FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
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Instrument/<br />
Equipment<br />
ICP<br />
ICP<br />
Maintenance<br />
Activity<br />
Interference<br />
check<br />
solutions/interfer<br />
ence check<br />
solution – A<br />
(ICS/ICS-A)<br />
ICAL<br />
blank/CCAL<br />
blank (ICB/CCB)<br />
Testing<br />
Activity<br />
Instrument<br />
Per<strong>for</strong>mance<br />
Instrument<br />
Per<strong>for</strong>mance<br />
Inspection<br />
Activity<br />
Con<strong>for</strong>manc<br />
e to<br />
interference<br />
check<br />
Instrument<br />
contaminati<br />
on check<br />
Frequency<br />
Prior to<br />
sample<br />
analysis<br />
After every<br />
calibration<br />
verification<br />
Acceptance Criteria<br />
Within + 20% of<br />
expected value<br />
No analytes detected<br />
greater than (>) three<br />
times instrument<br />
detection limit (IDL)<br />
Corrective<br />
Action<br />
Terminate<br />
analysis,<br />
reanalyze<br />
ICS to rule<br />
out standard<br />
degradation<br />
or<br />
inaccurate<br />
injection. If<br />
problem<br />
persist, then<br />
per<strong>for</strong>m<br />
instrument<br />
maintenanc<br />
e, repeat<br />
calibrations,<br />
and<br />
reanalyze all<br />
associated<br />
samples.<br />
Determine<br />
possible<br />
source of<br />
contaminati<br />
on and<br />
apply<br />
appropriate<br />
measure to<br />
correct the<br />
problem.<br />
Reanalyze<br />
calibration<br />
blank and all<br />
associated<br />
samples.<br />
Responsible<br />
Person<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
SOP<br />
Reference<br />
BCMET013<br />
BCMET013<br />
Final Sampling and Analysis Plan<br />
Installation Restoration Site 29, Hangar 1<br />
Former Naval Air Station, <strong>Moffett</strong> <strong>Field</strong>, <strong>Moffett</strong> <strong>Field</strong>, Cali<strong>for</strong>nia<br />
DCN: AMEC-8816-0005-0039<br />
April 2010<br />
Page 25-3
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