Guidelines for care & Use of Dry Solvent Stills [Example]

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WEEKLY CHECK LIST (DAYTIME HOURS) provided by Dr. Susan Jackels To be completed by last person to leave the laboratory each night (weekdays only). Put your initials in the appropriate space and add to notebook for record-keeping at the end of the week. You may also wish to add a few items of your own, like balances off, lights out, oven doors closed and computers off (especially if located next to a water faucet. Week of: Monday Tuesday Wednesday Thursday Friday Water faucets Off ? Stirrer/Hot Plate Distillation Apparatus Water Pumps Hood Sashes Rotary Evaporator Vacuum Pumps Gas/Air Jets Off ? Heat and water off ? Off ? Closed ? Water off ? Off ? Closed ? 146
(NIGHTS AND WEEKENDS) provided by Susan Jackels Indicate the general purpose of your lab entry in comments section (study, monitor overnight reaction, lab cleanup, use NMR, GC, etc.). Indicate general state of lab in Misc. section (OK or list specific safety problems, instrument failures, difficulties with service facilities, etc. Date/Initials Time In Time Out Comments Misc. (ok?) 147
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Wake Forest University Chemistry De
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11. Dr. Lachgar - Lab Room # 6 ....
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I. INTRODUCTION A hardcopy of this
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II. Telephone #s of Emergency Perso
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B. Emergency Exit Plan for All Sale
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A. Emergency Telephone Numbers of L
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2. Dr. Bierbach - Lab Room #107 Lab
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4. Dr. Buchmueller - Lab Room #1 La
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6. Dr. Hinze - Lab Room #109 Lab Pe
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8. Dr. Paul Jones - Lab Room #113 L
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10. Dr. Kondepudi - Lab Room #5 Lab
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12. Dr. Noftle - Lab Room #117 Lab
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14. Dr. Tobey - Room # 2 Lab Person
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16. Undergraduate - Lab Room #s 7,
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11. Do not force glass tubing into
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2. Cleanliness in the Research Labo
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3. Housekeeping for All Labs Housek
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INVENTORY OF EYEWASH FOUNTAINS AND
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“COMMON FIRE CODE VIOLATIONS “E
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) 4-Bromodimethylaniline HAZARDOUS
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manager and stockroom personnel usi
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Mineral acids (HCl, HNO 3 and H 2 S
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1. “Lecture Bottles must be Mathe
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(one kilogram per month, total amou
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All other organic solvents not on t
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2. Personal Protective Equipment: L
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3. VENTILATION AND PROPER USE OF HO
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3. Preliminary Considerations for S
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OPERATING INFORMATION FOR FHM 400 F
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6. Visionaire or Supreme Air hood o
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4. Chemical Storage in Research Lab
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E. Laboratory Operations which requ
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F. Provisions for Additional Protec
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G. Specific Procedures for Safe Rem
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2. Dr. Bierbach - Lab Room #107 SPE
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3. Dr. Brown - Lab Room #14 SPECIFI
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Dry soft things: Weighing paper, pa
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5. Dr. Colyer - Lab Room # 114 SPEC
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6. Dr. Hinze - Lab Room # 109 SPECI
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8. Dr. Paul Jones - Lab Room # 14 S
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10. Dr. Kondepudi - Lab Room # 5 SP
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� Ammonium hydroxide � Ammonium
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13. Dr. Swofford - Lab Room # 1 SPE
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� Hydrochloric acid � Acetic ac
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15. Dr. Welker - Lab Room # 13 SPEC
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H. Specific Decontamination Procedu
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egenerated with additional No-chrom
Page 95 and 96: 2. Dr. Bierbach - Lab Room # 107 Sp
Page 97 and 98: 4. Dr. Buchmueller - Lab Room # 1 S
Page 99 and 100: 6. Dr. Hinze - Lab Room # 109 Speci
Page 101 and 102: 8. Dr. Paul Jones - Lab Room # 14 S
Page 103 and 104: 10. Dr. Kondepudi - Lab Room # 5 Sp
Page 105 and 106: 12. Dr. Noftle - Lab Room # 117 Spe
Page 107 and 108: 14. Dr. Tobey - Lab Room # 2 For ro
Page 109 and 110: 16. Undergraduate Lab Rooms # 7, 10
Page 111 and 112: 1. Laboratory Inspection Form WFU C
Page 113 and 114: 2. Chemical Fire and Large Building
Page 115 and 116: Research hoods are great places to
Page 117 and 118: K. Provisions for medical exams, co
Page 119 and 120: If and when air-monitoring in your
Page 121 and 122: 5. Worker’s Compensation Procedur
Page 123 and 124: L. Standard Operating Procedures (S
Page 125 and 126: 2. Summary of Regulated Chemicals C
Page 127 and 128: 4. SOPs for all laboratories of Sal
Page 129 and 130: Compressed Gas Cylinders Gas cylind
Page 131 and 132: Summary of Liquid N2 Instructions 1
Page 133 and 134: cylinder valve, inlet fitting, high
Page 135 and 136: Laboratory Operations Involving Red
Page 137 and 138: Use of the Hydraulic Press (prepare
Page 139 and 140: At the present time, test strips fo
Page 141 and 142: The oxidation potential of sodium i
Page 143 and 144: Standard Operating procedure for us
Page 145: OVERNIGHT REACTION IN PROGRESS In c
Page 149 and 150: IV. Training 149
Page 151 and 152: B. Chemical Hygiene Plan (CHP) for
Page 153 and 154: 2. HMIS / NFPA Chemical Hazard Rati
Page 155 and 156: 4. INTERPRETING CHEMICAL HAZARD HMI
Page 157 and 158: 6. Summary of HMIS Ratings (from Na
Page 159 and 160: 7. Hazard Communication Training Lo
Page 161 and 162: Laboratory Safety and Regulations,
Page 163 and 164: When these audio-visuals and discus
Page 165 and 166: The alcohols show a regular depende
Page 167 and 168: Lead, mercury, arsenic, chromium, b
Page 169 and 170: 1. Certification of Safety Training
Page 171 and 172: 3. Summer School Safety Training An
Page 173 and 174: V. Chemistry Department Purchase Or
Page 175 and 176: faculty members personal "Professor
Page 177 and 178: Vendor’s List for Wake Forest Uni
Page 179 and 180: KODAK LABORATORY CHEMICALS BUY FR F
Page 181 and 182: MISCELLANEOUS INFORMATION Acros is
Page 183 and 184: VII. Alcohol Dispensing Procedure P
Page 185 and 186: B. Instructions for the Use of the
Page 187 and 188: C. General Information for Users (W
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Guidelines for care & Use of Dry Solvent Stills [Example]

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