Guidelines for care & Use of Dry Solvent Stills [Example]

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12. Dr. Noftle – Lab Room # 118 SPECIFIC PROCEDURES FOR SAFE REMOVAL OF HIGHLY TOXIC WASTE Consult with your research advisor concerning proper methods for packaging and storing extremely hazardous waste. Research usually involves working with selective types or classes of chemicals. Prepare brief summaries in this section for handling spent chemicals peculiar to your lab. The following common laboratory organic solvents can be collected in a waste container, labeled NON- SULFUR, NON-HALOGENATED ORGANIC SOLVENTS and be poured into one of the two 55 gallon waste drums located in the solvent room, #20, assuming they are not overly contaminated with acids or large amounts of toxic or odoriferous sulfur compounds. Each chemical should be recorded by name and amount. acetone methyl ethyl ketone pump oil benzaldehyde mineral spirits tetrahydrofuran benzene motor oil toluene cyclohexane naphtha xylenes ethyl ether paint thinner ethyl alcohol, (and, ethyl acetate petroleum ether low-molecular weight alcohols, The methylene chloride and chloroform must be collected in a well-labeled waste bottle and can be poured into labeled 20 liter empty white polyethylene containers kept next to the large 55 gallon steel drum on the floor in the wide yellow spill tray in the solvent room, #20. Sulfur containing compounds, complex heterocyclics, corrosives, organic acids, lachrymators, etc. (i.e. thiophene, pyrrole, acetonitrile, etc.) should be collected into well-labeled waste bottles and taken to the metal surface in the solvent room, #20. Consolidate compatible inorganic solids in a well-labeled waste container, organic solids in another. These can be placed on the metal surface table in the solvent room #20. Non-compatible solids should naturally be packaged separately. Typical waste streams originating from Dr. Noftle’s research lab are as follows: Organic Solvents (Non-Halogenated) Ethyl Acetate, Hexanes, Acetone Diethyl Ether, Methanol, Ethanol Tetrahydrofuran, Toluene, Pentane Cyclohexane, Benzene, Acetonitrile, and occasionally Nitrobenzene Halogenated Solvents Methylene chloride, chloroform Acetone, with: tetrabutylammonium perchlorate tetrabutylammonium hexafluorophosphate tetrabutylammonium trifluoromethanesulfonate copper(II) perchlorate hexahydrate copper(II) trifluoromethanesulfonate copper(II) acetate monohydrate copper(II) chloride zinc(II) perchlorate hexahydrate zinc(II) trifluoromethanesulfonate N2-(2-pyridylmethyl)-3-thienyl carboxamide N2-(2-pyridylmethyl)-3-thenyl carboxamide N2-(2-pyridylmethyl)-5-(3-thienyl)-butyl carboxamide N2-(2-pyridylmethyl)-trans-3-(3-thienyl) acrylamide 84
13. Dr. Swofford – Lab Room # 1 SPECIFIC PROCEDURES FOR SAFE REMOVAL OF HIGHLY TOXIC WASTE Consult with your research advisor concerning proper methods for packaging and storing extremely hazardous waste. Research usually involves working with selective types or classes of chemicals. Prepare brief summaries in this section for handling spent chemicals peculiar to your lab. Practically no highly toxic waste is generated in this lab. Only benign organic dyes and other small amounts of analytical samples (for example, polyaromatic hydrocarbons). Typical bottles of chemical waste (usually one or three one gallon jars collected over a period of 6 to 12 months) contain the following: methanol, ethanol, ethylene glycol, acetone, heptane, benzene, hexane, toluene, octane, and dyes, such as Rhodamine 590 and 61 and Keton red dye. 85
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Wake Forest University Chemistry De
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11. Dr. Lachgar - Lab Room # 6 ....
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I. INTRODUCTION A hardcopy of this
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II. Telephone #s of Emergency Perso
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B. Emergency Exit Plan for All Sale
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A. Emergency Telephone Numbers of L
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2. Dr. Bierbach - Lab Room #107 Lab
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4. Dr. Buchmueller - Lab Room #1 La
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6. Dr. Hinze - Lab Room #109 Lab Pe
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8. Dr. Paul Jones - Lab Room #113 L
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10. Dr. Kondepudi - Lab Room #5 Lab
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12. Dr. Noftle - Lab Room #117 Lab
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14. Dr. Tobey - Room # 2 Lab Person
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16. Undergraduate - Lab Room #s 7,
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11. Do not force glass tubing into
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2. Cleanliness in the Research Labo
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Page 35 and 36: INVENTORY OF EYEWASH FOUNTAINS AND
Page 37 and 38: “COMMON FIRE CODE VIOLATIONS “E
Page 39 and 40: ) 4-Bromodimethylaniline HAZARDOUS
Page 41 and 42: manager and stockroom personnel usi
Page 43 and 44: Mineral acids (HCl, HNO 3 and H 2 S
Page 45 and 46: 1. “Lecture Bottles must be Mathe
Page 47 and 48: (one kilogram per month, total amou
Page 49 and 50: All other organic solvents not on t
Page 51 and 52: 2. Personal Protective Equipment: L
Page 53 and 54: 3. VENTILATION AND PROPER USE OF HO
Page 55 and 56: 3. Preliminary Considerations for S
Page 57 and 58: OPERATING INFORMATION FOR FHM 400 F
Page 59 and 60: 6. Visionaire or Supreme Air hood o
Page 61 and 62: 4. Chemical Storage in Research Lab
Page 63 and 64: E. Laboratory Operations which requ
Page 65 and 66: F. Provisions for Additional Protec
Page 67 and 68: G. Specific Procedures for Safe Rem
Page 69 and 70: 2. Dr. Bierbach - Lab Room #107 SPE
Page 71 and 72: 3. Dr. Brown - Lab Room #14 SPECIFI
Page 73 and 74: Dry soft things: Weighing paper, pa
Page 75 and 76: 5. Dr. Colyer - Lab Room # 114 SPEC
Page 77 and 78: 6. Dr. Hinze - Lab Room # 109 SPECI
Page 79 and 80: 8. Dr. Paul Jones - Lab Room # 14 S
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Page 89 and 90: 15. Dr. Welker - Lab Room # 13 SPEC
Page 91 and 92: H. Specific Decontamination Procedu
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Page 97 and 98: 4. Dr. Buchmueller - Lab Room # 1 S
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Page 101 and 102: 8. Dr. Paul Jones - Lab Room # 14 S
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Page 105 and 106: 12. Dr. Noftle - Lab Room # 117 Spe
Page 107 and 108: 14. Dr. Tobey - Lab Room # 2 For ro
Page 109 and 110: 16. Undergraduate Lab Rooms # 7, 10
Page 111 and 112: 1. Laboratory Inspection Form WFU C
Page 113 and 114: 2. Chemical Fire and Large Building
Page 115 and 116: Research hoods are great places to
Page 117 and 118: K. Provisions for medical exams, co
Page 119 and 120: If and when air-monitoring in your
Page 121 and 122: 5. Worker’s Compensation Procedur
Page 123 and 124: L. Standard Operating Procedures (S
Page 125 and 126: 2. Summary of Regulated Chemicals C
Page 127 and 128: 4. SOPs for all laboratories of Sal
Page 129 and 130: Compressed Gas Cylinders Gas cylind
Page 131 and 132: Summary of Liquid N2 Instructions 1
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Laboratory Operations Involving Red
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Use of the Hydraulic Press (prepare
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At the present time, test strips fo
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The oxidation potential of sodium i
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Standard Operating procedure for us
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OVERNIGHT REACTION IN PROGRESS In c
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(NIGHTS AND WEEKENDS) provided by S
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IV. Training 149
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B. Chemical Hygiene Plan (CHP) for
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2. HMIS / NFPA Chemical Hazard Rati
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4. INTERPRETING CHEMICAL HAZARD HMI
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6. Summary of HMIS Ratings (from Na
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7. Hazard Communication Training Lo
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Laboratory Safety and Regulations,
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When these audio-visuals and discus
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The alcohols show a regular depende
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Lead, mercury, arsenic, chromium, b
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1. Certification of Safety Training
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3. Summer School Safety Training An
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V. Chemistry Department Purchase Or
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faculty members personal "Professor
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Vendor’s List for Wake Forest Uni
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KODAK LABORATORY CHEMICALS BUY FR F
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MISCELLANEOUS INFORMATION Acros is
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VII. Alcohol Dispensing Procedure P
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B. Instructions for the Use of the
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C. General Information for Users (W
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Guidelines for care & Use of Dry Solvent Stills [Example]

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