Grace Catalog 2008

gc applications
Pharmaceuticals
1 2
Depressants
3
4
5
1. Glutethimide
2. Methaqualone
3. Diazepam
4. Chlorpromazine
5. Flurazepam
2560
1
2
3
4
Anticonvulsants
5 6
1. Ethosuximide
2. Methsuximide
3. Normethsuximide
4. Mephenytoin
5. PEMA
6. MPEMA
2568
0
2 4 6 8 10 12 14 Min.
Column: Heliflex ® AT-5ms, 30m x 0.25mm x 0.25µm
(Part No. 15807)
Temp: 270°C
Carrier Gas: Helium at 0.65mL/min (24cm/sec)
Detector: FID
0 1 2 3 4 5 6 Min.
Column: Heliflex ® AT-5ms, 15m x 0.25mm x 0.25µm
(Part No. 15801)
Temp:
190°C (1 min hold) to 235°C at 10°C/min
Carrier Gas: Helium at 0.7mL/min (26cm/sec)
Detector: FID
Antidepressants
Antihistamines
2187
4
1005
drugs
1
3
4
2
6
5
7
8
1. Amitriptyline
2. Trimipramine
3. Doxepin (cis-Doxepin)
4. Imipramine
5. Doxepin (trans-Doxepin)
6. Desipramine
7. Maprotyline
8. Clomipramine
1
2
3
5
6
7
1. Pheniramine
2. Doxylamine
3. Orphenadrine
4. Methapyraline
5. Chlorpheniramine
6. Diphenylpyraline
7. Promethazine
0
4 8 12 16 20 Min. 0 2 4 6 8 Min.
Column: Econo-Cap AT-20, 30m x 0.32mm x 0.25µm
(Part No. 19677)
Temp: 235°C
Carrier Gas: Helium at 22 cm/sec
Detector: FID
Antihistamines
Column: Econo-Cap EC-1, 15m x 0.53mm x 1.20µm
(Part No. 19650)
Temp: 210°C
Carrier Gas: Helium at 8.5mL/min
Detector: FID
Hypnotics
2567
4
1009
1
3
2
4 5 6
1. Pheniramine
2. Doxylamine
3. Orphenadrine
4. Methapyraline
5. Chlorpheniramine
6. Diphenylpyraline
2
3
5
1. Trichloroethanol
2. Allobarbital
3. Butabarbital
4. Secobarbital
5. Methaqualone
1
0
1 2 3 4 5 Min.
0 2 4 6 8 10 12 14 Min.
Column:
Temp:
Carrier Gas:
Detector:
Heliflex ® AT-5ms, 15m x 0.25mm x 0.25µm
(Part No. 15801)
210°C (1 min hold) to 230°C at 5°C/min
Helium at 0.7mL/min (25cm/sec)
FID
Column:
Temp:
Carrier Gas:
Detector:
Econo-Cap EC-1, 30m x 0.32mm x 0.25µm
(Part No. 19651)
160°C to 220°C at 10°C/min
Helium at 1.08mL/min
FID
466
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