FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field

Instrument
Calibration
Procedure
GC/MS
GC/MS DFTPP
Tune
Prior to start of analysis
GC/MS CCAL
and every 12 hours
thereafter
ICP ICAL Daily and prior to sample
analysis
ICP ICV After ICAL, prior to
beginning a sample run
ICP CCV Daily before sample
analysis, every 10
samples, and at the end of
the analysis sequence
Polarized Light
Microscopy
(PLM)
Blank
Table 24-1. Analytical Instrument Calibration
Frequency of Calibration Acceptance Criteria Corrective Action
Person
Responsible for
Corrective Action
SOP
Reference
Beginning of 12-hour shift Method-specified Repeat until criteria are met Laboratory Analyst BCORG020
Friable – one blank side
daily or every 50 samples,
whichever is less.
Non-friable – one
asbestos containing
material (ACM) or nonfriable
material every 20
samples.
RRF ≥ 0.05, %D±25%
All analytes within ±10%
of expected value. r ≥
0.995.
All analytes within + 10%
of expected value
RSD of replicate
integrations: < 5%
All analytes within + 10%
of expected value
RSD of replicate
integrations < 5%
Repeat CCAL once; repeat ICAL if
second CCAL fails
Prepare fresh standard and re-analyze
ICV to rule out standard degradation or
inaccurate injection. If problem persists,
then perform instrument adjustment
and/or maintenance to correct the
problem and repeat ICAL.
If RSDs 5%, then perform
instrument maintenance to correct the
problem and repeat ICAL.
If RSDs 5%, then perform
instrument maintenance to correct the
problem. Recalibrate and reanalyze all
samples since last successful CCV.
Laboratory Analyst
Laboratory Analyst
Laboratory Analyst
Laboratory Analyst
Negative Prepare and analyze another blank. Laboratory Analyst 1265
BCORG020
BCMET013
BCMET013
BCMET013
Final Sampling and Analysis Plan
Installation Restoration Site 29, Hangar 1
Former Naval Air Station, Moffett Field, Moffett Field, California
DCN: AMEC-8816-0005-0039
April 2010
Page 24-2