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PLENARY LECTURES
PLENARY LECTURES
PL-1HOW TO DESIGN <strong>OP</strong>TIMAL CATALYTIC REACTOR?HONORARY PLENARY LECTURE DEDICATED TO PROFESSORMIKHAIL SLIN’KOYurii Sh. MatrosPresident of Matros Technologies, Inc., St. Louis, MO 63017, USA,E-mail: yurii@matrostech.comProfessor Mikhail Gavrilovich Slin’ko (1914-2009) was a watershed figure inRussian chemical process engineering. Though he published little and was not verywell-known in the West, he is merited among other leading scholars, whichestablished the chemical reaction engineering discipline in its present state.In the beginning of his carrier just after World War <strong>II</strong>, M. G. Slin’ko was activelyinvolved in heavy water production through hydrogen isotope separation. This was asecret Soviet weaponry project quickly realized in large scale. As M.G. Slin’ko noted[1], the development was based on calculations and direct scale-up without lengthystages of pilot testing. At approximately the same time, Prof. G. K. Boreskov andM.G. Slin’ko developed sulfuric acid reactors using advanced technique involvingchemical kinetics, transport phenomena, and rigorous mathematical optimization.Apparently, from these early works, M. G. Slin’ko understood power of physicchemicalmodels for industrial process engineering.From 1957 to beginning of 70 s , M.G. Slin’ko built a team of enthusiastic youngscientists and engineers in headed by him Department of Mathematical Modeling inthe newly created Institute of Catalysis (Novosibirsk, Russia). His own and hisstudents contributions at this time form a basis for his legacy. M.G. Slin’ko’s curiouslycombined great research and educational activities with vigorous publicizing hismathematical modeling method and results of the Department to Soviet and thenRussian chemical engineers.His commandments for the designers of heterogeneous catalytic processes (seefor example [1]) included:− building a kinetic model as an essential step of reactor design,− exploring theoretical-optimal conditions and revealing fully maximumpotential of the catalyst,7
- Page 1 and 2: Boreskov Institute of Catalysisof t
- Page 3 and 4: INTERNATIONAL SCIENTIFIC COMMITTEEV
- Page 5: SILVER SPONSORThe organizers expres
- Page 9 and 10: MULTIFUNCTIONAL DEVICES FOR INTENSI
- Page 11 and 12: PL-3DESIGN OF CATALYTIC PROCESSES F
- Page 13 and 14: PL-3Indeed preparation and testing
- Page 15 and 16: PL-4The second part of the lecture
- Page 17 and 18: PL-5Reactor designs with intensifie
- Page 19 and 20: PL-6MEMBRANE REACTORS: STATE OF THE
- Page 21 and 22: KEY-NOTE PRESENTATIONS
- Page 23 and 24: KN-1description, that can be charac
- Page 25 and 26: KN-2selective catalytic reduction o
- Page 27 and 28: KN-3Fig. 1. Experimental burner of
- Page 29 and 30: KN-4~200°C. This is based on the H
- Page 31 and 32: KN-5for addressing the quality of t
- Page 33 and 34: KN-6reaction with ethanol and the b
- Page 35 and 36: KN-7at temperature lower than 873K,
- Page 37 and 38: REACTION KINETICS AND REACTION ENHA
- Page 39 and 40: OP-I-2RELATION BETWEEN THE ACTIVATI
- Page 41 and 42: COMPARISON OF CHEMICAL AND ENZYMATI
- Page 43 and 44: OP-I-4NONLINEAR PHENOMENA DURING ME
- Page 45 and 46: OP-I-5SPECIFICITY OF THE OSCILLATIO
- Page 47 and 48: OP-I-6TRENDS IN BISTABILITY DOMAINS
- Page 49 and 50: OP-I-7NON-STEADY-STATE CATALYST CHA
- Page 51 and 52: OP-I-8TRANSIENT KINETIC STUDIES OF
- Page 53 and 54: OP-I-9A REDOX KINETICS FOR THE PART
- Page 55 and 56: OP-I-9500Flow of Air = 0.3 m 3 (STP
- Page 57 and 58:
OP-I-11ELUCIDATION OF THE REACTIVIT
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KINETIC MODELLING OF THE JOINT TRAN
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OP-I-13n-HEXANE SKELETAL ISOMERIZAT
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OP-I-14the slow branch of kinetic c
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OP-I-15The hydride palladium comple
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Energy Conservation (field j)∂∂
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OP-I-17Selectivity (mol. %)10099989
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OP-I-18According to GLC the main pr
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OP-I-19and slug dimensions, formati
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OP-I-20A RANS volume of fluids [1]
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OP-I-21the physical-chemical charac
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OP-I-22calculated values of pressur
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OP-I-23where L c - capillary length
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OP-I-24and diffuse transmission thr
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OP-I-25effect of bubble break-up wo
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OP-I-26strong influence on the soli
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OP-I-27wHCOOH=1+K2K1(1 + K3⋅ P⋅
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OP-I-28dimensional profiles detecte
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OP-I-29results. The results of the
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OP-I-30Fig. 1. Hydrodynamics and co
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OP-I-31Convection and diffusion wit
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TEMPERATURE RISE DURING REGENERATIO
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OP-II-2[4]. Similar temperature pro
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OP-II-3(Fig, 1 a, b) upon testing i
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OP-II-4In the second step optimizat
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OP-II-5membrane contactors were stu
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OP-II-6reaction over Cu/CeO 2-x cat
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OP-II-7is modelled by means of a tw
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OP-II-8the reactor [6]. However, th
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OP-II-9Figure 1. Computed volume fr
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OP-II-10assumes variables’ distri
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OP-II-11oxide support, it comes tha
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OP-II-12was connected to G.C. via s
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OP-II-13catalyst bed was 6 mm. Thre
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OP-II-14as coolant is an important
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OP-II-15Flow (L/h)7654321Bottoms ra
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OP-II-16(4) The gas recirculation r
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OP-II-17Catalytic reactions were ca
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OP-II-18At steady surface coverage
- Page 135 and 136:
OP-II-19gaimpulsegeneratorwateFig.
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OP-II-20examined (see Figure 1). Th
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OP-II-21References[1]. M.P. Dudukov
- Page 141 and 142:
OP-II-22of the hydrogen oxidation a
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OP-II-23TemperaturesensorsThe efflu
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OP-II-24of reactant conversions. Pa
- Page 147 and 148:
OP-II-25(surface) ‘wall-reaction
- Page 149 and 150:
OP-II-26It was found that the 10 wt
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OP-II-27non-flow type. During the M
- Page 153 and 154:
OP-III-A-1A NEW SIMPLE MICROCHANNEL
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BUBBLING FLUIDISED BED PYROLYSIS OF
- Page 157 and 158:
PINEWOOD PYROLYSIS UNDER VACUUM CON
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OP-III-A-5PYROLYSIS OF HDPE IN A CO
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OP-III-A-6REACTORS FOR THE GREEN TR
- Page 163 and 164:
DEHYDRATION OF GLYCEROL TO ACROLEIN
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OP-III-A-8LACTIC ACID BASED ON BIO
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RECOVERY OF ACETIC ACID FROM PYROLY
- Page 169 and 170:
OP-III-A-10LIPASE-CATALYZED REACTIO
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OP-III-A-11INVESTIGATION ON THERMOC
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OP-III-A-12SELECTIVE CATALYTIC DEOX
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ETHANOL STEAM REFORMING OVER COBALT
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OP-III-A-14HYDROTREATMENT CATALYSTS
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ORAL PRESENTATIONSSECTION IIIChemic
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OP-III-B-1Reactor parameters:Intern
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OP-III-B-2JOINT STEAM REFORMING OF
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OP-III-B-3LANDFILL BIOGAS PURIFICAT
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OP-III-B-4MODELING AND SIMULATION O
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OP-III-B-5DemonstratorThe medium-te
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OP-III-B-630/19.6 Nl/min (space vel
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OP-III-B-7mixed in the ratios: 94,8
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OP-III-B-8Table 1.Material balance
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OP-III-B-9Based on the results of t
- Page 199 and 200:
OP-III-B-10On this basis it can be
- Page 201 and 202:
OP-III-B-11Similar trends caused by
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OP-III-B-12(mol/s g cat)x108r4,6-DM
- Page 205 and 206:
OP-III-B-13carbon in Wyoming coal i
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OP-III-B-14MODELING PRODUCT DISTRIB
- Page 209 and 210:
OP-III-B-15COMBINED TECHNOLOGY OF U
- Page 211 and 212:
MATEMATICAL MODEL FOR DOWNDRAFT BIO
- Page 213 and 214:
OP-III-B-17CATALYTIC DEHYDRATION OF
- Page 215 and 216:
OP-III-B-18SYNGAS AND HYDROGEN PROD
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POSTER PRESENTATIONSSECTION I
- Page 219 and 220:
PP-I-1influence of the direction of
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PP-I-2At the agitation of the liqui
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PP-I-3NOLINEAR PHENOMENA IN CATALYT
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PP-I-4A NEW APPROACH TO KINETIC STU
- Page 227 and 228:
PP-I-5KINETICS OF PROX REACTION OVE
- Page 229 and 230:
PP-I-6PHENOMENA OF SUPERADIABATIC T
- Page 231 and 232:
ELECTROMAGNETIC REACTOR OF WATER TR
- Page 233 and 234:
PP-I-8DIRECT SYNTHESIS OF HYDROGEN
- Page 235 and 236:
PP-I-9DYNAMICS OF FIRST-ORDER PHASE
- Page 237 and 238:
PP-I-10ELECTROCHEMICAL OXIDATION OF
- Page 239 and 240:
PP-I-11CHEMPAK SOFTWARE PACKAGE: OP
- Page 241 and 242:
PP-I-12COMPUTER SIMULATION OF ENDOT
- Page 243 and 244:
PP-I-13MODELLING KINETICS OF PROCES
- Page 245 and 246:
PP-I-14THE INVESTIGATION OF REACTIO
- Page 247 and 248:
PP-I-15The qualitative picture of s
- Page 249 and 250:
Thus, knowing the composition of ra
- Page 251 and 252:
PP-I-17current density. Preliminary
- Page 253 and 254:
PP-I-18Hydrogenation kinetics was d
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PP-I-19the active mixing, amplitude
- Page 257 and 258:
PP-I-20where r, h indicate the radi
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PP-I-21model is very anisotropic be
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PP-I-22- Reduction of the number of
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PP-I-23oscillations of intermediate
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PP-I-25SYNTHESIS OF ETHYLENE OXIDE
- Page 267 and 268:
PP-I-26OPTIMUM KINETICS FOR POLYSTY
- Page 269 and 270:
PP-I-27TableSpecific surface area (
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PP-I-28γ-preirradiated sample), th
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PP-I-29commercial CFD solver FLUENT
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PP-I-30modulus, a considerable decr
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PP-I-31The destruction ways of CF 3
- Page 279 and 280:
PP-I-32[7]. Karoor S, Sirkar K. Gas
- Page 281 and 282:
PP-I-33above 750°. The catalytic p
- Page 283 and 284:
PP-I-35REVERSE FLOW REACTOR WITH FO
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FLOW-RECIRCULATION METHOD FOR INVES
- Page 287 and 288:
TO A PROBLEM OF OPTIMIZATION OF FUN
- Page 289 and 290:
PP-I-38THE INFLUENCE OF REACTION MI
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PP-I-39METHANOL OXIDATIVE STEAM REF
- Page 293 and 294:
PP-I-41CORRECT INVESTIGATION OF THE
- Page 295 and 296:
PP-I-42NEW APPROACH OF DEFINITION O
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PP-I-43STREAM HEAT EXCHANGE OF AERO
- Page 299 and 300:
PP-I-44HIGH TEMPERATURE OXYGEN TRAN
- Page 301 and 302:
PP-I-45KINETICS OF TRANSESTERIFICAT
- Page 303 and 304:
MATHEMATICAL MODELING AND OPTIMIZAT
- Page 305 and 306:
PP-I-47The basic side reaction is r
- Page 307 and 308:
PP-I-49EXPERIMENTAL STUDY OF THE HA
- Page 309 and 310:
PP-I-51ON THE KINETICS AND REGULARI
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PP-I-52DIFFERENTIAL THERMAL ANALYSI
- Page 313 and 314:
PP-I-53oxidation reaction demonstra
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PP-I-54of reaction. It is establish
- Page 317 and 318:
PP-I-55effects, are energetically c
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PP-I-56The experiments and simulati
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PP-I-57In the studied range of temp
- Page 323 and 324:
PP-I-58HeadingsAdvances in Chemical
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PP-I-59calculated. During the aroma
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PP-I-60with honeycomb catalyst) act
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Т - temperature, K, D eff - effect
- Page 331 and 332:
PP-I-62stirring rate were adopted u
- Page 333 and 334:
PP-I-63m 2 = (k 1 y 0 1 +k -1 +k 1
- Page 335 and 336:
POSTER PRESENTATIONSSECTION II
- Page 337 and 338:
PP-II-1values of operating paramete
- Page 339 and 340:
⎡⎛⎢⎜bF⎣⎝=2ab ⎞ 6+ ⎟
- Page 341 and 342:
PP-II-4HONEYCOMB MONOLITHIC CATALYS
- Page 343 and 344:
MATHEMATICAL MODELING OF THE ALUMIN
- Page 345 and 346:
PP-II-6MODELING OF VINYL ACETATE SY
- Page 347 and 348:
PP-II-7СENTRIFUGAL DISK REACTORAvv
- Page 349 and 350:
PP-II-83) An opportunity of operati
- Page 351 and 352:
PP-II-10UV-ACTIVATION OF METHANE CO
- Page 353 and 354:
PP-II-11COMBINED APPROACH (FMEA- HA
- Page 355 and 356:
PP-II-12Testing the pilot variant o
- Page 357 and 358:
PP-II-14NOVEL MICROREACTOR FOR THE
- Page 359 and 360:
PP-II-15of 1-2.5 lead to a decreasi
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PP-II-16stages. Kinetic parameters
- Page 363 and 364:
PP-II-17whiskers, which assure an a
- Page 365 and 366:
PP-II-18с m , с cat - density of
- Page 367 and 368:
PP-II-19decrease. So, the potential
- Page 369 and 370:
PP-II-20products became a mixture o
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PP-II-21A numerical algorithm and s
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PP-II-22motions at any external con
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PP-II-23One of the main technologic
- Page 377 and 378:
PP-II-24100 m x 250 μm x 0.5 μm,
- Page 379 and 380:
PP-II-25A model was developed to ca
- Page 381 and 382:
PP-II-26The results of calculations
- Page 383 and 384:
PP-II-27modes of reaction and two d
- Page 385 and 386:
PP-II-29OZONE-DESTRUCTION REACTOR B
- Page 387 and 388:
PP-II-30Fig. 1. Axial profile of me
- Page 389 and 390:
PP-II-31isobutylene in butene fract
- Page 391 and 392:
PP-II-322.5x10 -3 ( i )2.5x10 -3 (
- Page 393 and 394:
PP-II-33No olefinreadsorptionWith o
- Page 395 and 396:
PP-II-34using titania or Ag-doped t
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PP-II-35accidents, is condition dep
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PP-II-36be seen that at temperature
- Page 401 and 402:
PP-II-37the solid phase solute conc
- Page 403 and 404:
PP-II-38As shown in Table 1, the ca
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PP-II-39better to the obtained in t
- Page 407 and 408:
PP-II-40Hydrodynamic regime in the
- Page 409 and 410:
PP-II-41activity, relative unit1,21
- Page 411 and 412:
PP-II-42One of the major indicators
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PP-II-43These conditions are confor
- Page 415 and 416:
PP-II-44For the hepten, alpha-methy
- Page 417 and 418:
PP-II-46PARTIAL OXIDATION OF METHAN
- Page 419 and 420:
PP-II-47DEVELOPMENT OF VORTEX APPAR
- Page 421 and 422:
MODELING OF CFTALYTIC α-OLEFINS OL
- Page 423 and 424:
PP-II-49Hinselwood kinetic equation
- Page 425 and 426:
3) iterate concentrations at a cut
- Page 427 and 428:
PP-II-51data such flow sheet provid
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PP-II-53ON THE TECNOLOGY OF TECHNIC
- Page 431 and 432:
PP-II-54PROPYLENE POLYMERIZATION AN
- Page 433 and 434:
REACTOR FOR LIQUID-PHASE PROCESSES
- Page 435 and 436:
PP-II-56MODELING OF CATALYTIC MICRO
- Page 437 and 438:
PP-II-57MATHEMATICAL MODELING OF BE
- Page 439 and 440:
PP-II-58HONEYCOMB CATALYSTS WITH PO
- Page 441 and 442:
POSTER PRESENTATIONSSECTION IIISECT
- Page 443 and 444:
ReferencesPP-III-1[1]. A.N. Pestrya
- Page 445 and 446:
PP-III-2Table1. Percentages of diff
- Page 447 and 448:
PP-III-3conversion for the reaction
- Page 449 and 450:
PP-III-4900Reformer temperature (K)
- Page 451 and 452:
PP-III-5Catalytic performance of th
- Page 453 and 454:
PP-III-6optimization permit better
- Page 455 and 456:
PP-III-8DE-NO X SYSTEM BASED ON H 2
- Page 457 and 458:
PP-III-9SEPARATION BETWEEN CHLORIDE
- Page 459 and 460:
CONVERSION OF WASTE COTTON TO BIOET
- Page 461 and 462:
PP-III-12THE METHOD OF GLYCERIC ACI
- Page 463 and 464:
NOx conversion vs. temperature is p
- Page 465 and 466:
PP-III-14intermetallic diffusion at
- Page 467 and 468:
PP-III-15The conversion of O 2 was
- Page 469 and 470:
PP-III-16H 2consumpition (a.u)(a)39
- Page 471 and 472:
PP-III-17the characteristic structu
- Page 473 and 474:
PP-III-18Figure 1. Influence of tem
- Page 475 and 476:
PP-III-19(a)(b)CH 4conversion, %100
- Page 477 and 478:
PP-III-20take into account own size
- Page 479 and 480:
PP-III-2110080CS-18CS-34CHZ30CHZ801
- Page 481 and 482:
EXPERIMENTALPP-III-22We synthesized
- Page 483 and 484:
PP-III-23Base composition component
- Page 485 and 486:
PP-III-25CO REMOVAL AT THE MICROSCA
- Page 487 and 488:
HYDROGEN PRODUCTION FROM METHANOL U
- Page 489 and 490:
PP-III-27NON CATALITIC PRODUCTION O
- Page 491 and 492:
PP-III-28Different reaction conditi
- Page 493 and 494:
PP-III-29followed by WGS reaction.
- Page 495 and 496:
PP-III-30As a solvent-coreactants w
- Page 497 and 498:
PP-III-31It was concluded that on t
- Page 499 and 500:
PP-III-32Hydrogenolysis of glycerol
- Page 501 and 502:
PP-III-331,6W 0, μmol Н 2/min1,20
- Page 503 and 504:
PP-III-34preparation (glass fiber f
- Page 505 and 506:
PP-III-35In the modification proces
- Page 507 and 508:
PP-III-36The kinetics of acid hydro
- Page 509 and 510:
PP-III-37reaction: i) C=O double bo
- Page 511 and 512:
PP-III-38methane and carbon monoxid
- Page 513 and 514:
PP-III-39from 25 to 60, which was d
- Page 515 and 516:
PP-III-401% w/w for Pd with respect
- Page 517 and 518:
PP-III-41material. Besides, the mol
- Page 519 and 520:
PP-III-43METHANOL AND DIMETHYL ETHE
- Page 521 and 522:
PP-III-44goal is attained by using
- Page 523 and 524:
OLIGOMERISATION OF TERTIARY AMINE L
- Page 525 and 526:
PP-III-47meter (Shimazu Co.; TOC-50
- Page 527 and 528:
PP-III-48the range of 29-87 kJ/mol
- Page 529 and 530:
PP-III-49determine the optimal type
- Page 531 and 532:
PP-III-50NEW CONCEPT FOR A SELF CLE
- Page 533 and 534:
PP-III-51HYDROGEN PRODUCTION BY MET
- Page 535 and 536:
PP-III-52CATALYTIC UPGRADING OF PRO
- Page 537 and 538:
PP-III-53CATALYTIC CONVERSION OF FI
- Page 539 and 540:
PROCESS FOR THE PRODUCTION OF BUTYL
- Page 541 and 542:
PP-III-55been previously fixed and
- Page 543 and 544:
PP-III-56The influence of reaction
- Page 545 and 546:
PP-III-57sample does not contain so
- Page 547 and 548:
PP-III-58The re-activation of the e
- Page 549 and 550:
PP-III-59The aim of this work is th
- Page 551 and 552:
PP-III-61BIODIESEL FROM MICROALGAE
- Page 553 and 554:
DEVELOPING MICROFLUIDIC DEVICE WITH
- Page 555 and 556:
THREE-PHASE DIRECT OILS HYDROGENATI
- Page 557 and 558:
Co-BASED CATALYSTS FOR THE HYDROLYS
- Page 559 and 560:
PP-III-65KINETIC STUDY OF THE CATAL
- Page 561 and 562:
PP-III-66PRODUCTION OF HYDROGEN AND
- Page 563 and 564:
PP-III-67ENHANCED GASIFICATION OF P
- Page 565 and 566:
PP-III-68INFLUENCE OF SPILLOVER ON
- Page 567 and 568:
PP-III-69AEROBIC OXIDATIVE COUPLING
- Page 569 and 570:
PP-III-70MECHANISMS FOR CHEMICAL RE
- Page 571 and 572:
PP-III-70SBS molecules and increase
- Page 573 and 574:
PP-III-71and as a resut, could enha
- Page 575 and 576:
PP-III-72conversion). Al 2 O 3 /PSS
- Page 577 and 578:
PP-III-73SBA50TiSBA% Transmittance5
- Page 579 and 580:
PP-III-74stove heating. Another par
- Page 581 and 582:
PP-III-75TG [%]0-10-20-30380°C400
- Page 583 and 584:
PP-III-76The elementary version of
- Page 585 and 586:
PP-III-77thermodynamically enhanced
- Page 587 and 588:
PP-III-78GFC textileStructuringmeta
- Page 589 and 590:
PP-III-79All the prepared spinel-ox
- Page 591 and 592:
PP-III-80Our new process is polluti
- Page 593 and 594:
PP-III-81Fig. 1. Scheme of the biog
- Page 595 and 596:
PP-III-82Pic. 1 Pic. 2Pic. 1. Schem
- Page 597 and 598:
ARKHIPOV Vladimir AfanasievichResea
- Page 599 and 600:
CENTENO Felipe OrlandoNúcleo de Ex
- Page 601 and 602:
FLID Mark RafailovichScientific Res
- Page 603 and 604:
HOSEN Mohammad AnwarUniversity of M
- Page 605 and 606:
KOZLOVA EkaterinaBoreskov Institute
- Page 607 and 608:
MAKARSHIN Lev LvovichBoreskov Insti
- Page 609 and 610:
ONSAN Zeynep IlsenDepartment of Che
- Page 611 and 612:
REBOLLAR MoisesInstituto De Investi
- Page 613 and 614:
SHEIKH Munir AhmedTraining and Staf
- Page 615 and 616:
SULMAN Esfir MikhailovnaTver Techni
- Page 617 and 618:
ZHAPBASBYEV Uzak KairbekovichKazakh
- Page 619 and 620:
OP-I-3 Pécar D., Gorsek A.COMPARIS
- Page 621 and 622:
OP-II-3Kucherov A.V., Finashina E.D
- Page 623 and 624:
OP-III-A-9 Rasrendra C.B., Girisuta
- Page 625 and 626:
PP-I-9Bykov V., Tsybenova S.B.DYNAM
- Page 627 and 628:
PP-I-43 Pechenegov Y.Y., Kuzmina R.
- Page 629 and 630:
PP-II-10 Basov N.L., Oreshkin I., T
- Page 631 and 632:
PP-II-45 Stepanek J., Koci P., Kubi
- Page 633 and 634:
PP-III-19 Fedorova Z.A., Danilova M
- Page 635 and 636:
PP-III-53 Pölczmann G., Valyon J.,
- Page 637:
XIX International Conference on Che
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