Guidelines for care & Use of Dry Solvent Stills [Example]

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11. Dr. Lachgar – Lab Room # 6 SPECIFIC PROCEDURES FOR SAFE REMOVAL OF HIGHLY TOXIC WASTE Consult with your research advisor concerning proper methods for packaging and storing extremely hazardous waste. Research usually involves working with selective types or classes of chemicals. Prepare brief summaries in this section for handling spent chemicals peculiar to your lab. Solid wastes are to be collected into labeled waste bottles and then transferred to waste storage areas. The liquids used are usually aqueous acid and base solutions. They are to be disposed after being neutralized. Aqueous solutions(usually acidic) of inorganic saltsare kept in typical glass waste jars, labeled with all components, and taken to the waste storage area in room # 20. Typical waste streams generated in this lab are as follows: 1) Water, methanol, acetonitrile and ethanol (acidic) with: � Niobium chloride � Potassium cyanide � Silver nitrate � Copper chloride � Ethylenediamine � Vanadium acetylacetonate � salicylaldehyde � Tetramethylammonium chloride � Manganese acetate 2) Water and ethanol (acidic) with: � Niobium chloride � Potassium cyanide � Cadmium chloride � Iron chloride � Tetramethylammonium chloride � Sodium chloride � Potassium chloride 3) Hydrochloric acid (dilute) with: � Niobium chloride, trace amount � Tantalum chloride, trace amount 4) Two jars of Water (acidic) with: � Hydrochloric acid � Nitric acid � Niobium chloride (trace amounts) � Tantalum chloride (trace amounts) 5) One container of: � Acetone � Water � Dimethyl formamide � Iron cyanide � 4,4’-Dipyridyl � Methylammonium chloride 82
� Ammonium hydroxide � Ammonium nitrate � Iron(III) chloride � Ethylenediamine � Acetonitrile � Ethanol � Niobium chloride � Salicylaldehyde 83
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Wake Forest University Chemistry De
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11. Dr. Lachgar - Lab Room # 6 ....
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I. INTRODUCTION A hardcopy of this
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II. Telephone #s of Emergency Perso
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B. Emergency Exit Plan for All Sale
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A. Emergency Telephone Numbers of L
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2. Dr. Bierbach - Lab Room #107 Lab
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4. Dr. Buchmueller - Lab Room #1 La
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6. Dr. Hinze - Lab Room #109 Lab Pe
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8. Dr. Paul Jones - Lab Room #113 L
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10. Dr. Kondepudi - Lab Room #5 Lab
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12. Dr. Noftle - Lab Room #117 Lab
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14. Dr. Tobey - Room # 2 Lab Person
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16. Undergraduate - Lab Room #s 7,
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11. Do not force glass tubing into
Page 31 and 32: 2. Cleanliness in the Research Labo
Page 33 and 34: 3. Housekeeping for All Labs Housek
Page 35 and 36: INVENTORY OF EYEWASH FOUNTAINS AND
Page 37 and 38: “COMMON FIRE CODE VIOLATIONS “E
Page 39 and 40: ) 4-Bromodimethylaniline HAZARDOUS
Page 41 and 42: manager and stockroom personnel usi
Page 43 and 44: Mineral acids (HCl, HNO 3 and H 2 S
Page 45 and 46: 1. “Lecture Bottles must be Mathe
Page 47 and 48: (one kilogram per month, total amou
Page 49 and 50: All other organic solvents not on t
Page 51 and 52: 2. Personal Protective Equipment: L
Page 53 and 54: 3. VENTILATION AND PROPER USE OF HO
Page 55 and 56: 3. Preliminary Considerations for S
Page 57 and 58: OPERATING INFORMATION FOR FHM 400 F
Page 59 and 60: 6. Visionaire or Supreme Air hood o
Page 61 and 62: 4. Chemical Storage in Research Lab
Page 63 and 64: E. Laboratory Operations which requ
Page 65 and 66: F. Provisions for Additional Protec
Page 67 and 68: G. Specific Procedures for Safe Rem
Page 69 and 70: 2. Dr. Bierbach - Lab Room #107 SPE
Page 71 and 72: 3. Dr. Brown - Lab Room #14 SPECIFI
Page 73 and 74: Dry soft things: Weighing paper, pa
Page 75 and 76: 5. Dr. Colyer - Lab Room # 114 SPEC
Page 77 and 78: 6. Dr. Hinze - Lab Room # 109 SPECI
Page 79 and 80: 8. Dr. Paul Jones - Lab Room # 14 S
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Page 85 and 86: 13. Dr. Swofford - Lab Room # 1 SPE
Page 87 and 88: � Hydrochloric acid � Acetic ac
Page 89 and 90: 15. Dr. Welker - Lab Room # 13 SPEC
Page 91 and 92: H. Specific Decontamination Procedu
Page 93 and 94: egenerated with additional No-chrom
Page 95 and 96: 2. Dr. Bierbach - Lab Room # 107 Sp
Page 97 and 98: 4. Dr. Buchmueller - Lab Room # 1 S
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Page 101 and 102: 8. Dr. Paul Jones - Lab Room # 14 S
Page 103 and 104: 10. Dr. Kondepudi - Lab Room # 5 Sp
Page 105 and 106: 12. Dr. Noftle - Lab Room # 117 Spe
Page 107 and 108: 14. Dr. Tobey - Lab Room # 2 For ro
Page 109 and 110: 16. Undergraduate Lab Rooms # 7, 10
Page 111 and 112: 1. Laboratory Inspection Form WFU C
Page 113 and 114: 2. Chemical Fire and Large Building
Page 115 and 116: Research hoods are great places to
Page 117 and 118: K. Provisions for medical exams, co
Page 119 and 120: If and when air-monitoring in your
Page 121 and 122: 5. Worker’s Compensation Procedur
Page 123 and 124: L. Standard Operating Procedures (S
Page 125 and 126: 2. Summary of Regulated Chemicals C
Page 127 and 128: 4. SOPs for all laboratories of Sal
Page 129 and 130: Compressed Gas Cylinders Gas cylind
Page 131 and 132: Summary of Liquid N2 Instructions 1
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cylinder valve, inlet fitting, high
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Laboratory Operations Involving Red
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Use of the Hydraulic Press (prepare
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At the present time, test strips fo
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The oxidation potential of sodium i
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Standard Operating procedure for us
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OVERNIGHT REACTION IN PROGRESS In c
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(NIGHTS AND WEEKENDS) provided by S
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IV. Training 149
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B. Chemical Hygiene Plan (CHP) for
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2. HMIS / NFPA Chemical Hazard Rati
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4. INTERPRETING CHEMICAL HAZARD HMI
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6. Summary of HMIS Ratings (from Na
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7. Hazard Communication Training Lo
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Laboratory Safety and Regulations,
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When these audio-visuals and discus
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The alcohols show a regular depende
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Lead, mercury, arsenic, chromium, b
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1. Certification of Safety Training
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3. Summer School Safety Training An
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V. Chemistry Department Purchase Or
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faculty members personal "Professor
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Vendor’s List for Wake Forest Uni
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KODAK LABORATORY CHEMICALS BUY FR F
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MISCELLANEOUS INFORMATION Acros is
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VII. Alcohol Dispensing Procedure P
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B. Instructions for the Use of the
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C. General Information for Users (W
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