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PP-<strong>II</strong>I-5Al, Fe-PILLARED CLAYS IN CATALYTIC DECOLORIZATIONOF DYE CONTAINING WATERBanković P. 1 , Milutinović-Nikolić A. 1 , Mojović Z. 1 , Jović-Jovičić N. 1 ,Žunić M. 1 , Dondur V. 2 , Jovanović D. 11 Institute of Chemistry, Technology and Metallurgy, University of Belgrade,Department of Catalysis and Chemical Engineering, Njegoševa 12, 11000 Belgrade,Republic of Serbia, E-mail: predragb@nanosys.ihtm.bg.ac.rs2 Faculty of Physical Chemistry, University of BelgradeAl,Fe-pillared clays (PILCs) have shown good performance in catalytic wetperoxide oxidation (CWPO) of organic pollutants in water. They have predominantlybeen tested in the degradation of phenol [1]. There are seldom reports on their use inthe degradation of other organic pollutants such as toluene [2] and dyes [3]. In thiswork a series of Al,Fe–PILCs with different Fe 3+ content was synthesized andcharacterized. Their catalytic performance was studied in the CWPO of food dyetartrazine used as a model compound. Degree of decolorization of tartrazinecontaining aqueous solution was monitored in relation to different parameters suchas Fe 3+ content and temperature.The PILCs were obtained using a common procedure [4] consisting of thefollowing steps: grinding, sieving, Na exchange, intercalation, drying and calcination.Fe 3+ to (Al 3+ +Fe 3+ ) molar ratios in the pillaring solutions were 0%, 1%, 5%, 10%, 15%and 20%, and the corresponding materials were denominated Al–PILC, Al,Fe1–PILC,Al,Fe5–PILC, Al,Fe10–PILC, Al,Fe15–PILC and Al,Fe20–PILC, respectively. Phasecomposition, textural and morphological properties of the starting clay and thesynthesized PILCs were determined using X-ray diffraction (Philips PW 1710 X-raypowder diffractometer with a Cu anode), physisorption of nitrogen (Sorptomatic 1990Thermo Finningen), UV-Vis diffuse reflectance spectrometry (Thermo Evolution 500)and scanning electron microscopy (JSM-646 OLV JEOL). Chemical composition ofthe PILCs was determined using Spectro Spectroflame M - inductively coupledplasma optical emission spectrometer, together with atomic absorption spectrometer.X-ray diffraction analysis confirmed that the pillaring was successful. Chemicalanalysis confirmed the incorporation of Al 3+ and Fe 3+ species in the PILCs.Catalytic tests were carried out in a semibatch reactor under stirring and constanttemperature maintained by circulation of thermostatic fluid using Julabo MC 4 heatingcirculator. Initial dye concentration was 50 ppm in the presence of excess of H 2 O 2 .450
PP-<strong>II</strong>I-5Catalytic performance of the catalysts was examined using UV-Visspectrophotometry. Figures 1 and 2 represent degradation of dye during the courseof the reaction. The former shows the influence of Fe 3+ content at temperature as lowas 35°C, and the latter the influence of reaction temperature.Fig. 1. CWPO of tartrazine on the series ofAl,Fe–PILCs at 35°CFig. 2. CWPO of tartrazine on Al,Fe15–PILCat different temperaturesThe catalytic tests showed good performance of the obtained Al,Fe–PILCs in thedegradation of tartrazine, dependant on the Fe 3+ content and temperature. ForAl,Fe15–PILC it reaches about 98% after 4 h of the reaction conducted at 75 °C.Here investigated method was proven to be efficient in the decolorization of tartrazinecontaining water, thus reducing sunlight cut-off effects, and have prospects as a firststep in a two stage water purification method, where the second one could bebiodegradation.References[1]. Appl. Clay Sci. 2003 Vol. 22, 303-308.[2]. Chin. J. Cat. 2009 Vol. 30, 14-18.[3]. Appl. Catal., B 2009 Vol. 88, 127-134.[4]. Microporous Mater. 1995 Vol. 5, 97-106.AcknowledgementsSupported by the Ministry of Science and Technological Development of the Republic ofSerbia (Projects 166001 and 142019B).451
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Boreskov Institute of Catalysisof t
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INTERNATIONAL SCIENTIFIC COMMITTEEV
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SILVER SPONSORThe organizers expres
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PL-1HOW TO DESIGN OPTIMAL CATALYTIC
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MULTIFUNCTIONAL DEVICES FOR INTENSI
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PL-3DESIGN OF CATALYTIC PROCESSES F
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PL-3Indeed preparation and testing
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PL-4The second part of the lecture
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PL-5Reactor designs with intensifie
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PL-6MEMBRANE REACTORS: STATE OF THE
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KEY-NOTE PRESENTATIONS
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KN-1description, that can be charac
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KN-2selective catalytic reduction o
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KN-3Fig. 1. Experimental burner of
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KN-4~200°C. This is based on the H
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KN-5for addressing the quality of t
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KN-6reaction with ethanol and the b
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KN-7at temperature lower than 873K,
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REACTION KINETICS AND REACTION ENHA
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OP-I-2RELATION BETWEEN THE ACTIVATI
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COMPARISON OF CHEMICAL AND ENZYMATI
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OP-I-4NONLINEAR PHENOMENA DURING ME
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OP-I-5SPECIFICITY OF THE OSCILLATIO
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OP-I-6TRENDS IN BISTABILITY DOMAINS
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OP-I-7NON-STEADY-STATE CATALYST CHA
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OP-I-8TRANSIENT KINETIC STUDIES OF
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OP-I-9A REDOX KINETICS FOR THE PART
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OP-I-9500Flow of Air = 0.3 m 3 (STP
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OP-I-11ELUCIDATION OF THE REACTIVIT
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KINETIC MODELLING OF THE JOINT TRAN
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OP-I-13n-HEXANE SKELETAL ISOMERIZAT
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OP-I-14the slow branch of kinetic c
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OP-I-15The hydride palladium comple
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Energy Conservation (field j)∂∂
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OP-I-17Selectivity (mol. %)10099989
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OP-I-18According to GLC the main pr
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OP-I-19and slug dimensions, formati
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OP-I-20A RANS volume of fluids [1]
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OP-I-21the physical-chemical charac
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OP-I-22calculated values of pressur
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OP-I-23where L c - capillary length
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OP-I-24and diffuse transmission thr
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OP-I-25effect of bubble break-up wo
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OP-I-26strong influence on the soli
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OP-I-27wHCOOH=1+K2K1(1 + K3⋅ P⋅
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OP-I-28dimensional profiles detecte
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OP-I-29results. The results of the
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OP-I-30Fig. 1. Hydrodynamics and co
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OP-I-31Convection and diffusion wit
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TEMPERATURE RISE DURING REGENERATIO
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OP-II-2[4]. Similar temperature pro
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OP-II-3(Fig, 1 a, b) upon testing i
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OP-II-4In the second step optimizat
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OP-II-5membrane contactors were stu
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OP-II-6reaction over Cu/CeO 2-x cat
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OP-II-7is modelled by means of a tw
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OP-II-8the reactor [6]. However, th
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OP-II-9Figure 1. Computed volume fr
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OP-II-10assumes variables’ distri
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OP-II-11oxide support, it comes tha
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OP-II-12was connected to G.C. via s
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OP-II-13catalyst bed was 6 mm. Thre
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OP-II-14as coolant is an important
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OP-II-15Flow (L/h)7654321Bottoms ra
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OP-II-16(4) The gas recirculation r
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OP-II-17Catalytic reactions were ca
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OP-II-18At steady surface coverage
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OP-II-19gaimpulsegeneratorwateFig.
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OP-II-20examined (see Figure 1). Th
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OP-II-21References[1]. M.P. Dudukov
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OP-II-22of the hydrogen oxidation a
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OP-II-23TemperaturesensorsThe efflu
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OP-II-24of reactant conversions. Pa
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OP-II-25(surface) ‘wall-reaction
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OP-II-26It was found that the 10 wt
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OP-II-27non-flow type. During the M
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OP-III-A-1A NEW SIMPLE MICROCHANNEL
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BUBBLING FLUIDISED BED PYROLYSIS OF
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PINEWOOD PYROLYSIS UNDER VACUUM CON
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OP-III-A-5PYROLYSIS OF HDPE IN A CO
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OP-III-A-6REACTORS FOR THE GREEN TR
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DEHYDRATION OF GLYCEROL TO ACROLEIN
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OP-III-A-8LACTIC ACID BASED ON BIO
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RECOVERY OF ACETIC ACID FROM PYROLY
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OP-III-A-10LIPASE-CATALYZED REACTIO
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OP-III-A-11INVESTIGATION ON THERMOC
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OP-III-A-12SELECTIVE CATALYTIC DEOX
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ETHANOL STEAM REFORMING OVER COBALT
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OP-III-A-14HYDROTREATMENT CATALYSTS
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ORAL PRESENTATIONSSECTION IIIChemic
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OP-III-B-1Reactor parameters:Intern
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OP-III-B-2JOINT STEAM REFORMING OF
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OP-III-B-3LANDFILL BIOGAS PURIFICAT
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OP-III-B-4MODELING AND SIMULATION O
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OP-III-B-5DemonstratorThe medium-te
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OP-III-B-630/19.6 Nl/min (space vel
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OP-III-B-7mixed in the ratios: 94,8
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OP-III-B-8Table 1.Material balance
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OP-III-B-9Based on the results of t
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OP-III-B-10On this basis it can be
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OP-III-B-11Similar trends caused by
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OP-III-B-12(mol/s g cat)x108r4,6-DM
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OP-III-B-13carbon in Wyoming coal i
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OP-III-B-14MODELING PRODUCT DISTRIB
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OP-III-B-15COMBINED TECHNOLOGY OF U
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MATEMATICAL MODEL FOR DOWNDRAFT BIO
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OP-III-B-17CATALYTIC DEHYDRATION OF
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OP-III-B-18SYNGAS AND HYDROGEN PROD
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POSTER PRESENTATIONSSECTION I
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PP-I-1influence of the direction of
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PP-I-2At the agitation of the liqui
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PP-I-3NOLINEAR PHENOMENA IN CATALYT
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PP-I-4A NEW APPROACH TO KINETIC STU
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PP-I-5KINETICS OF PROX REACTION OVE
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PP-I-6PHENOMENA OF SUPERADIABATIC T
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ELECTROMAGNETIC REACTOR OF WATER TR
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PP-I-8DIRECT SYNTHESIS OF HYDROGEN
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PP-I-9DYNAMICS OF FIRST-ORDER PHASE
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PP-I-10ELECTROCHEMICAL OXIDATION OF
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PP-I-11CHEMPAK SOFTWARE PACKAGE: OP
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PP-I-12COMPUTER SIMULATION OF ENDOT
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PP-I-13MODELLING KINETICS OF PROCES
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PP-I-14THE INVESTIGATION OF REACTIO
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PP-I-15The qualitative picture of s
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Thus, knowing the composition of ra
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PP-I-17current density. Preliminary
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PP-I-18Hydrogenation kinetics was d
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PP-I-19the active mixing, amplitude
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PP-I-20where r, h indicate the radi
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PP-I-21model is very anisotropic be
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PP-I-22- Reduction of the number of
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PP-I-23oscillations of intermediate
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PP-I-25SYNTHESIS OF ETHYLENE OXIDE
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PP-I-26OPTIMUM KINETICS FOR POLYSTY
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PP-I-27TableSpecific surface area (
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PP-I-28γ-preirradiated sample), th
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PP-I-29commercial CFD solver FLUENT
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PP-I-30modulus, a considerable decr
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PP-I-31The destruction ways of CF 3
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PP-I-32[7]. Karoor S, Sirkar K. Gas
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PP-I-33above 750°. The catalytic p
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PP-I-35REVERSE FLOW REACTOR WITH FO
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FLOW-RECIRCULATION METHOD FOR INVES
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TO A PROBLEM OF OPTIMIZATION OF FUN
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PP-I-38THE INFLUENCE OF REACTION MI
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PP-I-39METHANOL OXIDATIVE STEAM REF
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PP-I-41CORRECT INVESTIGATION OF THE
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PP-I-42NEW APPROACH OF DEFINITION O
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PP-I-43STREAM HEAT EXCHANGE OF AERO
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PP-I-44HIGH TEMPERATURE OXYGEN TRAN
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PP-I-45KINETICS OF TRANSESTERIFICAT
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MATHEMATICAL MODELING AND OPTIMIZAT
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PP-I-47The basic side reaction is r
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PP-I-49EXPERIMENTAL STUDY OF THE HA
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PP-I-51ON THE KINETICS AND REGULARI
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PP-I-52DIFFERENTIAL THERMAL ANALYSI
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PP-I-53oxidation reaction demonstra
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PP-I-54of reaction. It is establish
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PP-I-55effects, are energetically c
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PP-I-56The experiments and simulati
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PP-I-57In the studied range of temp
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PP-I-58HeadingsAdvances in Chemical
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PP-I-59calculated. During the aroma
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PP-I-60with honeycomb catalyst) act
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Т - temperature, K, D eff - effect
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PP-I-62stirring rate were adopted u
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PP-I-63m 2 = (k 1 y 0 1 +k -1 +k 1
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POSTER PRESENTATIONSSECTION II
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PP-II-1values of operating paramete
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⎡⎛⎢⎜bF⎣⎝=2ab ⎞ 6+ ⎟
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PP-II-4HONEYCOMB MONOLITHIC CATALYS
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MATHEMATICAL MODELING OF THE ALUMIN
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PP-II-6MODELING OF VINYL ACETATE SY
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PP-II-7СENTRIFUGAL DISK REACTORAvv
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PP-II-83) An opportunity of operati
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PP-II-10UV-ACTIVATION OF METHANE CO
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PP-II-11COMBINED APPROACH (FMEA- HA
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PP-II-12Testing the pilot variant o
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PP-II-14NOVEL MICROREACTOR FOR THE
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PP-II-15of 1-2.5 lead to a decreasi
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PP-II-16stages. Kinetic parameters
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PP-II-17whiskers, which assure an a
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PP-II-18с m , с cat - density of
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PP-II-19decrease. So, the potential
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PP-II-20products became a mixture o
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PP-II-21A numerical algorithm and s
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PP-II-22motions at any external con
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PP-II-23One of the main technologic
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PP-II-24100 m x 250 μm x 0.5 μm,
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PP-II-25A model was developed to ca
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PP-II-26The results of calculations
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PP-II-27modes of reaction and two d
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PP-II-29OZONE-DESTRUCTION REACTOR B
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PP-II-30Fig. 1. Axial profile of me
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PP-II-31isobutylene in butene fract
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PP-II-322.5x10 -3 ( i )2.5x10 -3 (
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PP-II-33No olefinreadsorptionWith o
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PP-II-34using titania or Ag-doped t
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PP-II-35accidents, is condition dep
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Page 401 and 402: PP-II-37the solid phase solute conc
Page 403 and 404: PP-II-38As shown in Table 1, the ca
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Page 407 and 408: PP-II-40Hydrodynamic regime in the
Page 409 and 410: PP-II-41activity, relative unit1,21
Page 411 and 412: PP-II-42One of the major indicators
Page 413 and 414: PP-II-43These conditions are confor
Page 415 and 416: PP-II-44For the hepten, alpha-methy
Page 417 and 418: PP-II-46PARTIAL OXIDATION OF METHAN
Page 419 and 420: PP-II-47DEVELOPMENT OF VORTEX APPAR
Page 421 and 422: MODELING OF CFTALYTIC α-OLEFINS OL
Page 423 and 424: PP-II-49Hinselwood kinetic equation
Page 425 and 426: 3) iterate concentrations at a cut
Page 427 and 428: PP-II-51data such flow sheet provid
Page 429 and 430: PP-II-53ON THE TECNOLOGY OF TECHNIC
Page 431 and 432: PP-II-54PROPYLENE POLYMERIZATION AN
Page 433 and 434: REACTOR FOR LIQUID-PHASE PROCESSES
Page 435 and 436: PP-II-56MODELING OF CATALYTIC MICRO
Page 437 and 438: PP-II-57MATHEMATICAL MODELING OF BE
Page 439 and 440: PP-II-58HONEYCOMB CATALYSTS WITH PO
Page 441 and 442: POSTER PRESENTATIONSSECTION IIISECT
Page 443 and 444: ReferencesPP-III-1[1]. A.N. Pestrya
Page 445 and 446: PP-III-2Table1. Percentages of diff
Page 447 and 448: PP-III-3conversion for the reaction
Page 449: PP-III-4900Reformer temperature (K)
Page 453 and 454: PP-III-6optimization permit better
Page 455 and 456: PP-III-8DE-NO X SYSTEM BASED ON H 2
Page 457 and 458: PP-III-9SEPARATION BETWEEN CHLORIDE
Page 459 and 460: CONVERSION OF WASTE COTTON TO BIOET
Page 461 and 462: PP-III-12THE METHOD OF GLYCERIC ACI
Page 463 and 464: NOx conversion vs. temperature is p
Page 465 and 466: PP-III-14intermetallic diffusion at
Page 467 and 468: PP-III-15The conversion of O 2 was
Page 469 and 470: PP-III-16H 2consumpition (a.u)(a)39
Page 471 and 472: PP-III-17the characteristic structu
Page 473 and 474: PP-III-18Figure 1. Influence of tem
Page 475 and 476: PP-III-19(a)(b)CH 4conversion, %100
Page 477 and 478: PP-III-20take into account own size
Page 479 and 480: PP-III-2110080CS-18CS-34CHZ30CHZ801
Page 481 and 482: EXPERIMENTALPP-III-22We synthesized
Page 483 and 484: PP-III-23Base composition component
Page 485 and 486: PP-III-25CO REMOVAL AT THE MICROSCA
Page 487 and 488: HYDROGEN PRODUCTION FROM METHANOL U
Page 489 and 490: PP-III-27NON CATALITIC PRODUCTION O
Page 491 and 492: PP-III-28Different reaction conditi
Page 493 and 494: PP-III-29followed by WGS reaction.
Page 495 and 496: PP-III-30As a solvent-coreactants w
Page 497 and 498: PP-III-31It was concluded that on t
Page 499 and 500: PP-III-32Hydrogenolysis of glycerol
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PP-III-331,6W 0, μmol Н 2/min1,20
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PP-III-34preparation (glass fiber f
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PP-III-35In the modification proces
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PP-III-36The kinetics of acid hydro
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PP-III-37reaction: i) C=O double bo
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PP-III-38methane and carbon monoxid
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PP-III-39from 25 to 60, which was d
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PP-III-401% w/w for Pd with respect
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PP-III-41material. Besides, the mol
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PP-III-43METHANOL AND DIMETHYL ETHE
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PP-III-44goal is attained by using
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OLIGOMERISATION OF TERTIARY AMINE L
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PP-III-47meter (Shimazu Co.; TOC-50
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PP-III-48the range of 29-87 kJ/mol
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PP-III-49determine the optimal type
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PP-III-50NEW CONCEPT FOR A SELF CLE
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PP-III-51HYDROGEN PRODUCTION BY MET
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PP-III-52CATALYTIC UPGRADING OF PRO
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PP-III-53CATALYTIC CONVERSION OF FI
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PROCESS FOR THE PRODUCTION OF BUTYL
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PP-III-55been previously fixed and
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PP-III-56The influence of reaction
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PP-III-57sample does not contain so
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PP-III-58The re-activation of the e
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PP-III-59The aim of this work is th
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PP-III-61BIODIESEL FROM MICROALGAE
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DEVELOPING MICROFLUIDIC DEVICE WITH
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THREE-PHASE DIRECT OILS HYDROGENATI
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Co-BASED CATALYSTS FOR THE HYDROLYS
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PP-III-65KINETIC STUDY OF THE CATAL
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PP-III-66PRODUCTION OF HYDROGEN AND
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PP-III-67ENHANCED GASIFICATION OF P
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PP-III-68INFLUENCE OF SPILLOVER ON
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PP-III-69AEROBIC OXIDATIVE COUPLING
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PP-III-70MECHANISMS FOR CHEMICAL RE
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PP-III-70SBS molecules and increase
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PP-III-71and as a resut, could enha
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PP-III-72conversion). Al 2 O 3 /PSS
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PP-III-73SBA50TiSBA% Transmittance5
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PP-III-74stove heating. Another par
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PP-III-75TG [%]0-10-20-30380°C400
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PP-III-76The elementary version of
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PP-III-77thermodynamically enhanced
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PP-III-78GFC textileStructuringmeta
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PP-III-79All the prepared spinel-ox
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PP-III-80Our new process is polluti
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PP-III-81Fig. 1. Scheme of the biog
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PP-III-82Pic. 1 Pic. 2Pic. 1. Schem
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ARKHIPOV Vladimir AfanasievichResea
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CENTENO Felipe OrlandoNúcleo de Ex
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FLID Mark RafailovichScientific Res
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HOSEN Mohammad AnwarUniversity of M
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KOZLOVA EkaterinaBoreskov Institute
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MAKARSHIN Lev LvovichBoreskov Insti
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ONSAN Zeynep IlsenDepartment of Che
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REBOLLAR MoisesInstituto De Investi
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SHEIKH Munir AhmedTraining and Staf
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SULMAN Esfir MikhailovnaTver Techni
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ZHAPBASBYEV Uzak KairbekovichKazakh
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OP-I-3 Pécar D., Gorsek A.COMPARIS
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OP-II-3Kucherov A.V., Finashina E.D
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OP-III-A-9 Rasrendra C.B., Girisuta
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PP-I-9Bykov V., Tsybenova S.B.DYNAM
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PP-I-43 Pechenegov Y.Y., Kuzmina R.
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PP-II-10 Basov N.L., Oreshkin I., T
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PP-II-45 Stepanek J., Koci P., Kubi
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PP-III-19 Fedorova Z.A., Danilova M
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PP-III-53 Pölczmann G., Valyon J.,
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XIX International Conference on Che
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