Grace Catalog 2008
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hplc applications<br />

food & beverage<br />

Oils / Lipids<br />

5 Palm Kernel Olein Fraction<br />

2<br />

1<br />

7<br />

3 4<br />

89 10 11 12 17<br />

14 15 16<br />

6<br />

13<br />

0 5 10 15 20 25 30 Min.<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm,<br />

150 x 3.0mm (Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

Coconut Oil<br />

2<br />

1<br />

4 5 3<br />

6<br />

7<br />

9<br />

8 10 11 12<br />

0 5 10 15 20 25 30 35 Min.<br />

1<br />

2<br />

3<br />

4<br />

5 6 7 8 9<br />

13<br />

1. CCLa<br />

2. C11<br />

3. CLaLa<br />

4. CCM<br />

5. LaLaLa<br />

6. CLaM<br />

7. LaLaM<br />

8. LaLaO<br />

9. LaMM<br />

1. CCLa<br />

2. C11<br />

3. CLaLa<br />

4. CCM<br />

5. LaLaLa<br />

6. CLaM<br />

10573<br />

10. LaMO<br />

11. LaMP/MMM<br />

12. MMO/LaPO<br />

13. MMP/LaPP/MPO<br />

14. PLP<br />

15. POO<br />

16. POP<br />

17. C17<br />

10564<br />

7. LaLaM<br />

8. LaLaO<br />

9. LaMM<br />

10. LaMO<br />

11. LaMP/MMM<br />

12. MMP/LaPP/MPO<br />

13. C17<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm, 150 x 3.0mm<br />

(Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

Sunflower Oil<br />

1. LLL<br />

2. LLO<br />

3. PLL<br />

4. LOO<br />

5. LLS<br />

6. PLO<br />

7. OOO<br />

8. SLO<br />

9. POO<br />

10567<br />

0 5 10 15 20 25 30 Min.<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm,<br />

150 x 3.0mm (Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

Cocoa Butter<br />

9<br />

0 5 10 15 20 25 30 35 Min.<br />

1<br />

1<br />

2<br />

3<br />

6<br />

23 4 5 7 8<br />

Butter<br />

11<br />

13<br />

10 12<br />

4 5 67<br />

8 9 10<br />

11<br />

14<br />

1. C13<br />

2. PLO<br />

3. PLP<br />

4. POO<br />

5. PLS<br />

6. POP<br />

7. SOO/PPP<br />

8. SLS<br />

9. POS<br />

10. PPS<br />

11. SOS<br />

12. PSS<br />

13. SOA<br />

14. C19<br />

10563<br />

10565<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm, 150 x 3.0mm<br />

(Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

Refined Sunflower Oil<br />

1. C11<br />

2. LLL<br />

3. LLO<br />

4. PLL<br />

5. LOO<br />

6. LLS<br />

7. PLO<br />

8. OOO<br />

9. SLO<br />

10. POO<br />

11. C17<br />

10569<br />

0 5 10 15 20 25 30 35 Min.<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm,<br />

150 x 3.0mm (Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

0 5 10 15 20 25 30 Min.<br />

Column: Alltech ® Alltima HP C18 Hi-Load, 3µm,<br />

150 x 3.0mm (Part No. 87610)<br />

Mobile Phase: A: Acetonitrile B: Dichloromethane<br />

Gradient: Time: 0 25 26 27 28<br />

%B: 30 51 70 70 30<br />

Flow Rate: 0.72mL/min<br />

Detector: ELSD<br />

426<br />

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