FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
FINAL SAMPLING AND ANALYSIS PLAN - Documents for Moffett Field
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WORKSHEET #25: ANALYTICAL INSTRUMENT <strong>AND</strong> EQUIPMENT MAINTENANCE, TESTING, <strong>AND</strong> INSPECTION<br />
TABLE<br />
This worksheet identifies all analytical instrumentation that requires maintenance, testing, or inspection and provides the laboratory<br />
SOP reference number <strong>for</strong> each. In addition, documentation of the frequency, acceptance criteria, and corrective action requirements<br />
are also provided on this worksheet. This worksheet will be completed upon laboratory procurement.<br />
Instrument/<br />
Equipment<br />
Table 25-1. Analytical Instrument and Equipment Maintenance, Testing, and Inspection<br />
Maintenance<br />
Activity<br />
Testing<br />
Activity<br />
Inspection<br />
Activity<br />
GC Parameter Setup Physical check Physical<br />
check<br />
GC Retention time<br />
(RT) window<br />
width calculated<br />
<strong>for</strong> each analyte<br />
and surrogate<br />
GC RT window<br />
position <strong>for</strong> each<br />
analyte check<br />
Instrument<br />
Per<strong>for</strong>mance<br />
Instrument<br />
Per<strong>for</strong>mance<br />
Instrument<br />
per<strong>for</strong>mance<br />
check<br />
Instrument<br />
per<strong>for</strong>mance<br />
check<br />
Frequency<br />
Initially; prior<br />
to daily<br />
calibration<br />
check<br />
At method setup<br />
and after<br />
major<br />
maintenance<br />
(e.g. column<br />
change)<br />
Once per ICAL<br />
and at the<br />
beginning of<br />
the analytical<br />
shift<br />
Acceptance Criteria<br />
Autosampler must<br />
move to the expected<br />
position when<br />
activated.<br />
Refer to instrument<br />
optimize temperature<br />
program setup.<br />
RT width is ± 3 times<br />
standard deviation <strong>for</strong><br />
each analyte RT from<br />
a 72-hour study.<br />
Position shall be set<br />
using the midpoint<br />
standard of the ICAL<br />
curve when ICAL is<br />
per<strong>for</strong>med. On days<br />
when ICAL is not<br />
per<strong>for</strong>med, the initial<br />
CCV is used.<br />
Corrective<br />
Action<br />
Reset if<br />
incorrect<br />
Locate<br />
source of<br />
the problem.<br />
Repeat if<br />
incorrect.<br />
Locate<br />
source of<br />
the problem.<br />
Repeat if<br />
incorrect.<br />
Responsible<br />
Person<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
Laboratory<br />
Analyst<br />
SOP<br />
Reference<br />
BCORG019<br />
BCORG005<br />
BCORG019<br />
BCORG005<br />
BCORG019<br />
BCORG005<br />
Final Sampling and Analysis Plan<br />
Installation Restoration Site 29, Hangar 1<br />
Former Naval Air Station, <strong>Moffett</strong> <strong>Field</strong>, <strong>Moffett</strong> <strong>Field</strong>, Cali<strong>for</strong>nia<br />
DCN: AMEC-8816-0005-0039<br />
April 2010<br />
Page 25-1
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