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HMX 5. THERMAL PROPERTIES 46 5.1 Phase Changes.6-8 Latent Heat ‘be Temperaturea w W/d (kcal/mole) Solid-to-solid Bba atoy ato6 Solid-to-liquid a* ; Solid-to-gas 102-104 Metastable 160-164 2.0 0.6 --_ ___ 7.8 2.3 256-257 _-_ --_ 246-247 50.0 17.0 279-280 _-_ __- 280-281 --_ --- --- 141.4 41.8gb --------- “There is some controversy about the temperature stability ranges of the four HMX polymorphs. These data are from Ref. 8. Vomputed from the vapor pressure data presented in Sec. 5.2. 5.2 Vapor Pressure.B A least squares fit to these data gives Temperature Vapor Pressure (“(2 (mm Hg x 10’) 97.6 0.032 108.2 0.164 115.6 0.385-0.419 129.3 2.830-2.870 log,, P(mm Hg) = 16.18 - 41 890/4.576 T(K) . r
5.3 Heat Capacity. 5.4 Thermal Conductivity.l” Heat Capacity at Constant Pressure (Cal/g-“C) 0.231 + 5.5 X 1O-4 T Conductivity (Cal/s-cm-“C) Temperature Range (“C) 37 < T < 167 Temperature (“C) 1.2 x 10-a 25 9.7 x 10-d 160 5.6 Heats of Combustion and Formation at 25%k11 AH; AH; kcal/mole kcal/mole -660.7 11.3 5.7 Thermal Decomposition Kinetics.l*. Decomposition energy 500 Cal/g Activation energy 52.7 kcal/mole Pre-exponential factor 5 x 10lg/s 5.8 Other Thermal Stability Test Results. Test Results Vacuum 0: l-O.4 ml/g of gas evolved after 48 h at 120°C DTA and pyrolysis See Fig. 2 Critical temperature, Tm 253°C Charge radius, a 3.3 mm Density, p 1.81 g/cm* HMX 47
Page 2 and 3:
LOS ALAMOS SERIES ON DYNAMIC MATERI
Page 4 and 5: University of California Press Berk
Page 6 and 7: PART II. EXPLOSIVES PROPERTIES BY P
Page 8 and 9: treats pure explosives first, alpha
Page 10 and 11: EXPLOSIVES PROPERTIES BY EXPLOSIVE
Page 12 and 13: BARATOL 2.3 Shipping.2 Baratol is s
Page 14 and 15: BARATOL 6 5.4 Thermal Conductivity.
Page 16 and 17: BARATOL 6.2 Detonation Pressure. We
Page 18 and 19: BARATOL REFERENCES . . 1. N. I. Sax
Page 20 and 21: COMP B slowly. Heating and stirring
Page 22 and 23: COMP B 14 3.3 Solubility.‘The sol
Page 24 and 25: COMP B 16 5.3 Heat Capacity. Heat C
Page 26 and 27: COMP B 18 6.2 Detonation Pressure.
Page 28 and 29: COMP B 7.3 Shock Hugoniots.12J8 Com
Page 30 and 31: COMP B 9. MECHANICAL PROPERTIES 22
Page 32 and 33: CYCLOTOL 1. GENERAL PROPERTIES 1.1
Page 34 and 35: CYCLOTOL 26 3.2 Molecular Weight. C
Page 36 and 37: CYCLOTOL 4.3 Infrared Spectrum. See
Page 38 and 39: CYCLOTOL where D = detonation veloc
Page 40 and 41: CYCLOTOL 8.3 Skid Test Results. Den
Page 42 and 43: DATB 1. GENERAL PROPERTIES 1.1 Chem
Page 44 and 45: DATB 4. PHYSICAL PROPERTIES 4.1 Cry
Page 46 and 47: DATB 5.4 Thermal Conductivity, Cond
Page 48 and 49: DATB 7.3 Shock Hugoniot.9 Density k
Page 50 and 51: HMX* 1. GENERAL PROPERTIES 1.1 Chem
Page 52 and 53: HMX 3.2 Molecular Weight. 296.17 3.
Page 56 and 57: HMX 6. DETONATION PROPERTIES 6.1 De
Page 58 and 59: HMX 7.3 Shock Hugoniots.” Density
Page 60 and 61: NITROGUANIDINE 1. GENERAL PROPERTIE
Page 62 and 63: NQ 54 4.2 Density.’ Crystal Metho
Page 64 and 65: NQ 56 5.6 Heats of Combustion and F
Page 66 and 67: NQ 6.2 Detonation Pressure. There a
Page 68 and 69: NQ 8. SENSITIVITY 8.1 Drop Weight I
Page 70 and 71: OCTOL These are shipped to an ordna
Page 72 and 73: 64 OCTOL 3.3 Solubility.6 The solub
Page 74 and 75: OCTOL 5. THERMAL PROPERTIES 66 5.1
Page 76 and 77: OCTOL 68 6.4 Plate Dent Test Result
Page 78 and 79: OCTOL 8.3 Skid Test Results. Weight
Page 80 and 81: PBX 9011 1. GENERAL PROPERTIES 1.1
Page 82 and 83: PBX 9011 3.3 Solubility. The solubi
Page 84 and 85: PBX 9011 76 5.5 Coefficient of Ther
Page 86 and 87: PBX 9011 78 6.3 Cylinder Test Resul
Page 88 and 89: PBX 9011 7.5 Detonation Failure Thi
Page 90 and 91: PBX 9011 82 9.3 Compressive Strengt
Page 92 and 93: PBX9404 1. GENERAL PROPERTIES 1.1 C
Page 94 and 95: PBX 9404 86 3.2 Molecular Weight. C
Page 96 and 97: PBX 9404 88 4.3 Infrared Spectrum.
Page 98 and 99: PBX 9404 > 1 1 o- r 0 I I I, / PYRO
Page 100 and 101: PBX 9404 7. SHOCK INITIATION PROPER
Page 102 and 103: PBX 9404 7.5 Detonation Failure Thi
Page 104 and 105:
PBX 9404 8.5 Spark Sensitivity. Ele
Page 106 and 107:
PBX 9404 REFERENCE‘S 1. Committee
Page 108 and 109:
PBX 9407 2.3 Shipping.2 PBX-9407 mo
Page 110 and 111:
PBX 9407 4.3 Infrared Spectrum. See
Page 112 and 113:
PBX 9407 6. DETONATION PROPERTIES I
Page 114 and 115:
PBX 9407 106 7.2 Wedge Test Results
Page 116 and 117:
PBX 9407 9.3 Compressive Strength a
Page 118 and 119:
PBX 9501 2.3 Shipping.* PBX-9501mol
Page 120 and 121:
PBX 9501 5. THERMAL PROPERTIES 112
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PBX 9501 6. DETONATION PROPERTIES 6
Page 124 and 125:
PBX 9501 7.3 Shock Hugoniot. Densit
Page 126 and 127:
PBX 9501 9. MECHANICAL PROPERTIES*
Page 128 and 129:
PBX9502 1. GENERAL PROPERTIES 1.1 C
Page 130 and 131:
PBX 9502 3.3 Solubility. The solubi
Page 132 and 133:
PBX 9502 124 5.3 Heat Capacity. 5.4
Page 134 and 135:
PBX 9502 6.3 Cylinder Test Results.
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PBX 9502 9. MECHANICAL PROPERTIES 1
Page 138 and 139:
PENTAERYTHRITOLTETRANITRATE (PETN)
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PETN 3.2 Molecular Weight. 316.15 3
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PETN 4.4 Refractive Indices.s Omega
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PETN 5.7 Thermal Decomposition Kine
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PETN 138 7.2 Wedge Test Results. De
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, PETN 5. US Army Materiel Command,
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RDX developed into a continuous hig
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RDX 4. PHYSICAL PROPERTIES 4.1 Crys
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RDX 146 5.2 Vapor Pressure.8 Temper
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RDX 6. DETONATION PROPERTIES 148 6.
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RDX 7.3 Shock Hugoniot.” 8. SENSI
Page 160 and 161:
TATB 1. GENERAL PROPERTIES 1.1 Chem
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TATB TATB solubility in sulfuric ac
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TATB 5.2 Vapor Pressure.6 A least s
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TATB I / / I I I I I I I ! \ I 1 \
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TATB 7.3 Shock Hugoniots.“+ A num
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TATB REFERENCES 1. T. M Benziger an
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TETRYL acetone. In the second proce
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TETRYL 2.5 100 80 60 % T 40 20 0 :;
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TETRYL 6. DETONATION PROPERTIES 6.1
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TETRYL 7.5 Detonation Failure Thick
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TNT 1. GENERAL PROPERTIES 1.1 Chemi
Page 182 and 183:
TNT 4. PHYSICAL PROPERTIES 4.1 Crys
Page 184 and 185:
TNT 4.3 Infrared Spectrum. See Fig.
Page 186 and 187:
TNT 178 5.5 Coefficient of Thermal
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TNT The charge preparation method a
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TNT 182 6.4 Plate Dent Test Results
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TNT 7.3 Shock Hugoniots.2aJ4 Densit
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TNT 9.3 Compressive Strength and Mo
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XTX8003 1. GENERAL PROPERTIES 1.1 C
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XTX 8003 3.3 Solubility.6 The solub
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XTX 8003 5.7 Thermal Decomposition
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XTX 8003 8. SENSITIVITY 8.1 Drop We
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XTX8004 1. GENERAL PROPERTIES 1.1 C
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XTX 8004 3.3 Solubility. The solubi
Page 208 and 209:
XTX 8004 6. DETONATION PROPERTIES 6
Page 210 and 211:
PART II EXPLOSIVES PROPERTIES BY IP
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Explosive Alex/20 Alex/30 Amatex/20
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Explosive PBX 9007 PBX 9010 PBX 901
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Explosive Constituents X-0234-60 X-
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Alex/20 Alex/30 Amatexl20 Amatexl30
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NQ octo1 PAT0 Explosive PBX 9007 PB
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X-0234-60 X-0234-70 X-0234-80 X-028
Page 224 and 225:
THERMAL PROPERTIES 2. THERMAL PROPE
Page 226 and 227:
THERMAL PROPERTIES k2 = kl - (4, -
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Explosive PETN RDX TNT Table 2.03 C
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THERMAL PROPERTIES AEE = standard i
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THERMAL PROPERTIES Fig. 2.02. Pyrol
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,’ THERMAL PROPERTIES L Y !s :: B
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THERMAL PROPERTIES 228 Composition
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THERMAL PROPERTIES B Y !3 E E “I
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THERMAL PROPERTIES This assembly is
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DETONATION PROPERTIES 3. DETONATION
Page 244 and 245:
DETONATION PROPERTIES 236 Table 3.0
Page 246 and 247:
Shot No. c-4394 E-4672 E-4067 E-406
Page 248 and 249:
DETONATION PROPERTIES Table 3.06 CY
Page 250 and 251:
Table 3.08 OCTOL DETONATION VELOCIT
Page 252 and 253:
Rate Stick Shot ’ Diameter No. (m
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DETONATION PROPERTIES 246 Table 3.1
Page 256 and 257:
Shot No. C-4436 E-3621 - Rate Stick
Page 258 and 259:
Table 3.15 GENERAL CYLINDER TEST SH
Page 260 and 261:
DETONATION PROPERTIES 252 Expansion
Page 262 and 263:
Expansion Radius (mm) Table 3.19 X-
Page 264 and 265:
N VI UY Table 3.21 X-0285 WALL VELO
Page 266 and 267:
DETONATION PROPERTIES Table 3.25 X-
Page 268 and 269:
Explosive Table 3.26 DETONATION (C-
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DETONATION PROPERTIES Analysis Line
Page 272 and 273:
DETONATION PROPERTIES Explosive Tab
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Page 276 and 277:
Page 278 and 279:
Page 280 and 281:
Page 282 and 283:
Page 284 and 285:
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DETONATION PROPERTIES 3.4 Plate Den
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Exnlosive Table 3.46 (continued) De
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Explosive PBX 9501 x-0007 86 HMX/14
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85 RDX/lS Kel-F Explosive 88 RDXI12
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DETONATION PROPERTIES Table 3.47 LE
Page 298 and 299:
DETONATION PROPERTIES Table 3.48 DE
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SHOCK INITIATION PROPERTIES PETN Ba
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SHOCK INITIATION PROPERTIES Fig. 4.
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SHOCK INITIATION PROPERTIES each sh
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SHOCK INITIATION’PROPERTIES Table
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SHOCK INITIATION PROPERTIES 300 i;
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w R Table 4.04 NITROMETHANE Composi
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SHOCK INITIATION PROPERTIES 304 Tab
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SHOCK INITIATION PROPERTIES 306 / D
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SHOCK INITIATION PROPERTIES 308 2 0
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Table 4.06 (continued) Coordinates
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SHOCK INITIATION PROPERTIES 312 I-
Page 322 and 323:
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SHOCK INITIATION PROPERTIES 316 05
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Table 4.07 PETN (SINGLE CRYSTAL) Co
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Table 4.08 (continued) Shot Number
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SHOCK INITIATION PROPERTIES 324 2 u
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SHOCK INITIATION PROPERTIES Table 4
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SHOCK INITIATION PROPERTIES 334 2T
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Initial Shock Parameters Table 4.12
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SHOCK INITIATION PROPERTIES 342 Ini
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3 *a i 8 3 x j > f m e c u,, = (2.3
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SHOCK INITIATION PROPERTIES 348 Dis
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w ul 0 Composition 95 wt% DATB, 5 w
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SHOCK INITIATION PROPERTIES 5.5- 5.
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5 Table 4.17 (continued) Coordinate
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SHOCK INITIATION PROPERTIES 40- 20
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Shot E-3120 3.370 $0.022 E-3131 2.4
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_. Shot Number E-771 E-781 B-4481 B
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SHOCK INITIATION PROPERTIES 364 2 I
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SHOCK INITIATION PROPERTIES 366 0.6
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SHOCK INITIATION PROPERTIES Composi
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Table 4.21 X-0219-50-14-10 Composit
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Composition 95 wt% NQ, 5 wt% Estane
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Shot Number (G?a) E-3245 16.2 5.904
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SHOCK INITIATION PROPERTIES 380 c x
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w R Table 4.24 (continued) Reduced
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Table 4.25 XTX-8003 (EXTEX) Composi
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SHOCK INITIATION PROPERTIES 386 a--
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Table 4.27 PBX 9407 Compositon 94 w
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SHOCK INITIATION PROPERTIES 390 3 g
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Table 4.28 PBX 9405 Cotiposition 93
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SHOCK INITIATION PROPERTIES 394 c 5
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% OY Table 4.30 x-0250-40-19 Compos
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SHOCK INITIATION PROPERTIES 398 Dis
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Table 4.32 95 TATB/2.5 Kel-F 800/2.
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Table 4.39 (continued) Coordinates
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z Table 4.44 FKM CLASS VII PROPELLA
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Theoretical Maximum Density >1.910
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Ammonium picrate Raratol(76/24) mix
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HMX-Based PBX 9011 PBX 9404 PBX-950
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SHOCK INITIATION PROPERTIES 0.360 c
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SHOCK INITIATION PROPERTIES 432 I I
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SHOCK INITIATION PROPERTIES Fig. 4.
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SHOCK INITIATION PROPERTIES Explosi
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SHOCK INITIATION PROPERTIES TRANSIT
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SHOCK INITIATION PROPERTIES 442 FOI
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Page 454 and 455:
SENSITIVITY TESTS 5. SENSITIVITY TE
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Ammonium nitrate Ammonium picrate B
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-’ .-- _- ..- _ “. Cyclotol75/2
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Explosive RDX-Based with Metal Fill
Page 462 and 463:
SENSITIVITY TESTS 5.2 Skid Test. Th
Page 464 and 465:
Explosive Comp A-3 1.638 45 PBX 901
Page 466 and 467:
SENSITIVITY TESTS 5.3 Large-Scale D
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SENSITIVITY TESTS 5.4 Spark Sensiti
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GLOSSARY ABH Amatex-20 ATNI BDNPA B
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NP OFHC ONT P-16 P-22 P-40 P-80 P-1
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AUTHOR IND Ablard, J. E. 141, 151 A
Page 476 and 477:
SUBJECT INDEX ABH 461 Alex/20 204,
Page 478 and 479:
pentaerythritol tetranitrate (PETN)
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