FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
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Instrument/<br />
Equipment<br />
Mass<br />
Spectrometer<br />
Mass<br />
Spectrometer<br />
Mass<br />
Spectrometer<br />
Mass<br />
Spectrometer<br />
Maintenance<br />
Activity<br />
Pump Oil Level<br />
Detector<br />
Bakeout<br />
Clean source,<br />
replace filament<br />
Detector Precalibration<br />
Testing<br />
Activity<br />
NA<br />
Observation of<br />
deteriorating<br />
chromatograp<br />
hy<br />
Observation of<br />
deteriorating<br />
chromatograp<br />
hy<br />
Resolution<br />
adjustment<br />
Inspection<br />
Activity<br />
Visual<br />
inspection of<br />
oil gauge<br />
and color of<br />
oil<br />
NA<br />
Visual<br />
inspection of<br />
filaments<br />
Observation<br />
of tuning<br />
spectrum<br />
ICP Parameter Setup Physical check Physical<br />
check<br />
Frequency<br />
Check<br />
Monthly;<br />
Change<br />
Annually<br />
As needed<br />
As needed<br />
Every 12<br />
hours<br />
Initially; prior<br />
to DCC<br />
Acceptance Criteria<br />
Adequate oil<br />
level<br />
No interference/<br />
carryover peaks<br />
No interference;<br />
adequate<br />
spectral<br />
resolution<br />
Per method<br />
tuning<br />
requirements<br />
Predetermined<br />
optimum parameter<br />
settings<br />
Corrective<br />
Action<br />
Add oil<br />
Clean<br />
detector<br />
Clean<br />
source;<br />
replace<br />
filament<br />
Adjust<br />
optics<br />
Reset if<br />
incorrect<br />
Responsible<br />
Person<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
SOP<br />
Reference<br />
BCORG020<br />
BCORG020<br />
BCORG020<br />
BCORG020<br />
BCMET013<br />
Final Sampling and Analysis Plan<br />
Installation Restoration Site 29, Hangar 1<br />
Former Naval Air Station, <strong>Moffett</strong> <strong>Field</strong>, <strong>Moffett</strong> <strong>Field</strong>, Cali<strong>for</strong>nia<br />
DCN: AMEC-8816-0005-0039<br />
April 2010<br />
Page 25-2
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