OP-II-3

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PL-3Main features of developed technology are:− biofuel production of two types: biodiesel and green diesel;− varying of biodiesel and green diesel yields depending needs;− optimization of hydrogen consumption;− energy-supply of both stages via burning of gaseous products, produced on2nd step.Catalytic characteristics of the technology include application of heterogeneousbasic trasetherification catalysts under 200-220°C and 2.0 MPa and possibility ofmultiple catalyst regeneration for the first stage. For the second stage these onescomprise using of non-sulfided and non-noble metal catalysts, mild reactionconditions (300-340°C and 2.0 MPa H 2 ) and possibility of green diesel productionwith different cetane number via hydroisomerization catalysts application.The bio-oil, which is a product of flash pyrolysis of grinded wood, is anotherperspective feedstock for the petrol production. However bio-oil cannot substitutetraditional gasoline and diesel in the internal-combustion engines on its own owing totheir lower operational properties. The main reason is the high oxygen content inabove mentioned bio-fuels. Bioethanol and biodiesel can be used as the additive togasoline and diesel correspondingly while bio-oil requires catalytic elimination ofoxygen from it and simultaneous saturation by hydrogen.It should be pointed out that one cannot use traditional hydrocracking catalystsfor oil-refinery at hydrotreatment of bio-fuels because of low sulfur content in originalfeedstock. The main reason of these phenomena is reduction of the sulfided Co- orNi- containing active center to the metal state, followed by coke formation and thecatalyst deactivation. When so, sulfur is removed from the catalysts and the targetproducts are contaminated by sulfur. Thus, the objective of the present investigationis to develop non-sulfided catalysts for upgraded bio-fuels production. The obtainedupgraded products can be used as additives to fossil crude-oil in the standard oilrefining.On the whole catalytic process development is carried out within FP6BIOCOUP project with following conception:BiomassresiduesLiquefactionProcessresiduesFractionationduring andaftercondensationHydrocarbon-rich fractionLignin-richfractionDe-oxygenationDerivatives of hemicellulosesand cellulosesCo-processing inconventionalpetroleum refineryConversionConventional fuelsand chemicals(blending)Oxygenated productsEnergyproductionNote: hydrocarbon-rich fractions are formed when the biomass feedstock contains asignificant amount of extractive substances; e.g the case for forestry residues.12
PL-3Indeed preparation and testing in target processes such binary catalytic systemshas shown that developed mild hydrocracking catalysts permit not only to obtainalkanes C 11 – C 17 in one stage with the yield 100% both from biodiesel and fromvegetable oils at mild conditions: 260 – 350°C, hydrogen pressure 1,0 – 2,5 MPa, butalso to reduce oxygen content in bio-oils in one stage too from 45 wt% until 5 wt% at320 – 350°C, hydrogen pressure 12–15 MPa.AcknowledgmentsFP6 project № 518312, integration project №2 SB RAS are gratefully acknowledged.13
Page 1 and 2: Boreskov Institute of Catalysisof t
Page 3 and 4: INTERNATIONAL SCIENTIFIC COMMITTEEV
Page 5 and 6: SILVER SPONSORThe organizers expres
Page 7 and 8: PL-1HOW TO DESIGN OPTIMAL CATALYTIC
Page 9 and 10: MULTIFUNCTIONAL DEVICES FOR INTENSI
Page 11: PL-3DESIGN OF CATALYTIC PROCESSES F
Page 15 and 16: PL-4The second part of the lecture
Page 17 and 18: PL-5Reactor designs with intensifie
Page 19 and 20: PL-6MEMBRANE REACTORS: STATE OF THE
Page 21 and 22: KEY-NOTE PRESENTATIONS
Page 23 and 24: KN-1description, that can be charac
Page 25 and 26: KN-2selective catalytic reduction o
Page 27 and 28: KN-3Fig. 1. Experimental burner of
Page 29 and 30: KN-4~200°C. This is based on the H
Page 31 and 32: KN-5for addressing the quality of t
Page 33 and 34: KN-6reaction with ethanol and the b
Page 35 and 36: KN-7at temperature lower than 873K,
Page 37 and 38: REACTION KINETICS AND REACTION ENHA
Page 39 and 40: OP-I-2RELATION BETWEEN THE ACTIVATI
Page 41 and 42: COMPARISON OF CHEMICAL AND ENZYMATI
Page 43 and 44: OP-I-4NONLINEAR PHENOMENA DURING ME
Page 45 and 46: OP-I-5SPECIFICITY OF THE OSCILLATIO
Page 47 and 48: OP-I-6TRENDS IN BISTABILITY DOMAINS
Page 49 and 50: OP-I-7NON-STEADY-STATE CATALYST CHA
Page 51 and 52: OP-I-8TRANSIENT KINETIC STUDIES OF
Page 53 and 54: OP-I-9A REDOX KINETICS FOR THE PART
Page 55 and 56: OP-I-9500Flow of Air = 0.3 m 3 (STP
Page 57 and 58: OP-I-11ELUCIDATION OF THE REACTIVIT
Page 59 and 60: KINETIC MODELLING OF THE JOINT TRAN
Page 61 and 62: OP-I-13n-HEXANE SKELETAL ISOMERIZAT
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OP-I-14the slow branch of kinetic c
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OP-I-15The hydride palladium comple
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Energy Conservation (field j)∂∂
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OP-I-17Selectivity (mol. %)10099989
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OP-I-18According to GLC the main pr
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OP-I-19and slug dimensions, formati
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OP-I-20A RANS volume of fluids [1]
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OP-I-21the physical-chemical charac
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OP-I-22calculated values of pressur
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OP-I-23where L c - capillary length
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OP-I-24and diffuse transmission thr
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OP-I-25effect of bubble break-up wo
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OP-I-26strong influence on the soli
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OP-I-27wHCOOH=1+K2K1(1 + K3⋅ P⋅
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OP-I-28dimensional profiles detecte
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OP-I-29results. The results of the
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OP-I-30Fig. 1. Hydrodynamics and co
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OP-I-31Convection and diffusion wit
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TEMPERATURE RISE DURING REGENERATIO
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OP-II-2[4]. Similar temperature pro
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OP-II-3(Fig, 1 a, b) upon testing i
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OP-II-4In the second step optimizat
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OP-II-5membrane contactors were stu
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OP-II-6reaction over Cu/CeO 2-x cat
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OP-II-7is modelled by means of a tw
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OP-II-8the reactor [6]. However, th
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OP-II-9Figure 1. Computed volume fr
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OP-II-10assumes variables’ distri
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OP-II-11oxide support, it comes tha
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OP-II-12was connected to G.C. via s
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OP-II-13catalyst bed was 6 mm. Thre
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OP-II-14as coolant is an important
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OP-II-15Flow (L/h)7654321Bottoms ra
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OP-II-16(4) The gas recirculation r
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OP-II-17Catalytic reactions were ca
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OP-II-18At steady surface coverage
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OP-II-19gaimpulsegeneratorwateFig.
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OP-II-20examined (see Figure 1). Th
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OP-II-21References[1]. M.P. Dudukov
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OP-II-22of the hydrogen oxidation a
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OP-II-23TemperaturesensorsThe efflu
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OP-II-24of reactant conversions. Pa
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OP-II-25(surface) ‘wall-reaction
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OP-II-26It was found that the 10 wt
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OP-II-27non-flow type. During the M
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OP-III-A-1A NEW SIMPLE MICROCHANNEL
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BUBBLING FLUIDISED BED PYROLYSIS OF
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PINEWOOD PYROLYSIS UNDER VACUUM CON
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OP-III-A-5PYROLYSIS OF HDPE IN A CO
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OP-III-A-6REACTORS FOR THE GREEN TR
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DEHYDRATION OF GLYCEROL TO ACROLEIN
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OP-III-A-8LACTIC ACID BASED ON BIO
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RECOVERY OF ACETIC ACID FROM PYROLY
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OP-III-A-10LIPASE-CATALYZED REACTIO
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OP-III-A-11INVESTIGATION ON THERMOC
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OP-III-A-12SELECTIVE CATALYTIC DEOX
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ETHANOL STEAM REFORMING OVER COBALT
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OP-III-A-14HYDROTREATMENT CATALYSTS
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ORAL PRESENTATIONSSECTION IIIChemic
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OP-III-B-1Reactor parameters:Intern
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OP-III-B-2JOINT STEAM REFORMING OF
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OP-III-B-3LANDFILL BIOGAS PURIFICAT
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OP-III-B-4MODELING AND SIMULATION O
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OP-III-B-5DemonstratorThe medium-te
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OP-III-B-630/19.6 Nl/min (space vel
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OP-III-B-7mixed in the ratios: 94,8
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OP-III-B-8Table 1.Material balance
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OP-III-B-9Based on the results of t
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OP-III-B-10On this basis it can be
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OP-III-B-11Similar trends caused by
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OP-III-B-12(mol/s g cat)x108r4,6-DM
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OP-III-B-13carbon in Wyoming coal i
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OP-III-B-14MODELING PRODUCT DISTRIB
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OP-III-B-15COMBINED TECHNOLOGY OF U
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MATEMATICAL MODEL FOR DOWNDRAFT BIO
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OP-III-B-17CATALYTIC DEHYDRATION OF
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OP-III-B-18SYNGAS AND HYDROGEN PROD
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POSTER PRESENTATIONSSECTION I
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PP-I-1influence of the direction of
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PP-I-2At the agitation of the liqui
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PP-I-3NOLINEAR PHENOMENA IN CATALYT
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PP-I-4A NEW APPROACH TO KINETIC STU
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PP-I-5KINETICS OF PROX REACTION OVE
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PP-I-6PHENOMENA OF SUPERADIABATIC T
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ELECTROMAGNETIC REACTOR OF WATER TR
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PP-I-8DIRECT SYNTHESIS OF HYDROGEN
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PP-I-9DYNAMICS OF FIRST-ORDER PHASE
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PP-I-10ELECTROCHEMICAL OXIDATION OF
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PP-I-11CHEMPAK SOFTWARE PACKAGE: OP
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PP-I-12COMPUTER SIMULATION OF ENDOT
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PP-I-13MODELLING KINETICS OF PROCES
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PP-I-14THE INVESTIGATION OF REACTIO
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PP-I-15The qualitative picture of s
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Thus, knowing the composition of ra
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PP-I-17current density. Preliminary
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PP-I-18Hydrogenation kinetics was d
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PP-I-19the active mixing, amplitude
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PP-I-20where r, h indicate the radi
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PP-I-21model is very anisotropic be
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PP-I-22- Reduction of the number of
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PP-I-23oscillations of intermediate
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PP-I-25SYNTHESIS OF ETHYLENE OXIDE
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PP-I-26OPTIMUM KINETICS FOR POLYSTY
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PP-I-27TableSpecific surface area (
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PP-I-28γ-preirradiated sample), th
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PP-I-29commercial CFD solver FLUENT
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PP-I-30modulus, a considerable decr
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PP-I-31The destruction ways of CF 3
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PP-I-32[7]. Karoor S, Sirkar K. Gas
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PP-I-33above 750°. The catalytic p
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PP-I-35REVERSE FLOW REACTOR WITH FO
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FLOW-RECIRCULATION METHOD FOR INVES
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TO A PROBLEM OF OPTIMIZATION OF FUN
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PP-I-38THE INFLUENCE OF REACTION MI
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PP-I-39METHANOL OXIDATIVE STEAM REF
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PP-I-41CORRECT INVESTIGATION OF THE
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PP-I-42NEW APPROACH OF DEFINITION O
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PP-I-43STREAM HEAT EXCHANGE OF AERO
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PP-I-44HIGH TEMPERATURE OXYGEN TRAN
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PP-I-45KINETICS OF TRANSESTERIFICAT
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MATHEMATICAL MODELING AND OPTIMIZAT
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PP-I-47The basic side reaction is r
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PP-I-49EXPERIMENTAL STUDY OF THE HA
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PP-I-51ON THE KINETICS AND REGULARI
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PP-I-52DIFFERENTIAL THERMAL ANALYSI
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PP-I-53oxidation reaction demonstra
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PP-I-54of reaction. It is establish
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PP-I-55effects, are energetically c
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PP-I-56The experiments and simulati
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PP-I-57In the studied range of temp
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PP-I-58HeadingsAdvances in Chemical
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PP-I-59calculated. During the aroma
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PP-I-60with honeycomb catalyst) act
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Т - temperature, K, D eff - effect
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PP-I-62stirring rate were adopted u
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PP-I-63m 2 = (k 1 y 0 1 +k -1 +k 1
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POSTER PRESENTATIONSSECTION II
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PP-II-1values of operating paramete
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⎡⎛⎢⎜bF⎣⎝=2ab ⎞ 6+ ⎟
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PP-II-4HONEYCOMB MONOLITHIC CATALYS
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MATHEMATICAL MODELING OF THE ALUMIN
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PP-II-6MODELING OF VINYL ACETATE SY
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PP-II-7СENTRIFUGAL DISK REACTORAvv
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PP-II-83) An opportunity of operati
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PP-II-10UV-ACTIVATION OF METHANE CO
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PP-II-11COMBINED APPROACH (FMEA- HA
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PP-II-12Testing the pilot variant o
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PP-II-14NOVEL MICROREACTOR FOR THE
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PP-II-15of 1-2.5 lead to a decreasi
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PP-II-16stages. Kinetic parameters
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PP-II-17whiskers, which assure an a
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PP-II-18с m , с cat - density of
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PP-II-19decrease. So, the potential
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PP-II-20products became a mixture o
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PP-II-21A numerical algorithm and s
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PP-II-22motions at any external con
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PP-II-23One of the main technologic
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PP-II-24100 m x 250 μm x 0.5 μm,
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PP-II-25A model was developed to ca
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PP-II-26The results of calculations
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PP-II-27modes of reaction and two d
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PP-II-29OZONE-DESTRUCTION REACTOR B
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PP-II-30Fig. 1. Axial profile of me
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PP-II-31isobutylene in butene fract
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PP-II-322.5x10 -3 ( i )2.5x10 -3 (
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PP-II-33No olefinreadsorptionWith o
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PP-II-34using titania or Ag-doped t
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PP-II-35accidents, is condition dep
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PP-II-36be seen that at temperature
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PP-II-37the solid phase solute conc
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PP-II-38As shown in Table 1, the ca
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PP-II-39better to the obtained in t
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PP-II-40Hydrodynamic regime in the
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PP-II-41activity, relative unit1,21
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PP-II-42One of the major indicators
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PP-II-43These conditions are confor
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PP-II-44For the hepten, alpha-methy
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PP-II-46PARTIAL OXIDATION OF METHAN
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PP-II-47DEVELOPMENT OF VORTEX APPAR
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MODELING OF CFTALYTIC α-OLEFINS OL
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PP-II-49Hinselwood kinetic equation
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3) iterate concentrations at a cut
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PP-II-51data such flow sheet provid
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PP-II-53ON THE TECNOLOGY OF TECHNIC
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PP-II-54PROPYLENE POLYMERIZATION AN
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REACTOR FOR LIQUID-PHASE PROCESSES
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PP-II-56MODELING OF CATALYTIC MICRO
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PP-II-57MATHEMATICAL MODELING OF BE
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PP-II-58HONEYCOMB CATALYSTS WITH PO
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POSTER PRESENTATIONSSECTION IIISECT
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ReferencesPP-III-1[1]. A.N. Pestrya
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PP-III-2Table1. Percentages of diff
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PP-III-3conversion for the reaction
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PP-III-4900Reformer temperature (K)
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PP-III-5Catalytic performance of th
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PP-III-6optimization permit better
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PP-III-8DE-NO X SYSTEM BASED ON H 2
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PP-III-9SEPARATION BETWEEN CHLORIDE
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CONVERSION OF WASTE COTTON TO BIOET
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PP-III-12THE METHOD OF GLYCERIC ACI
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NOx conversion vs. temperature is p
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PP-III-14intermetallic diffusion at
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PP-III-15The conversion of O 2 was
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PP-III-16H 2consumpition (a.u)(a)39
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PP-III-17the characteristic structu
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PP-III-18Figure 1. Influence of tem
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PP-III-19(a)(b)CH 4conversion, %100
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PP-III-20take into account own size
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PP-III-2110080CS-18CS-34CHZ30CHZ801
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EXPERIMENTALPP-III-22We synthesized
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PP-III-23Base composition component
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PP-III-25CO REMOVAL AT THE MICROSCA
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HYDROGEN PRODUCTION FROM METHANOL U
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PP-III-27NON CATALITIC PRODUCTION O
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PP-III-28Different reaction conditi
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PP-III-29followed by WGS reaction.
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PP-III-30As a solvent-coreactants w
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PP-III-31It was concluded that on t
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PP-III-32Hydrogenolysis of glycerol
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PP-III-331,6W 0, μmol Н 2/min1,20
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PP-III-34preparation (glass fiber f
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PP-III-35In the modification proces
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PP-III-36The kinetics of acid hydro
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PP-III-37reaction: i) C=O double bo
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PP-III-38methane and carbon monoxid
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PP-III-39from 25 to 60, which was d
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PP-III-401% w/w for Pd with respect
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PP-III-41material. Besides, the mol
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PP-III-43METHANOL AND DIMETHYL ETHE
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PP-III-44goal is attained by using
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OLIGOMERISATION OF TERTIARY AMINE L
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PP-III-47meter (Shimazu Co.; TOC-50
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PP-III-48the range of 29-87 kJ/mol
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PP-III-49determine the optimal type
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PP-III-50NEW CONCEPT FOR A SELF CLE
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PP-III-51HYDROGEN PRODUCTION BY MET
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PP-III-52CATALYTIC UPGRADING OF PRO
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PP-III-53CATALYTIC CONVERSION OF FI
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PROCESS FOR THE PRODUCTION OF BUTYL
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PP-III-55been previously fixed and
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PP-III-56The influence of reaction
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PP-III-57sample does not contain so
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PP-III-58The re-activation of the e
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PP-III-59The aim of this work is th
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PP-III-61BIODIESEL FROM MICROALGAE
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DEVELOPING MICROFLUIDIC DEVICE WITH
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THREE-PHASE DIRECT OILS HYDROGENATI
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Co-BASED CATALYSTS FOR THE HYDROLYS
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PP-III-65KINETIC STUDY OF THE CATAL
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PP-III-66PRODUCTION OF HYDROGEN AND
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PP-III-67ENHANCED GASIFICATION OF P
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PP-III-68INFLUENCE OF SPILLOVER ON
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PP-III-69AEROBIC OXIDATIVE COUPLING
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PP-III-70MECHANISMS FOR CHEMICAL RE
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PP-III-70SBS molecules and increase
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PP-III-71and as a resut, could enha
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PP-III-72conversion). Al 2 O 3 /PSS
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PP-III-73SBA50TiSBA% Transmittance5
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PP-III-74stove heating. Another par
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PP-III-75TG [%]0-10-20-30380°C400
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PP-III-76The elementary version of
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PP-III-77thermodynamically enhanced
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PP-III-78GFC textileStructuringmeta
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PP-III-79All the prepared spinel-ox
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PP-III-80Our new process is polluti
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PP-III-81Fig. 1. Scheme of the biog
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PP-III-82Pic. 1 Pic. 2Pic. 1. Schem
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ARKHIPOV Vladimir AfanasievichResea
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CENTENO Felipe OrlandoNúcleo de Ex
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FLID Mark RafailovichScientific Res
Page 603 and 604:
HOSEN Mohammad AnwarUniversity of M
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KOZLOVA EkaterinaBoreskov Institute
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MAKARSHIN Lev LvovichBoreskov Insti
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ONSAN Zeynep IlsenDepartment of Che
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REBOLLAR MoisesInstituto De Investi
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SHEIKH Munir AhmedTraining and Staf
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SULMAN Esfir MikhailovnaTver Techni
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ZHAPBASBYEV Uzak KairbekovichKazakh
Page 619 and 620:
OP-I-3 Pécar D., Gorsek A.COMPARIS
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OP-II-3Kucherov A.V., Finashina E.D
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OP-III-A-9 Rasrendra C.B., Girisuta
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PP-I-9Bykov V., Tsybenova S.B.DYNAM
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PP-I-43 Pechenegov Y.Y., Kuzmina R.
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PP-II-10 Basov N.L., Oreshkin I., T
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PP-II-45 Stepanek J., Koci P., Kubi
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PP-III-19 Fedorova Z.A., Danilova M
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PP-III-53 Pölczmann G., Valyon J.,
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XIX International Conference on Che
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