 20<br />

Vanadium 48.79 0.583 29.17 23.29 87.4 75 125 48.73 0.120 20<br />

Qualifiers:<br />

ND - Not Detected at the Reporting Limit<br />

S - Spike Recovery outside accepted recovery limits<br />

B - Analyte detected in the associated Method Blank<br />

J - Analyte detected below quantitation limits<br />

R - RPD outside accepted recovery limits<br />

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