Grace Catalog 2008
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gc applications<br />

Steroids<br />

1<br />

2 3<br />

4<br />

5<br />

6<br />

7<br />

Steroids, TMS Derivatives<br />

11<br />

10<br />

12<br />

0 2 4 6 8 10 12 14 Min.<br />

8<br />

9<br />

1. Androsterone<br />

2. Estrone<br />

3. Estradiol<br />

4. Testosterone<br />

5. Progesterone<br />

6. 5-α-Cholestane<br />

(underivatized)<br />

7. Estriol<br />

8. Coprostanol<br />

9. Cholesterol<br />

10. Campesterol<br />

11. Stigmasterol<br />

12. β-Sitosterol<br />

Column: Econo-Cap EC-1, 30m x 0.32mm x 0.25µm<br />

(Part No. 19651)<br />

Temp: 290°C<br />

Carrier Gas: Helium at 1.09mL/min<br />

Detector: FID<br />

1008<br />

1<br />

2 3<br />

4<br />

5<br />

Anabolic Steroids<br />

1. Nandrolone<br />

2. Testosterone<br />

3. Norethandrolone<br />

4. Clostebol<br />

5. Fluoxymesterone<br />

0 2 4 6 8 10 Min.<br />

Column: Econo-Cap EC-5, 30m x 0.25mm x 0.25µm<br />

(Part No. 19647)<br />

Temp: 300°C<br />

Carrier Gas: Helium at 0.65mL/min<br />

Detector: FID<br />

1019<br />

environmental<br />

Chlorinated Disinfection<br />

EPA Method 551: Chlorinated Disinfection<br />

<br />

Byproducts by NPD<br />

2280<br />

<br />

1. Trichloroacetonitrile<br />

2. Dichloroacetonitrile<br />

3. Bromochloroacetonitrile<br />

4. Dibromoacetonitrile<br />

<br />

<br />

Column: Heliflex ® AT-5, 30m x 0.32mm x 0.25µm<br />

(Part No. 13658)<br />

Temp:<br />

55°C (2 min hold) to 75°C at 5°C/min<br />

Carrier Gas: Helium at 2.2mL/min<br />

Detector: NPD<br />

Haloacetic Acids<br />

EPA Method 552.1: Haloacetic Acids<br />

1. Monochloroacetic Acid<br />

2. Monobromoacetic Acid<br />

3. Dalapon<br />

4. Dichloroacetic Acid<br />

5. Trichloroacetic Acid<br />

6. Bromochloroacetic Acid<br />

7. Dibromoacetic Acid<br />

0<br />

Column:<br />

Temp:<br />

Carrier Gas:<br />

Detector:<br />

1<br />

4<br />

2<br />

3<br />

2 4 6 8 10 12 14 16 18 Min.<br />

Heliflex ® AT-1701, 30m x 0.32mm x 0.25µm<br />

(Part No. 13690)<br />

50°C (10 min hold) to 120°C at 10°C/min<br />

Helium at 35cm/sec<br />

ECD<br />

5<br />

6<br />

7<br />

2105<br />

Pesticides<br />

1 2 3<br />

4<br />

Carbamates<br />

1. Naled<br />

2. Metacil<br />

3. Zectran<br />

4. Carbaryl<br />

1232<br />

Organophosphorus Pesticides<br />

1. TEPP<br />

14. Carbophenothion<br />

2. Sulfotepp<br />

15. Phosmet<br />

3. Monocrotophos 16. EPN<br />

4. Dimethoate 17. Leptophos<br />

5. Dioxathion<br />

18. Azinphos-ethyl<br />

6. Terbufos<br />

2<br />

7. Phosphamidon<br />

4<br />

8. Malathion<br />

6<br />

9. Parathion<br />

10. cis-Chlorfenvinphos<br />

3<br />

11. trans-Chlorfenvinphos<br />

12. Ethion<br />

1<br />

13. Famphur<br />

5<br />

7<br />

8 9<br />

10<br />

11<br />

16<br />

12<br />

14<br />

13 15 17 18<br />

2469<br />

0 5 Min.<br />

Column: Heliflex ® AT-Pesticide, 20m x 0.53mm x 0.60µm<br />

(Part No. 16846)<br />

Temp: 200°C<br />

Carrier Gas: Helium at 7.5mL/min<br />

Detector: ECD<br />

Column:<br />

Temp:<br />

Carrier Gas:<br />

Detector:<br />

4 8 12 16 20 24 28 32 36 40 Min.<br />

Heliflex ® AT-5ms, 30m x 0.25mm x 0.25µm<br />

(Part No. 15807)<br />

120°C (3 min hold) to 285°C at 5°C/min<br />

Helium at 26cm/sec<br />

MSD<br />

468<br />

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