Grace Catalog 2008

gc applications
Semivolatiles
EPA Method 610: Polynuclear Aromatic Hydrocarbons
Fast PAH Analysis
1. Naphthalene
2. Acenaphthylene
3. Acenaphthene
4. Fluorene
5. Phenanthrene 2208
6. Anthracene
7. Fluoranthene
8. Pyrene
9. Benz[a]anthracene
10. Chrysene
11. Benzo[b]fluoranthene
12. Benzo[k]fluoranthene
13. Benzo[a]pyrene
14. Indeno[1,2,3-c,d]pyrene
15. Dibenz[a,h]anthracene
16. Benzo[g,h,i]perylene
1. Naphthalene
2. Acenaphthylene
3. Acenaphthene
4. Fluorene
5. Phenanthrene
6. Anthracene
7. Fluoranthene
2284
8. Pyrene
9. Benz[a]anthracene
10. Chrysene
11. Benzo[b]fluoranthene
12. Benzo[k]fluoranthene
13. Benzo[a]pyrene
14. Indeno[1,2,3-c,d]pyrene
15. Dibenz[a,h]anthracene
16. Benzo[g,h,i]perylene
Column: Heliflex ® AT-5, 30m x 0.32mm x 0.25µm
Column: Heliflex ® AT-5, 10m x 0.10mm x 0.10µm
(Part No. 13658)
(Part No. 14438)
Temp:
60°C (2 min hold) to 315°C at 8°C/min
Temp:
100°C to 340°C at 20°C/min
Carrier Gas: Helium at 1.6mL/min
Carrier Gas: Helium at 0.1mL/min (25 cm/sec)
Detector: FID
Detector: FID
environmental
PAHs
Column:
Temp:
Carrier Gas:
Detector:
1. Naphthalene
2. Acenaphthylene
3. Acenaphthene
4. Fluorene
5. Phenanthrene
6. Anthracene
7. Fluoranthene
8. Pyrene
9. Benz[a]anthracene
10. Chrysene
11. Benzo[b]fluoranthene
12. Benzo[k]fluoranthene
13. Benzo[a]pyrene
14. Indeno[1,2,3-c,d]pyrene
15. Dibenz[a,h]anthracene
16. Benzo[g,h,i]perylene
Heliflex ® AT-5ms, 30m x 0.25mm x 0.25µm
(Part No. 15807)
80°C (1 min hold) to 160°C at 25°C/min,
to 300°C at 3°C min,
to 325°C at 25°C/min
Helium at 0.8mL/min (26cm/sec)
FID
2463
Phenols Mix on AT-1ms
2621
1. Phenol
2. 2-Chlorophenol
3. o-Cresol
4. m & p-Cresol
5. 2-Nitrophenol
6. 2,4-Dimethylphenol
7. 2,4-Dichlorophenol
8. 2,6-Dichlorophenol
9. 4-Chloro-3-methylphenol
10. 2,4,6-trichlorophenol
11. 2,4,5-Trichlorophenol
12. 2,4-Dinitrophenol
13. 4-Nitrophenol
14. 2,3,4,6-Tetrachlorophenol
15. 2-Methyl-4,6-dinitrophenol
16. Pentachlorophenol
Column: Heliflex ® AT-1ms, 30m x 0.25mm x 0.25μm
(Part No. 15897)
Temp:
60°C (0.5 min hold) to 235°C at 10°C/min
Carrier:
Helium at 1mL/min (28cm/sec)
Detector: FID at 340°C
472
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