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HMX 3.2 Molecular Weight. 296.17 3.3 Solubility. Grams Dissolved/100 g of Solvent Solvent 20°C 40°C 60” C Acetic acid Glacial 70% Acetic anhydride Acetone Anhydrous 70% Acetonitrile Cyclohexanone Dimethylformamide Dimethylsulfoxide 4. PHYSICAL PROPERTIES 0.037 0.044 0.090 -__ 0.033 0.103 -_- 1.29 1.94 2.4 3.4 ___ 0.66 1.20 --_ __- 3.07 4.34 __- 5.91 7.17 __- 6.1 11.1 _-- 45.5 47.2 4.1 Crystal Structure.4-6 The cell parameters of the four polymorphic forms of HMX are given. 44 Cell Parameters Unit cell edge length (A) Angle p ; C Molecules per unit cell a 23.89 15.14 5.91 --- 8 P Y 6 11.05 6.54 10.95 7.93 7.66 ___ 7.37 14.61 32.49 102.8” 119.4” ___ 2 4 6
4.2 Density.’ Method of Determination State a Density (g/cm”) P - Y 6 __ X-ray Solid 1.838 1.902 1.78 1.786 Direct measurement Solid 1.84 1.905 1.76 1.80 HMX HMX cannot be consolidated into charges by conventional pressing. Obtaining large pieces of polycrystalline HMX requires solvent pressing techniques. 4.3 Infrared Spectrum. See Fig. 1. 4.4 Refractive Index.’ The refractive indices of the four polymorphs in sodium light are shown. Face a B HMX Polymorph Alpha 1.561-1.565 1.589 Beta 1.562-1.566 1.594-1.595 Gamma 1.720-1.740 1.730-1.773 Epsilon Omega Double refraction 2.5 __- ___ Pas WAVELI ENGTH 6 li 16OC I (pm) WAVE NUMBER (I/cm 1 6 ___ ___ Pas 14 Y 6 1.537 _-_ 1.585 _-_ 1.666 __- ___ 1.566 _-_ 1.607 Pas neg Fig. 1. Infrared spectrum. 45
Page 2 and 3: LOS ALAMOS SERIES ON DYNAMIC MATERI
Page 4 and 5: University of California Press Berk
Page 6 and 7: PART II. EXPLOSIVES PROPERTIES BY P
Page 8 and 9: treats pure explosives first, alpha
Page 10 and 11: EXPLOSIVES PROPERTIES BY EXPLOSIVE
Page 12 and 13: BARATOL 2.3 Shipping.2 Baratol is s
Page 14 and 15: BARATOL 6 5.4 Thermal Conductivity.
Page 16 and 17: BARATOL 6.2 Detonation Pressure. We
Page 18 and 19: BARATOL REFERENCES . . 1. N. I. Sax
Page 20 and 21: COMP B slowly. Heating and stirring
Page 22 and 23: COMP B 14 3.3 Solubility.‘The sol
Page 24 and 25: COMP B 16 5.3 Heat Capacity. Heat C
Page 26 and 27: COMP B 18 6.2 Detonation Pressure.
Page 28 and 29: COMP B 7.3 Shock Hugoniots.12J8 Com
Page 30 and 31: COMP B 9. MECHANICAL PROPERTIES 22
Page 32 and 33: CYCLOTOL 1. GENERAL PROPERTIES 1.1
Page 34 and 35: CYCLOTOL 26 3.2 Molecular Weight. C
Page 36 and 37: CYCLOTOL 4.3 Infrared Spectrum. See
Page 38 and 39: CYCLOTOL where D = detonation veloc
Page 40 and 41: CYCLOTOL 8.3 Skid Test Results. Den
Page 42 and 43: DATB 1. GENERAL PROPERTIES 1.1 Chem
Page 44 and 45: DATB 4. PHYSICAL PROPERTIES 4.1 Cry
Page 46 and 47: DATB 5.4 Thermal Conductivity, Cond
Page 48 and 49: DATB 7.3 Shock Hugoniot.9 Density k
Page 50 and 51: HMX* 1. GENERAL PROPERTIES 1.1 Chem
Page 54 and 55: HMX 5. THERMAL PROPERTIES 46 5.1 Ph
Page 56 and 57: HMX 6. DETONATION PROPERTIES 6.1 De
Page 58 and 59: HMX 7.3 Shock Hugoniots.” Density
Page 60 and 61: NITROGUANIDINE 1. GENERAL PROPERTIE
Page 62 and 63: NQ 54 4.2 Density.’ Crystal Metho
Page 64 and 65: NQ 56 5.6 Heats of Combustion and F
Page 66 and 67: NQ 6.2 Detonation Pressure. There a
Page 68 and 69: NQ 8. SENSITIVITY 8.1 Drop Weight I
Page 70 and 71: OCTOL These are shipped to an ordna
Page 72 and 73: 64 OCTOL 3.3 Solubility.6 The solub
Page 74 and 75: OCTOL 5. THERMAL PROPERTIES 66 5.1
Page 76 and 77: OCTOL 68 6.4 Plate Dent Test Result
Page 78 and 79: OCTOL 8.3 Skid Test Results. Weight
Page 80 and 81: PBX 9011 1. GENERAL PROPERTIES 1.1
Page 82 and 83: PBX 9011 3.3 Solubility. The solubi
Page 84 and 85: PBX 9011 76 5.5 Coefficient of Ther
Page 86 and 87: PBX 9011 78 6.3 Cylinder Test Resul
Page 88 and 89: PBX 9011 7.5 Detonation Failure Thi
Page 90 and 91: PBX 9011 82 9.3 Compressive Strengt
Page 92 and 93: PBX9404 1. GENERAL PROPERTIES 1.1 C
Page 94 and 95: PBX 9404 86 3.2 Molecular Weight. C
Page 96 and 97: PBX 9404 88 4.3 Infrared Spectrum.
Page 98 and 99: PBX 9404 > 1 1 o- r 0 I I I, / PYRO
Page 100 and 101: PBX 9404 7. SHOCK INITIATION PROPER
Page 102 and 103:
PBX 9404 7.5 Detonation Failure Thi
Page 104 and 105:
PBX 9404 8.5 Spark Sensitivity. Ele
Page 106 and 107:
PBX 9404 REFERENCE‘S 1. Committee
Page 108 and 109:
PBX 9407 2.3 Shipping.2 PBX-9407 mo
Page 110 and 111:
PBX 9407 4.3 Infrared Spectrum. See
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PBX 9407 6. DETONATION PROPERTIES I
Page 114 and 115:
PBX 9407 106 7.2 Wedge Test Results
Page 116 and 117:
PBX 9407 9.3 Compressive Strength a
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PBX 9501 2.3 Shipping.* PBX-9501mol
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PBX 9501 5. THERMAL PROPERTIES 112
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PBX 9501 6. DETONATION PROPERTIES 6
Page 124 and 125:
PBX 9501 7.3 Shock Hugoniot. Densit
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PBX 9501 9. MECHANICAL PROPERTIES*
Page 128 and 129:
PBX9502 1. GENERAL PROPERTIES 1.1 C
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PBX 9502 3.3 Solubility. The solubi
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PBX 9502 124 5.3 Heat Capacity. 5.4
Page 134 and 135:
PBX 9502 6.3 Cylinder Test Results.
Page 136 and 137:
PBX 9502 9. MECHANICAL PROPERTIES 1
Page 138 and 139:
PENTAERYTHRITOLTETRANITRATE (PETN)
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PETN 3.2 Molecular Weight. 316.15 3
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PETN 4.4 Refractive Indices.s Omega
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PETN 5.7 Thermal Decomposition Kine
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PETN 138 7.2 Wedge Test Results. De
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, PETN 5. US Army Materiel Command,
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RDX developed into a continuous hig
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RDX 4. PHYSICAL PROPERTIES 4.1 Crys
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RDX 146 5.2 Vapor Pressure.8 Temper
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RDX 6. DETONATION PROPERTIES 148 6.
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RDX 7.3 Shock Hugoniot.” 8. SENSI
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TATB 1. GENERAL PROPERTIES 1.1 Chem
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TATB TATB solubility in sulfuric ac
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TATB 5.2 Vapor Pressure.6 A least s
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TATB I / / I I I I I I I ! \ I 1 \
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TATB 7.3 Shock Hugoniots.“+ A num
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TATB REFERENCES 1. T. M Benziger an
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TETRYL acetone. In the second proce
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TETRYL 2.5 100 80 60 % T 40 20 0 :;
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TETRYL 6. DETONATION PROPERTIES 6.1
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TETRYL 7.5 Detonation Failure Thick
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TNT 1. GENERAL PROPERTIES 1.1 Chemi
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TNT 4. PHYSICAL PROPERTIES 4.1 Crys
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TNT 4.3 Infrared Spectrum. See Fig.
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TNT 178 5.5 Coefficient of Thermal
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TNT The charge preparation method a
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TNT 182 6.4 Plate Dent Test Results
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TNT 7.3 Shock Hugoniots.2aJ4 Densit
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TNT 9.3 Compressive Strength and Mo
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XTX8003 1. GENERAL PROPERTIES 1.1 C
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XTX 8003 3.3 Solubility.6 The solub
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XTX 8003 5.7 Thermal Decomposition
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XTX 8003 8. SENSITIVITY 8.1 Drop We
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XTX8004 1. GENERAL PROPERTIES 1.1 C
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XTX 8004 3.3 Solubility. The solubi
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XTX 8004 6. DETONATION PROPERTIES 6
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PART II EXPLOSIVES PROPERTIES BY IP
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Explosive Alex/20 Alex/30 Amatex/20
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Explosive PBX 9007 PBX 9010 PBX 901
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Explosive Constituents X-0234-60 X-
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Alex/20 Alex/30 Amatexl20 Amatexl30
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NQ octo1 PAT0 Explosive PBX 9007 PB
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X-0234-60 X-0234-70 X-0234-80 X-028
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THERMAL PROPERTIES 2. THERMAL PROPE
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THERMAL PROPERTIES k2 = kl - (4, -
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Explosive PETN RDX TNT Table 2.03 C
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THERMAL PROPERTIES AEE = standard i
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THERMAL PROPERTIES Fig. 2.02. Pyrol
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,’ THERMAL PROPERTIES L Y !s :: B
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THERMAL PROPERTIES 228 Composition
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THERMAL PROPERTIES B Y !3 E E “I
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THERMAL PROPERTIES This assembly is
Page 242 and 243:
DETONATION PROPERTIES 3. DETONATION
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DETONATION PROPERTIES 236 Table 3.0
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Shot No. c-4394 E-4672 E-4067 E-406
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DETONATION PROPERTIES Table 3.06 CY
Page 250 and 251:
Table 3.08 OCTOL DETONATION VELOCIT
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Rate Stick Shot ’ Diameter No. (m
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DETONATION PROPERTIES 246 Table 3.1
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Shot No. C-4436 E-3621 - Rate Stick
Page 258 and 259:
Table 3.15 GENERAL CYLINDER TEST SH
Page 260 and 261:
DETONATION PROPERTIES 252 Expansion
Page 262 and 263:
Expansion Radius (mm) Table 3.19 X-
Page 264 and 265:
N VI UY Table 3.21 X-0285 WALL VELO
Page 266 and 267:
DETONATION PROPERTIES Table 3.25 X-
Page 268 and 269:
Explosive Table 3.26 DETONATION (C-
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DETONATION PROPERTIES Analysis Line
Page 272 and 273:
DETONATION PROPERTIES Explosive Tab
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Page 276 and 277:
Page 278 and 279:
Page 280 and 281:
Page 282 and 283:
Page 284 and 285:
Page 286 and 287:
Page 288 and 289:
DETONATION PROPERTIES 3.4 Plate Den
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Exnlosive Table 3.46 (continued) De
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Explosive PBX 9501 x-0007 86 HMX/14
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85 RDX/lS Kel-F Explosive 88 RDXI12
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DETONATION PROPERTIES Table 3.47 LE
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DETONATION PROPERTIES Table 3.48 DE
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SHOCK INITIATION PROPERTIES PETN Ba
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SHOCK INITIATION PROPERTIES Fig. 4.
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SHOCK INITIATION PROPERTIES each sh
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SHOCK INITIATION’PROPERTIES Table
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SHOCK INITIATION PROPERTIES 300 i;
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w R Table 4.04 NITROMETHANE Composi
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SHOCK INITIATION PROPERTIES 304 Tab
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SHOCK INITIATION PROPERTIES 306 / D
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SHOCK INITIATION PROPERTIES 308 2 0
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Table 4.06 (continued) Coordinates
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SHOCK INITIATION PROPERTIES 312 I-
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SHOCK INITIATION PROPERTIES 316 05
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Table 4.07 PETN (SINGLE CRYSTAL) Co
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Table 4.08 (continued) Shot Number
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SHOCK INITIATION PROPERTIES 324 2 u
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SHOCK INITIATION PROPERTIES Table 4
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SHOCK INITIATION PROPERTIES 334 2T
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Initial Shock Parameters Table 4.12
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SHOCK INITIATION PROPERTIES 342 Ini
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3 *a i 8 3 x j > f m e c u,, = (2.3
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SHOCK INITIATION PROPERTIES 348 Dis
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w ul 0 Composition 95 wt% DATB, 5 w
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SHOCK INITIATION PROPERTIES 5.5- 5.
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5 Table 4.17 (continued) Coordinate
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SHOCK INITIATION PROPERTIES 40- 20
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Shot E-3120 3.370 $0.022 E-3131 2.4
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_. Shot Number E-771 E-781 B-4481 B
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SHOCK INITIATION PROPERTIES 364 2 I
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SHOCK INITIATION PROPERTIES 366 0.6
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SHOCK INITIATION PROPERTIES Composi
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Table 4.21 X-0219-50-14-10 Composit
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Composition 95 wt% NQ, 5 wt% Estane
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Shot Number (G?a) E-3245 16.2 5.904
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SHOCK INITIATION PROPERTIES 380 c x
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w R Table 4.24 (continued) Reduced
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Table 4.25 XTX-8003 (EXTEX) Composi
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SHOCK INITIATION PROPERTIES 386 a--
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Table 4.27 PBX 9407 Compositon 94 w
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SHOCK INITIATION PROPERTIES 390 3 g
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Table 4.28 PBX 9405 Cotiposition 93
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SHOCK INITIATION PROPERTIES 394 c 5
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% OY Table 4.30 x-0250-40-19 Compos
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SHOCK INITIATION PROPERTIES 398 Dis
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Table 4.32 95 TATB/2.5 Kel-F 800/2.
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Table 4.39 (continued) Coordinates
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z Table 4.44 FKM CLASS VII PROPELLA
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Theoretical Maximum Density >1.910
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Ammonium picrate Raratol(76/24) mix
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HMX-Based PBX 9011 PBX 9404 PBX-950
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SHOCK INITIATION PROPERTIES 0.360 c
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SHOCK INITIATION PROPERTIES 432 I I
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SHOCK INITIATION PROPERTIES Fig. 4.
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SHOCK INITIATION PROPERTIES Explosi
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SHOCK INITIATION PROPERTIES TRANSIT
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SHOCK INITIATION PROPERTIES 442 FOI
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SENSITIVITY TESTS 5. SENSITIVITY TE
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Ammonium nitrate Ammonium picrate B
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-’ .-- _- ..- _ “. Cyclotol75/2
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Explosive RDX-Based with Metal Fill
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SENSITIVITY TESTS 5.2 Skid Test. Th
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Explosive Comp A-3 1.638 45 PBX 901
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SENSITIVITY TESTS 5.3 Large-Scale D
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SENSITIVITY TESTS 5.4 Spark Sensiti
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GLOSSARY ABH Amatex-20 ATNI BDNPA B
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NP OFHC ONT P-16 P-22 P-40 P-80 P-1
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AUTHOR IND Ablard, J. E. 141, 151 A
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SUBJECT INDEX ABH 461 Alex/20 204,
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pentaerythritol tetranitrate (PETN)
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