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Site-Specific Health and Safety Plan (HASP) - Laschools.org

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Table 8-1 Flagging Conventions for Data Evaluation <strong>and</strong> Validation of Organic Methods<br />

LAUSD, South Gate, California<br />

Quality Control Check Evaluation Flag Samples Affected<br />

Calibration Verification If %D is >2X control criteria R all positive results <strong>and</strong> non-detects Compound in all associated samples<br />

(CCAL) (Continued)<br />

in analysis batch<br />

RRF 0.990<br />

Correlation coefficient of curve < 0.990<br />

J positive results<br />

UJ non-detects<br />

R all positive <strong>and</strong> non-detects<br />

Compound in all associated samples<br />

in analysis batch<br />

%D >15%<br />

J positive results<br />

UJ non-detects<br />

Compound in all associated samples<br />

in analysis batch<br />

If %D is > 2X control criteria R all positive results <strong>and</strong> non-detects Compound in all associated samples<br />

in analysis batch<br />

Laboratory Control Sample LCS or LCSD single compound:<br />

(LCS) <strong>and</strong> Laboratory Control %R UCL<br />

associated samples.<br />

i/ but < 150%. J positive results<br />

Spiked compound only in all<br />

% R > 30% but < LCL<br />

No qualification for non-detects associated samples.<br />

j/ J positive results<br />

Spiked compound only in all<br />

UJ non-detects<br />

associated samples.<br />

% R >UCL <strong>and</strong> >150% R all positive results good/non-detects Spiked compound only in all<br />

associated samples.<br />

If > 50% of all LCS or LCSD spiked<br />

compounds are out of control:<br />

RPD k/ R all positive results <strong>and</strong> non-detects All detected spike compounds in all<br />

>control limit<br />

J positive results<br />

samples<br />

All detected spike compounds in all<br />

samples<br />

Method Blank Multiply value by 5, common lab<br />

contaminants multiply by 10 l/<br />

U flag reported results < calculated<br />

value<br />

All samples in extraction batch<br />

Equipment Blank Convert to soil units, if applicable, multiply<br />

by 5, common lab contaminants multiply by<br />

10 b/<br />

U flag reported results < calculated All samples, same field team, matrix<br />

value<br />

<strong>and</strong> date (water) or all samples, same<br />

field team, matrix (soil)<br />

Trip Blank Convert to soil units, if applicable, multiply<br />

by 5, common lab contaminants multiply by<br />

10 b/<br />

U flag reported results < calculated All volatile samples shipped in the<br />

value<br />

same cooler<br />

K:\Depts\Dept48\LAUSD\MSA WORK\Soil Investigation\OU 1 RAP\Appendix\Appendix H - QAPP\Tables.doc 5/7/2008<br />

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