Guidelines for care & Use of Dry Solvent Stills [Example]

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D. TRAINING FOR GRADUATE STUDENTS, POST-DOCTORATES, AND RESEARCH UNDERGRADUATES .......... 168 1. Certification of Safety Training Form for Graduate Students, Post-Graduates, and Summer School Undergraduate Research Students .......................................................................................................... 169 2. Yearly Announcement of Gas Cylinder Safety and New Graduate Student Safety Review ................ 170 3. Summer School Safety Training Announcement for Research Undergrads: ...................................... 171 4. New Graduate Student and new Undergraduate Research Student Safety Orientation Announcement, in August of each year: ............................................................................................................................ 172 V. CHEMISTRY DEPARTMENT PURCHASE ORDER REQUEST SYSTEM .............................. 173 VI. PURCHASING PROCEDURE FOR DEA CONTROLLED SUBSTANCES ............................... 182 VII. ALCOHOL DISPENSING PROCEDURE..................................................................................... 183 VIII. OSHA/EPA INSPECTION PROCEDURE FOR SALEM HALL ............................................... 183 IX. CHEMICAL INVENTORIES ............................................................................................................ 184 A. INVENTORY OF ALL CHEMICALS AND MSDS SHEETS IN THE CHEMISTRY DEPARTMENT ........................ 184 B. INSTRUCTIONS FOR THE USE OF THE ONLINE INVENTORY SYSTEM ......................................................... 185 C. GENERAL INFORMATION FOR USERS ....................................................................................................... 187 D. INDIVIDUAL CHEMICAL INVENTORIES OF THE CHEMISTRY DEPARTMENT, SALEM HALL: ....................... 188 iv
I. INTRODUCTION A hardcopy of this Chemical Hygiene Plan and Safety Manual will be kept in the Chemistry Department Stockroom, Room 110, near the MSDS sheet collection, for your reference. Individual lab copies of the National Research Council’s Prudent Practices in the Laboratory, 2nd edition. Washington, D.C.: National Academy Press, 1995, hereinafter referred to as Prudent Practices, 2nd edition, will be kept in each research Lab as well as the stockroom. View the online Chemical Hygiene Plan and Safety Manual from the University Web site at http://www.wfu.edu/chem/cheminventory/index.html , Throughout this manual, you will find specific references to suggested reading of certain sections of Prudent Practices, 2nd edition (indicated in boldface type throughout). You are REQUIRED to read OSHA’s “Laboratory Standard”, a copy of which is located in Appendix A on pages 219-225 of that monograph (or at the internet site http://www.oshaslc.gov/OshStd_data/1910_1450.html). This is a reprint of the most recent governmental regulation governing all chemical laboratories under US jurisdiction. Upon graduation and exposure to any workplace laboratory in the country you will soon discover that companies and institutions will appreciate spending less time training new employees in their particular CHP as a direct result of your having read and understood the present one. This document was prepared in a Workbook format, with the help and assistance of students, staff, and Faculty personnel within the Chemistry and Physics departments. All sections in black type in this manual are meant to be read by all Lab workers in this building. All sections in red type are presented only as an elaboration of the Laws presently governing Laboratory work involving the use of chemicals. They need not be read by anyone other than WFU Safety staff members involved with interpreting OSHA Laws and as guidelines for interested Faculty members and students. For example, it is not necessary to read the chapter titled “Emergency Telephone numbers of Lab Supervisors and Lab Workers”. Likewise, the chapter titled “Summary of Regulated Chemicals Covered by this SOP (Standard Operating Procedure)” is meant only for WFU Safety Personnel and interested Faculty members wishing to review what the Law stipulates in a particular situation Also, it is not necessarily important to read all SOPs in the chapter titled “Laboratory Specific SOPs (Standard Operating Procedures)”. Please read only the SOPs (Standard Operating Procedures) which apply to your particular Research Laboratory. The following Safety Record-keeping forms will be filled out and recorded by the Chemistry Department’s Laboratory Manager, Chemistry Department Faculty members, Graduate Students, qualified Undergraduate stockroom personnel, Physical Facilities personnel, or Mr. Scott Frazier [WFU Assistant Environmental Health and Safety (EHS) Director] (phone #758-4329, or 758-4224) or Michelle Adkins, CHMM, Wake Forest University Director of Environmental Health and Safety: adkinsmm@wfu.edu, phone: 336-758-5385, cell: 336-480-8480, fax: 336-758-3088). The particular Safety Record-Keeping Forms and their storage locations in the Chemistry Department or elsewhere are listed below. Generally, the forms will be kept in the Chemistry Stockroom, room #110, in the top two file drawers of the tan colored OSHA file storage cabinet, next to the side-room #110D. If any particular form is kept elsewhere in the building or with the WFU Environmental Health and Safety Department, its location will be listed below. Spare Keys to the Chemistry Department‟s OSHA drawer are kept with the WFU Environmental Health and Safety Department, c/o Mr. Scott Frazier or Ms. Michelle Adkins. � Eyewash Fountain and Safety Shower Inspections, Physical Facilities, c/o Scott Frazier � Fume Hood Air-Flow Inspections, Physical Facilities, c/o Scott Frazier � Filled out Accident and Chemical Exposure Assessment Report forms, OSHA drawer, Chemistry Department Stockroom # 110 � Sophomore Chemistry Lab 221L Safety Quizzes, OSHA drawer, Chemistry Department Stockroom # 110 5
Page 1 and 2: Wake Forest University Chemistry De
Page 3: 11. Dr. Lachgar - Lab Room # 6 ....
Page 7 and 8: II. Telephone #s of Emergency Perso
Page 9 and 10: B. Emergency Exit Plan for All Sale
Page 11 and 12: A. Emergency Telephone Numbers of L
Page 13 and 14: 2. Dr. Bierbach - Lab Room #107 Lab
Page 15 and 16: 4. Dr. Buchmueller - Lab Room #1 La
Page 17 and 18: 6. Dr. Hinze - Lab Room #109 Lab Pe
Page 19 and 20: 8. Dr. Paul Jones - Lab Room #113 L
Page 21 and 22: 10. Dr. Kondepudi - Lab Room #5 Lab
Page 23 and 24: 12. Dr. Noftle - Lab Room #117 Lab
Page 25 and 26: 14. Dr. Tobey - Room # 2 Lab Person
Page 27 and 28: 16. Undergraduate - Lab Room #s 7,
Page 29 and 30: 11. Do not force glass tubing into
Page 31 and 32: 2. Cleanliness in the Research Labo
Page 33 and 34: 3. Housekeeping for All Labs Housek
Page 35 and 36: INVENTORY OF EYEWASH FOUNTAINS AND
Page 37 and 38: “COMMON FIRE CODE VIOLATIONS “E
Page 39 and 40: ) 4-Bromodimethylaniline HAZARDOUS
Page 41 and 42: manager and stockroom personnel usi
Page 43 and 44: Mineral acids (HCl, HNO 3 and H 2 S
Page 45 and 46: 1. “Lecture Bottles must be Mathe
Page 47 and 48: (one kilogram per month, total amou
Page 49 and 50: All other organic solvents not on t
Page 51 and 52: 2. Personal Protective Equipment: L
Page 53 and 54: 3. VENTILATION AND PROPER USE OF HO
Page 55 and 56:
3. Preliminary Considerations for S
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OPERATING INFORMATION FOR FHM 400 F
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6. Visionaire or Supreme Air hood o
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4. Chemical Storage in Research Lab
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E. Laboratory Operations which requ
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F. Provisions for Additional Protec
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G. Specific Procedures for Safe Rem
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2. Dr. Bierbach - Lab Room #107 SPE
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3. Dr. Brown - Lab Room #14 SPECIFI
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Dry soft things: Weighing paper, pa
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5. Dr. Colyer - Lab Room # 114 SPEC
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6. Dr. Hinze - Lab Room # 109 SPECI
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8. Dr. Paul Jones - Lab Room # 14 S
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10. Dr. Kondepudi - Lab Room # 5 SP
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� Ammonium hydroxide � Ammonium
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13. Dr. Swofford - Lab Room # 1 SPE
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� Hydrochloric acid � Acetic ac
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15. Dr. Welker - Lab Room # 13 SPEC
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H. Specific Decontamination Procedu
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egenerated with additional No-chrom
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2. Dr. Bierbach - Lab Room # 107 Sp
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4. Dr. Buchmueller - Lab Room # 1 S
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6. Dr. Hinze - Lab Room # 109 Speci
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8. Dr. Paul Jones - Lab Room # 14 S
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10. Dr. Kondepudi - Lab Room # 5 Sp
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12. Dr. Noftle - Lab Room # 117 Spe
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14. Dr. Tobey - Lab Room # 2 For ro
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16. Undergraduate Lab Rooms # 7, 10
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1. Laboratory Inspection Form WFU C
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2. Chemical Fire and Large Building
Page 115 and 116:
Research hoods are great places to
Page 117 and 118:
K. Provisions for medical exams, co
Page 119 and 120:
If and when air-monitoring in your
Page 121 and 122:
5. Worker’s Compensation Procedur
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L. Standard Operating Procedures (S
Page 125 and 126:
2. Summary of Regulated Chemicals C
Page 127 and 128:
4. SOPs for all laboratories of Sal
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Compressed Gas Cylinders Gas cylind
Page 131 and 132:
Summary of Liquid N2 Instructions 1
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cylinder valve, inlet fitting, high
Page 135 and 136:
Laboratory Operations Involving Red
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Use of the Hydraulic Press (prepare
Page 139 and 140:
At the present time, test strips fo
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The oxidation potential of sodium i
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Standard Operating procedure for us
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OVERNIGHT REACTION IN PROGRESS In c
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(NIGHTS AND WEEKENDS) provided by S
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IV. Training 149
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B. Chemical Hygiene Plan (CHP) for
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2. HMIS / NFPA Chemical Hazard Rati
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4. INTERPRETING CHEMICAL HAZARD HMI
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6. Summary of HMIS Ratings (from Na
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7. Hazard Communication Training Lo
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Laboratory Safety and Regulations,
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When these audio-visuals and discus
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The alcohols show a regular depende
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Lead, mercury, arsenic, chromium, b
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1. Certification of Safety Training
Page 171 and 172:
3. Summer School Safety Training An
Page 173 and 174:
V. Chemistry Department Purchase Or
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faculty members personal "Professor
Page 177 and 178:
Vendor’s List for Wake Forest Uni
Page 179 and 180:
KODAK LABORATORY CHEMICALS BUY FR F
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MISCELLANEOUS INFORMATION Acros is
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VII. Alcohol Dispensing Procedure P
Page 185 and 186:
B. Instructions for the Use of the
Page 187 and 188:
C. General Information for Users (W
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