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Grace Catalog 2008

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gas chromatography<br />

Graphitized Carbon Blacks<br />

Carbograph Packings<br />

• High speed analysis<br />

• Extremely hydrophobic—ideal for aqueous injections<br />

Equivalent to the Carbopack packings. Carbograph<br />

packings can be modified with a stationary phase giving them<br />

unique selectivities.<br />

Carbograph 1<br />

Equivalent to Carbopack B. It has a surface area of<br />

100m 2 /g. Carbograph 1-TD has a coarse mesh of 20/40<br />

which is suitable for thermal desorption work. Maximum<br />

temperature 500°C.<br />

Carbograph 1SC<br />

Similar to Carbopack BHT, specifically for the separation of<br />

sulfur compounds. It has a mesh of 40/60, and a maximum<br />

temperature of 225°C.<br />

Carbograph 2<br />

Equivalent to Carbopack C. It has a specific surface of<br />

10m 2 /g for the separation of volatile organic compounds.<br />

Carbograph 2-TD has a coarse mesh of 20/40 which<br />

is suitable for thermal desorption work. Maximum<br />

temperature 500°C.<br />

Carbograph<br />

Description Qty. Part No.<br />

Uncoated<br />

Carbograph 1-TD, 20/40, >500°C 15g 1740<br />

Carbograph 1, 60/80, >500°C 10g 1722<br />

Carbograph 1 80/120, >500°C 10g 1724<br />

Carbograph 2-TD, 20/40, >500°C 15g 1745<br />

Carbograph 2, 60/80, >500°C 10g 1726<br />

Carbograph 2, 80/100, >500°C 10g 1728<br />

Carbograph 1-SC, 40/60, 225°C 10g 1734<br />

Coated<br />

1% AT-1000 on Carbograph 1 60/80, 225°C 15g 1733<br />

0.1% AT-1000 on Carbograph 2<br />

15g 1737<br />

80/100, 225°C<br />

4% Carbowax ® 20M on Carbograph 1 DA 15g 17271<br />

80/120, 200°C<br />

0.2% Carbowax ® 1500 on Carbograph 2 15g 1725<br />

60/80, 175°C<br />

0.2% Carbowax ® 1500 on Carbograph 2 15g 1720<br />

80/100, 175°C<br />

5% Carbowax ® 20M on Carbograph<br />

15g 1729<br />

1 AW 80/120, 225°C<br />

6.6% Carbowax ® 20M on Carbograph 1 AW 15g 1731<br />

80/120, 225°C<br />

4% Carbowax ® 20M + 0.8% KOH on<br />

15g 1735<br />

Carbograph 1 60/80, 220°C<br />

0.19% Picric Acid on Carbograph 2<br />

15g 1736<br />

80/100, 120°C<br />

0.8% THEED on Carbograph 2 80/100, 125°C 15g 1942<br />

Graphpac-GC and -GB Packings<br />

• Graphitized carbon<br />

• Inert, non-specific surface<br />

• Unique separation properties<br />

• Optimized phase loading<br />

• Hydrophobic—ideal for aqueous injections<br />

Graphpac-GC has an average surface area of<br />

10–13m 2 /g, while Graphpac-GB has a larger surface area<br />

of 100–110m 2 /g. Both types interact with samples almost<br />

completely by non-specific adsorption. Which results in unique<br />

separations not achievable with fused silica open tubular<br />

(FSOT) capillary columns. Alcohols, hydrocarbons, and acids<br />

are separated in series according to carbon number.<br />

The carbons possess partitioning capabilities as uncoated<br />

packings, use stationary phases to modify the selectivity of<br />

these carbons.<br />

Graphpac<br />

Description Qty. Part No.<br />

Graphpac-GC<br />

0.1% AT-1000, 225°C, 80/100 15g 8542<br />

0.2% Carbowax ® 1500, 175°C, 80/100 15g 8546<br />

0.19% Picric Acid, 120°C, 80/100 15g 8550<br />

0.8% THEED, 125°C, 80/100 15g 8552<br />

Uncoated, 60/80 15g 8536<br />

Uncoated, 80/100 15g 8538<br />

Custom—Specify Phase and % Loading 15g C-2200<br />

Graphpac-GB<br />

1% AT-1000, 225°C, 60/80 15g 8517<br />

4% Carbowax ® 20M + 0.8% KOH Amines, 15g 8519<br />

220°C, 60/80<br />

Uncoated, 60/80 15g 8513<br />

Uncoated, Acid Washed, 60/80 15g 8533<br />

Custom—Specify Phase, Mesh, and % Loading 15g C-2200<br />

Custom, Acid Washed—Specify Phase, Mesh, 15g C-2300<br />

and % Loading<br />

Stock Packed Columns<br />

6ft x 1/8" SS Packed with 0.1% AT-1000, ea 8542PC<br />

225°C, 80/100<br />

6ft x 1/8" SS Packed with 0.2% Carbowax ® 1500, ea 8546PC<br />

175°C, 80/100<br />

7ft x 1/8" SS Packed with 0.19% Picric Acid, ea 85501PC<br />

120°C 80/100<br />

10ft x 1/8" SS Packed with 5% Krytox ® 143°C,<br />

60/80<br />

ea 85222<br />

gc columns | packed<br />

www.discoverysciences.com<br />

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