Guidelines for care & Use of Dry Solvent Stills [Example]

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In-house Monitoring of Research Laboratory Safety Conditions In an effort to encourage closer scrutiny of possible safety problems within each research laboratory, the Laboratory Manager is asking each research group to consider filling out the following two forms weekly (or bi-weekly) and keep them recorded in a notebook or file close to your Chemical Hygiene Plan Manual. Once a month, the Laboratory Manager will check out each laboratory and offer suggestions for improvements. The Laboratory Manager will also check the above mentioned records. An additional form for overnight reactions is meant for attachment on hoods next to reaction apparatus (not too close - otherwise they would burn up along with your ill-planned experiment!). Please note that additional plastic, wire, and metal hose clamps of various sizes are located in countertop drawers in the stockroom (#110) for tightening water hose connections on distillation apparatus. Also, the Laboratory Manager has ordered more miniature submersible pumps for each research laboratory, and has already distributed them. Please do not reflux overnight reactions with water faucet-condenser connections - use water bath pumps or recirculators as sources of water. Ace glass wire hose clamps are cheap and best for standard size hose connections to condenser apparatus. Order them from Ace Glass (catalog # 11145-20, tubing clamp, phone # 1-800-223-4524). Keep all or only a portion of the following procedures in your CHP, depending upon whether they are actually applicable to your laboratory setting. If some of the instruments or facilities listed in the nightly shutdown procedure are not present in your lab, discard these entries. If you would rather extend the time period for inspections or change the days, etc., just change the forms via work processor and write your own. At the very least, please use the “overnight reaction in progress” form with all indicated phone numbers for emergency contact. 144
OVERNIGHT REACTION IN PROGRESS In case of malfunction, please contact: Graduate Student Phone Number Dr. Phone Number Actions to be take in case of malfunction: 1. Turn off the stirrer/hotplate 2. Cut off water faucet 3. Call security in case of extensive damage (5911) or clear indications of problems with fire, flooding, electrical shortage, etc. 4. Other 145
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Wake Forest University Chemistry De
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11. Dr. Lachgar - Lab Room # 6 ....
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I. INTRODUCTION A hardcopy of this
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II. Telephone #s of Emergency Perso
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B. Emergency Exit Plan for All Sale
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A. Emergency Telephone Numbers of L
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2. Dr. Bierbach - Lab Room #107 Lab
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4. Dr. Buchmueller - Lab Room #1 La
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6. Dr. Hinze - Lab Room #109 Lab Pe
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8. Dr. Paul Jones - Lab Room #113 L
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10. Dr. Kondepudi - Lab Room #5 Lab
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12. Dr. Noftle - Lab Room #117 Lab
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14. Dr. Tobey - Room # 2 Lab Person
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16. Undergraduate - Lab Room #s 7,
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11. Do not force glass tubing into
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2. Cleanliness in the Research Labo
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3. Housekeeping for All Labs Housek
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INVENTORY OF EYEWASH FOUNTAINS AND
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“COMMON FIRE CODE VIOLATIONS “E
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) 4-Bromodimethylaniline HAZARDOUS
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manager and stockroom personnel usi
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Mineral acids (HCl, HNO 3 and H 2 S
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1. “Lecture Bottles must be Mathe
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(one kilogram per month, total amou
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All other organic solvents not on t
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2. Personal Protective Equipment: L
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3. VENTILATION AND PROPER USE OF HO
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3. Preliminary Considerations for S
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OPERATING INFORMATION FOR FHM 400 F
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6. Visionaire or Supreme Air hood o
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4. Chemical Storage in Research Lab
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E. Laboratory Operations which requ
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F. Provisions for Additional Protec
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G. Specific Procedures for Safe Rem
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2. Dr. Bierbach - Lab Room #107 SPE
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3. Dr. Brown - Lab Room #14 SPECIFI
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Dry soft things: Weighing paper, pa
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5. Dr. Colyer - Lab Room # 114 SPEC
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6. Dr. Hinze - Lab Room # 109 SPECI
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8. Dr. Paul Jones - Lab Room # 14 S
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10. Dr. Kondepudi - Lab Room # 5 SP
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� Ammonium hydroxide � Ammonium
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13. Dr. Swofford - Lab Room # 1 SPE
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� Hydrochloric acid � Acetic ac
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15. Dr. Welker - Lab Room # 13 SPEC
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H. Specific Decontamination Procedu
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Page 185 and 186: B. Instructions for the Use of the
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Guidelines for care & Use of Dry Solvent Stills [Example]

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