Grace Catalog 2008

gc applications
Semivolatiles
Column:
Temp:
Carrier Gas:
Detector:
1. Phenol
2. 2-Chlorophenol
3. 2-Nitrophenol
4. 2,4-Dimethylphenol
5. 2,4-Dichlorophenol
Phenols
6. 4-Chloro-3-Methylphenol
7. 2,4,6-Trichlorophenol
8. 2,4-Dinitrophenol
9. 4-Nitrophenol
10. 2-Methyl-4,6-Dinitrophenol
11. Pentachlorophenol
Heliflex ® AT-5, 30m x 0.25mm x 0.25µm
(Part No. 13656)
70°C (2 min hold) to 230°C at 8°C/min
Helium at 0.8mL/min
FID
Phthalate and Adipate Esters
2286
1. 1,3-Dichlorobenzene
2. 1,4-Dichlorobenzene
3. 1,2-Dichlorobenzene
4. Hexachloroethane
Base/Neutral Mix
5. Nitrobenzene
2207
6. Isophorone
7. 1,2,4-Trichlorobenzene
8. Hexachlorobutadiene
9. Hexachlorocyclopentadiene
10. 2-Chloronaphthalene
11. 2,6-Dinitrotoluene
12. 2,4-Dinitrotoluene
13. Azobenzene
14. Hexachlorobenzene
Column: Heliflex ® AT-5, 30m x 0.32mm x 0.25µm
(Part No. 13658)
Temp:
60°C (2 min hold) to 205°C at 8°C/min
Carrier Gas: Helium at 2.2mL/min
Detector: FID
EPA Method 606 - Phthalates
0
1
2
3
4
5
6 7
5 10 15 20 25 30 35 40 45 Min.
2104
1. Dimethyl Phthalate
2. Diethyl Phthalate
3. Di-n-Butyl Phthalate
4. Butylbenzyl Phthalate
5. Di(2-ethylhexyl) Adipate
6. Di(2-ethylhexyl) Phthalate
7. Di-n-Octyl Phthalate
Column: Heliflex ® AT-1, 30m x 0.32mm x 0.25µm
(Part No. 13640)
Temp:
60°C (1 min hold) to 260°C at 6°C/min
Carrier Gas: Helium at 32cm/sec
Detector: FID at 295°C
0
Column:
1
2
3
4 8 12 16 20 24 28 Min.
Temp:
Carrier Gas:
Detector:
4
5
6
1. Dimethylphthalate (20ng)
2. Diethylphthalate (20ng)
3. Di-n-butylphthalate (20ng)
4. Butylbenzyl Phthalate (20ng)
5. Bis(2-ethylhexyl)phthalate (20ng)
6. Di-n-octylphthalate (20ng)
Heliflex ® AT-5, 15m x 0.53mm x 1.00µm
(Part No. 13569)
115°C (4 min hold) to 250°C at 10°C/min
Helium at 3.4mL/min (35cm/sec)
FID
2583
environmental
EPA SW846 Method 8091
Nitroaromatics and Cyclic Ketones
EPA Method 612: Chlorinated Hydrocarbons
2114
1840
1. Isophorone
4. 2,6-Dinitrotoluene
1 2 2. Nitrobenzene
5. 1,3-Dinitrobenzene
3. 1,4-Napthoquinone 6. 2,4-Dinitrotoluene
3 4 6 5
1 23 4
5
6
7
8
9
1. 1,3-Dichlorobenzene
2. 1,4-Dichlorobenzene
3. 1,2-Dichlorobenzene
4. Hexachloroethane
5. 1,2,4-Trichlorobenzene
6. Hexachlorobutadiene
7. Hexachlorocyclopentadiene
8. 2-Chloronaphthalene
9. Hexachlorobenzene
0 4 8 12 16 20 Min.
Column: Heliflex ® AT-1701, 30m x 0.53mm x 1.00µm
(Part No. 13795)
Temp:
120°C (2 min hold) to 200°C at 3°C/min
Carrier Gas: Helium at 44.5cm/sec
Detector: FID
0 2 4 6 8 10 12 14 16 18 Min.
Column: Heliflex ® AT-1301, 30m x 0.53mm x 1.00µm
(Part No. 13970)
Temp:
90°C (4 min hold) to 190°C at 10°C/min
Carrier Gas: Helium at 8.1mL/min
Detector: FID
more applications
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